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IEEE Transactions on Applied Superconductivity

Development toward high-speed integrated circuits and AQUID qubits with Nb/AlO/sub x//Nb josephson junctions

W. Chen, Vijay Patel, Sergey K. Tolpygo, Daniel T. Yohannes, Shawn Pottorf, James E. Lukens

Published Jun 1, 2003• 10 citations
Publisher

Abstract

Our Nb/AlO/sub x//Nb planarized process has been upgraded by adding extra dielectric and Nb wiring layers and the installation of an Inductively Coupled Plasma (ICP) etcher. Much higher quartz etch rates as well as reduced residue are achieved with ICP etch. Etch uniformities of both Nb and quartz are also improved significantly. Damage to Nb during the fabrication process has been investigated. We have found that dry etching in SF/sub 6/ plasma has a significant effect on the quality of Nb films under certain conditions with damage coinciding with the presence of in situ deposited Al.

DOI
10.1109/tasc.2003.813656

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Our Nb/AlO/sub x//Nb planarized process has been upgraded by adding extra dielectric and Nb wiring layers and the installation of an Inductively Coupled Plasma (ICP) etcher. Much higher quartz etch rates as well as reduced residue are achieved with ICP etch. Etch uniformities of both Nb and quartz are also improved significantly. Damage to Nb during the fabrication process has been investigated. We have found that dry etching in SF/sub 6/ plasma has a significant effect on the quality of Nb films under certain conditions with damage coinciding with the presence of in situ deposited Al.
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We have developed our next generation Nb integrated circuit process which offers higher performance, particularly for SFQ-type logic, and increased density compared to our present 2000 A/cm/sup 2/ foundry process. The new process is based on our existing Nb foundry process, but has been optimized to utilize more of the sub-micron alignment and exposure capabilities of our optical lithography tools. Minimum linepitch and junction size have been reduced to 2.5 /spl mu/m (from 4 /spl mu/m) and 1.75 /spl mu/m (from 2.5 /spl mu/m), respectively, and J/sub c/ has been increased to 4000 A/cm/sup 2/. These goals have been achieved by an overall reduction in layer thicknesses, implementation of SF/sub 6/ dry etch for metal line definition, and optimization of the photolithography process. The new process offers lower inductance wiring and substantially lower parasitic circuit inductances compared with the existing Nb foundry process. In this paper, we discuss these improvements and report parametric test data for devices fabricated in this process.
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A simple and robust process for fabricating low-T/sub c/ Josephson junction integrated circuits has been developed. The process is designed around the Nb/Al/sub 2/O/sub 3/-Al/Nb trilayer, and utilized nine masking steps to form two separate levels of trilayer Josephson junctions, as well as resistors, capacitors, and transmission lines. Materials used for interlayer dielectrics and passivation layers are silicon dioxide and silicon nitride formed by plasma-enhanced chemical vapor deposition (PECVD). The PECVD equipment yields a high deposition rate at moderate substrate temperatures. No degradation of the junction characteristics due to these depositions is seen. The measured loss tangent of this dielectric at 10 GHz using a parallel plate technique is 4.44*10/sup -4/. The dielectric constant of this material is 5.1 in the range of 50 to 400 GHz, measured using an on-chip resonator capacitively coupled to a single shunted Josephson junction. The physical quality of the oxide has been investigated using a variety of tests and has proven to be excellent. A variety of simple circuits using this process technology have been fabricated and tested. More complex circuits are currently under development.
We report on technique and results for superconductor electronics fabrication process, featuring customizable number of planarized superconducting layers. The novel technique enhanced yield on stackable vias of our standard planarized process (RIPPLE) by eliminating the need for an additional deposition of aluminum as an etch stop in the metal-via stack. The drawback of the previous approach was the difficulty in processing aluminum using either wet or dry etch mechanisms. Here, we discuss details of the novel fabrication process flow and its realization for 4.5 kA/cm2 fabrication process with six Nb layers with two fully planarized layers. We report test results of various planarization diagnostics structures, accounting the influence of topology on Josephson junction quality, as well as yield and critical current of via stacks. We also report on inductance measurement results providing information on interlayer dielectric thickness for planarized layers; confirming a good uniformity over the wafer. Basic components of superconducting logic such as dc/SFQ, SFQ/dc converters, Josephson transmission lines (JTLs), and simple digital circuits such as half-adder (HA) have been designed, fabricated and tested using either conventional (RSFQ) or energy-efficient (ERSFQ) approach. The ERSFQ HA cells with bias inductors fabricated in two planarized layers were shown to function with the operational margins of +/-22%.
Superconducting qubits stand as a pivotal platform for quantum computing, where scalable fabrication is crucial for building complex quantum circuits. Here, we develop a fabrication process for Nb/Al-AlOx/Nb tri-layer Josephson junctions on 4-inch silicon wafers using full-stepper lithography. Utilizing this process, we have produced both transmon and C-shunt flux qubits. The well-behavedI-Vcharacteristics of junction arrays containing up to 1000 junctions highlight the excellent uniformity and scalability of our process. Furthermore, by introducing a RIE pre-etch before BOE treatment to remove most of the SiO2insulator, we have suppressed dielectric loss and increased the coherence time of the Nb-based transmon qubit by almost 10 times, achieving a quality factor comparable to state-of-the-art Nb-based qubits on sapphire substrates. Given its compatibility with silicon technology, our method paves the way for the integration of multi-qubit processors and the co-fabrication of complex quantum circuits.