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arXiv:2303.10685 · Physical Review Applied

Disentangling superconductor and dielectric microwave losses in submicrometer Nb / SiO 2 interconnects using a multimode microstrip resonator

Cougar A. T. Garcia, Nancyjane Bailey, Chris Kirby, Joshua Strong, Vladimir V. Talanov, Anna Herr, Steven M. Anlage

Published Feb 28, 2024• 3 citations
arXivHTMLPDF

Abstract

An understanding of the origins of power loss in superconducting interconnects is essential for the energy efficiency and scalability of superconducting digital logic. At microwave frequencies, power dissipates in both the superconducting wires and the dielectric and these losses can be of comparable magnitude. We describe an approach to accurately disentangle such losses by exploiting their frequency dependence in a multimode transmission-line resonator. This is supported by the concept of a resonator geometric factor extracted from the Ansys High Frequency Structure Simulator (hfss), a commercial three-dimensional finite-element method (FEM) that we adopt for solving a superconductor interior. Using the technique, we have optimized a planarized fabrication process of reciprocal quantum logic (RQL) for the minimum interconnect loss at 4.2 K and gigahertz frequencies. The microstrip interconnects are composed of niobium ($\mathrm{Nb}$) insulated by silicon dioxide ($\mathrm{Si}\mathrm{O}$${}_{2}$) made from a tetraethoxysilane (TEOS) precursor. Two process generations use damascene fabrication and the third one uses Cloisonn\'e fabrication. For all three, $\mathrm{Si}\mathrm{O}$${}_{2}$ exhibits a dielectric loss tangent $\mathrm{tan}\phantom{\rule{0.1em}{0ex}}\ensuremath{\delta}=0.0012\ifmmode\pm\else\textpm\fi{}0.0001$, independent of the $\mathrm{Nb}$ wire width over 0.25--4 $\text{\ensuremath{\mu}}\mathrm{m}$. The intrinsic microwave resistance ${R}_{s}$ of $\mathrm{Nb}$ varies with both the process and the wire width. For damascene fabrication, scanning transmission electron microscopy (STEM) and energy-dispersive x-ray spectroscopy (EDS) reveal that plasma oxidation and grain-growth orientation increase ${R}_{s}$ above the Bardeen-Cooper-Schrieffer (BCS) resistance ${R}_{\mathrm{BCS}}\ensuremath{\approx}17\phantom{\rule{0.2em}{0ex}}\text{\ensuremath{\mu}}\mathrm{\ensuremath{\Omega}}$ at 10 GHz. For Cloisonn\'e fabrication, we demonstrate ${R}_{s}=13\ifmmode\pm\else\textpm\fi{}1.4\phantom{\rule{0.2em}{0ex}}\text{\ensuremath{\mu}}\mathrm{\ensuremath{\Omega}}$ down to $0.25\phantom{\rule{0.2em}{0ex}}\text{\ensuremath{\mu}}\mathrm{m}$ wire width, which is below ${R}_{\mathrm{BCS}}$ and arguably the lowest microwave resistance reported for $\mathrm{Nb}$ at 4.2 K.

DOI
10.1103/physrevapplied.21.024056

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Dielectric loss in low-temperature superconducting integrated circuits can cause lower overall efficiency, particularly in the 90 to 220 GHz regime. We present a method to tune the dielectric loss for silicon oxide deposited by plasma-enhanced chemical-vapor deposition at ambient temperatures. Deposition in an environment with a higher silane-to-oxygen ratio produces silicon oxide films with a lower loss-tangent and a slightly higher optical index of refraction, while contributing no appreciable change in film stress. We measured the dielectric loss by fabricating a series of Nb-SiOx-Nb microstrip resonators in the frequency range of 6 to 9 GHz and comparing their temperature dependence to a model of parasitic two-level-system fluctuators. The dielectric loss-tangent of silicon oxide was improved from 6 ×10-3for stoichiometric silicon dioxide to 2 ×10-3for a more silicon-rich silicon oxide. We present details of the fabrication process and measurements of microstrip resonators.
Flexible interconnects with superconducting (SC) traces and polyimide dielectric can provide low signal loss and low thermal conductivity at cryogenic temperatures, and are expected to find use in densely integrated cryogenic electronics systems. The ultra-low loss of SC interconnects at microwave frequencies can be accurately characterized through the use of weakly coupled SC resonators. The high-quality factor resonators provide sensitive measurements of the aggregate loss properties of the conductor and dielectric, as functions of frequency, temperature, and signal power. In this work, resonators with different linewidths were fabricated and tested to study how the linewidth impacts the overall internal resonator loss, in order to better characterize and separate the individual loss components (i.e., dielectric loss vs. conductor loss). The results of this work are important for understanding loss and transmission properties of similarly designed and fabricated transmission line interconnects.
We report results of measurements of Nb stripline resonators with linewidths ranging from 1.0 to 0.25 μ m, fabricated using an 8-Nb-layer process with planarized SiO2 dielectric developed at MIT Lincoln Laboratory for superconductor single-flux-quantum circuits. The fundamental resonant frequency f 0 was varied from 2.3 to 4.5 GHz. The results show that, at 4 K, the losses for the narrowest lines are dominated by losses in the dielectric. At high power, the nonlinear niobium losses dominate. Spiral inductors have also been used to design and fabricate multipole low-pass filters with three and five poles with cutoff at 1 GHz. The measured and simulated results for the filters agree very well and show almost ideal properties. The precision and high reproducibility of this fabrication process hold the promise of fabricating multipole filters without the need for tuning the individual poles.
Abstract We perform an experimental and numerical study of dielectric loss in superconducting microwave resonators at low temperature. Dielectric loss, due to two-level systems, is a limiting factor in several applications, e.g. superconducting qubits, Josephson parametric amplifiers, microwave kinetic-inductance detectors, and superconducting single-photon detectors. Our devices are made of disordered NbN, which, due to magnetic-field penetration, necessitates 3D finite-element simulation of the Maxwell–London equations at microwave frequencies to accurately model the current density and electric field distribution. From the field distribution, we compute the geometric filling factors of the lossy regions in our resonator structures and fit the experimental data to determine the intrinsic loss tangents of its interfaces and dielectrics. We put emphasis on the loss caused by a spin-on-glass resist such as hydrogen silsesquioxane (HSQ), used for ultrahigh lithographic resolution relevant to the fabrication of nanowires. We find that, when used, HSQ is the dominant source of loss, with a loss tangent of δ HSQ i = 8 × 10 − 3 .
We present a lab-on-chip experiment to accurately measure losses of superconducting microstrip lines at microwave and sub-mm wavelengths. The microstrips are fabricated from NbTiN, which is deposited using reactive magnetron sputtering, and amorphous silicon which is deposited using plasma-enhanced chemical vapor deposition (PECVD). Sub-mm wave losses are measured using on-chip Fabry-P{é}rot resonators (FPR) operating around $350\ $GHz. Microwave losses are measured using shunted half-wave resonators with an identical geometry and fabricated on the same chip. We measure a loss tangent of the amorphous silicon at single-photon energies of tan⁡δ=3.7±0.5×10−5\tanδ=3.7\pm0.5\times10^{-5}tanδ=3.7±0.5×10−5 at $6\ $GHz and tan⁡δ=2.1±0.1×10−4\tanδ= 2.1\pm 0.1\times10^{-4}tanδ=2.1±0.1×10−4 at $350\ $GHz. These results represent very low losses for deposited dielectrics, but the sub-mm wave losses are significantly higher than the microwave losses, which cannot be understood using the standard two-level system loss model.
In this work, we investigated how different under- and capping layers on patterned Nb films impacted the RF losses of flexible thin-film superconducting microstrip transmission line resonators measured in a frequency range from 2 to 20 GHz. We studied how different thicknesses of Ti(10 and 50 nm) under-layer, used for adhesion, impacts conductor losses. We also studied Cu(20, 50, 100, and 200 nm) capping layers and how they affect conductor loss. These studies were carried out on 20-μm-thick spin-on polyimide (PI-2611) thin films and characterized at various cryogenic temperatures between 1.2 and 4.2 K. The results indicate normal-superconductor (Ti/Nb) and superconductor-normal (Nb/Cu) bilayer structures have increased surface resistance, which leads to an increase in microwave loss when compared to Nb-only signal traces. We quantified this additional loss by extracting resonator quality factors for weakly coupled resonators with various conductor stack-ups. Our experimental results can help inform decisions regarding material stack-ups when designing multiconductor multilayer superconducting flexible cables intended for use with ultralow-temperature electronic systems.