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Sensors

Fine-Tuning and Optimization of Superconducting Quantum Magnetic Sensors by Thermal Annealing

Antonio Vettoliere, B. Ruggiero, M. Valentino, P. Silvestrini, C. Granata

Published Aug 21, 2019• 7 citations
Publisher

Abstract

In the present article, we present the experimental results concerning the fine-tuning and optimization of superconducting quantum interference device (SQUID) parameters by thermal annealing. This treatment allows for the modification of the parameters in order to meet a specific application or to adjust the device parameters to prevent the increase of magnetic field noise and work instability conditions due to a different critical current with respect to the design value. In particular, we report the sensor critical current, the voltage-flux (V-Φ) characteristics and the spectral density of the magnetic field of SQUID magnetometers for different annealing temperatures. The measurements demonstrate that it is possible to achieve a fine control of the most important device parameters. In particular, we show that thermal annealing allows for the reduction of SQUID noise by more than a factor of 5 and makes the device working operations very stable. These results are very useful in view of quantum technology applications related to superconducting quantum computing where the correct functioning of the quantum bit depends on the fine control of the superconducting quantum device parameters and selectable annealing is possible by using a suitable laser as a thermal source.

DOI
10.3390/s19173635

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For over three decades, the presence of magnetic flux noise with a power spectral density scaling roughly as $S_Phi(f) propto 1/f^alpha$, where $alpha lesssim 1$, has been known to limit the low-frequency performance of dc superconducting quantum interference devices (SQUIDs). In recent years, experiments indicate that this same noise persists to frequencies up to 1~GHz and is a dominant source of dephasing in flux-sensitive superconducting quantum bits (qubits). Thus, the reduction of flux noise presents a major hurdle towards the successful realization of scalable quantum computers that are based on flux-based qubits. In this thesis, we present experimental measurements, theoretical analyses, and numerical simulations that support a more detailed understanding of both the microscopic and macroscopic properties of flux noise.Our experimental work begins with flux noise measurements of a large number of SQUIDs in the temperature range from 0.1~K to 4~K. We report on measurements of ten SQUIDs with systematically varied geometries and show that $alpha$ increases as the temperature is lowered; in so doing, each spectrum pivots about a nearly constant frequency. The mean square flux noise, inferred by integrating the power spectra, grows rapidly with temperature and at a given temperature is approximately independent of the outer dimension of a given SQUID washer. We show that these results are incompatible with a model based on the random reversal of independent, spins that are located at the surface of the SQUID washer.In the course of our flux noise measurements, we became aware of a spurious contribution to low-frequency critical current noise in Josephson junctions---normally attributed to charge trapping in the barrier---arising from temperature instabilities inherent in cryogenic systems. These temperature fluctuations modify the critical current via its temperature dependence. By computing cross-correlations between measured temperature and critical current noise in Al-AlOx-Al junctions, we show that, despite excellent temperature stability, temperature fluctuations induce observable critical current fluctuations. Particularly, because $1/f$ critical current noise has decreased with improved fabrication techniques in recent years, it is important to understand and eliminate this additional noise source.Next, we introduce a numerical method of calculating the mean square flux noise $Phisq$ from independently fluctuating spins on the surface of thin-film loops of arbitrary geometry. By reciprocity, $Phisq$ is proportional to $langleBbf(rbf)^2rangle$, where $Bbf(rbf)$ is the magnetic field generated by a circulating current around the loop and $rbf$ varies over the loop surface. By discretizing the loop nonuniformly, we efficiently and accurately compute the current distribution and resulting magnetic field, which may vary rapidly across the loop. We use this method to compute $Phisq$ in a number of scenarios in which we systematically vary physical parameters of the loop. We compare our simulations to an earlier analytic result predicting that $Phisq propto R/W$ in the limit where the loop radius $R$ is much greater than the linewidth $W$. We further show that the previously neglected contribution of edge spins to $Phisq$ is significant---even dominant---in narrow-linewidth loops.To calculate theoretical dephasing rates in qubits, we consider flux noise with a spectral density $S_Phi(f) = A^2/(f/1~hbox{Hz})^alpha$, where $A$ is of the order of 1~$muPhi_0 , hbox{Hz}^{-1/2}$ and $0.6 leq alpha leq 1.2$; $Phi_{0}$ is the flux quantum. For a qubit with an energy level splitting linearly coupled to the applied flux, our calculations of the dependence of the pure dephasing time $tau_phi$ of Ramsey and echo pulse sequences on $alpha$ for fixed $A$ show that $tau_phi$ decreases rapidly as $alpha$ is reduced. We find that $tau_phi$ is relatively insensitive to the noise bandwidth, $f_1 leq f leq f_2$, for all $alpha$ provided the ultraviolet cutoff frequency $f_2 > 1/tau_phi$. We calculate the ratio $tau_{phi,E} / tau_{phi,R}$ of the echo ($E$) and Ramsey ($R$) sequences, and the dependence of the decay function on $alpha$ and $f_2$. We investigate the case in which $S_Phi(f_0)$ is fixed at the ``pivot frequency'' $f_0 neq 1$~Hz while $alpha$ is varied, and find that the choice of $f_0$ can greatly influence the sensitivity of $tau_{phi,E}$ and $tau_{phi,R}$ to the value of $alpha$.Finally, we conclude with a brief review of our principal results and conclusions. We also comment on promising avenues of future research.

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arXiv:1106.1985•Applied Physics Letters•Jul 18, 2011•61 citations
In the present article, we present the experimental results concerning the fine-tuning and optimization of superconducting quantum interference device (SQUID) parameters by thermal annealing. This treatment allows for the modification of the parameters in order to meet a specific application or to adjust the device parameters to prevent the increase of magnetic field noise and work instability conditions due to a different critical current with respect to the design value. In particular, we report the sensor critical current, the voltage-flux (V-Φ) characteristics and the spectral density of the magnetic field of SQUID magnetometers for different annealing temperatures. The measurements demonstrate that it is possible to achieve a fine control of the most important device parameters. In particular, we show that thermal annealing allows for the reduction of SQUID noise by more than a factor of 5 and makes the device working operations very stable. These results are very useful in view of quantum technology applications related to superconducting quantum computing where the correct functioning of the quantum bit depends on the fine control of the superconducting quantum device parameters and selectable annealing is possible by using a suitable laser as a thermal source.
Integrated NbN direct current superconducting quantum interference device (DC-SQUID) magnetometers were developed based on high-quality epitaxial NbN/AlN/NbN Josephson junctions for SQUID applications operating at high temperatures. We report the current–voltage and voltage–flux characteristics and the noise performance of the NbN DC-SQUIDs for temperatures ranging from 4.2 to 9 K. The critical current and voltage swing of the DC-SQUIDs decreased by 15% and 25%, respectively, as the temperature was increased from 4.2 to 9 K. The white flux noise of the DC-SQUID magnetometer at 1 kHz increased from 3.9 μΦ0/Hz1/2 at 4.2 K to 4.8 μΦ0/Hz1/2 at 9 K with 23% increase, corresponding to the magnetic field noise of 6.6 and 8.1 fT/Hz1/2, respectively. The results show that NbN DC-SQUIDs improve the tolerance of the operating temperatures and temperature fluctuations in SQUID applications.
High-Tc_\text{c}c​ SQUID Optimization: Exploring Competing Design and Operating Parameters
Improving the design of superconducting quantum interference devices (SQUIDs) for quantum sensing applications can involve a compromise between competing device parameters. For SQUIDs made from high-temperature superconductors (HTS), accurate modelling for optimization should include the device geometry, material properties and their temperature dependences, as well as thermal noise. We outline here a lumped element model that calculates the voltage response to magnetic flux of a hairpin SQUID and use it to explore the effect of these parameters on optimizing the SQUID voltage output. We first validate our model by showing close agreement with current-voltage and voltage-flux measurements performed on Yttrium Barium Copper Oxide hairpin SQUIDs with different geometries by including structures such as the bias leads. We show the effect of track width on the kinetic to geometric inductance ratios (κ\kappaκ) for a range of film thicknesses and temperatures, to aid researchers how to optimize SQUID designs. Then, through numerical simulations, we show on how (i) the voltage modulation depth decreases exponentially with the total inductance, independent of the asymmetry ratio; (ii) narrower superconducting tracks lead to a broader temperature operation range,ΔT∼30\Delta T \sim 30ΔT∼30K, while wider tracks operate in a narrower temperature range,ΔT∼10\Delta T \sim 10ΔT∼10K, but are more sensitive to temperature changes; and (iv) the optimal bias current, which maximises the device performance, depends on the operating temperature.
For over three decades, the presence of magnetic flux noise with a power spectral density scaling roughly as SPhi(f)propto1/falphaS_Phi(f) propto 1/f^alphaSP​hi(f)propto1/falpha, where alphalesssim1alpha lesssim 1alphalesssim1, has been known to limit the low-frequency performance of dc superconducting quantum interference devices (SQUIDs). In recent years, experiments indicate that this same noise persists to frequencies up to 1~GHz and is a dominant source of dephasing in flux-sensitive superconducting quantum bits (qubits). Thus, the reduction of flux noise presents a major hurdle towards the successful realization of scalable quantum computers that are based on flux-based qubits. In this thesis, we present experimental measurements, theoretical analyses, and numerical simulations that support a more detailed understanding of both the microscopic and macroscopic properties of flux noise.Our experimental work begins with flux noise measurements of a large number of SQUIDs in the temperature range from 0.1~K to 4~K. We report on measurements of ten SQUIDs with systematically varied geometries and show that alphaalphaalpha increases as the temperature is lowered; in so doing, each spectrum pivots about a nearly constant frequency. The mean square flux noise, inferred by integrating the power spectra, grows rapidly with temperature and at a given temperature is approximately independent of the outer dimension of a given SQUID washer. We show that these results are incompatible with a model based on the random reversal of independent, spins that are located at the surface of the SQUID washer.In the course of our flux noise measurements, we became aware of a spurious contribution to low-frequency critical current noise in Josephson junctions---normally attributed to charge trapping in the barrier---arising from temperature instabilities inherent in cryogenic systems. These temperature fluctuations modify the critical current via its temperature dependence. By computing cross-correlations between measured temperature and critical current noise in Al-AlOx-Al junctions, we show that, despite excellent temperature stability, temperature fluctuations induce observable critical current fluctuations. Particularly, because 1/f1/f1/f critical current noise has decreased with improved fabrication techniques in recent years, it is important to understand and eliminate this additional noise source.Next, we introduce a numerical method of calculating the mean square flux noise PhisqPhisqPhisq from independently fluctuating spins on the surface of thin-film loops of arbitrary geometry. By reciprocity, PhisqPhisqPhisq is proportional to langleBbf(rbf)2ranglelangleBbf(rbf)^2ranglelangleBbf(rbf)2rangle, where Bbf(rbf)Bbf(rbf)Bbf(rbf) is the magnetic field generated by a circulating current around the loop and rbfrbfrbf varies over the loop surface. By discretizing the loop nonuniformly, we efficiently and accurately compute the current distribution and resulting magnetic field, which may vary rapidly across the loop. We use this method to compute PhisqPhisqPhisq in a number of scenarios in which we systematically vary physical parameters of the loop. We compare our simulations to an earlier analytic result predicting that PhisqproptoR/WPhisq propto R/WPhisqproptoR/W in the limit where the loop radius RRR is much greater than the linewidth WWW. We further show that the previously neglected contribution of edge spins to PhisqPhisqPhisq is significant---even dominant---in narrow-linewidth loops.To calculate theoretical dephasing rates in qubits, we consider flux noise with a spectral density SPhi(f)=A2/(f/1 hboxHz)alphaS_Phi(f) = A^2/(f/1~hbox{Hz})^alphaSP​hi(f)=A2/(f/1 hboxHz)alpha, where AAA is of the order of 1~muPhi0,hboxHz−1/2muPhi_0 , hbox{Hz}^{-1/2}muPhi0​,hboxHz−1/2 and 0.6leqalphaleq1.20.6 leq alpha leq 1.20.6leqalphaleq1.2; Phi0Phi_{0}Phi0​ is the flux quantum. For a qubit with an energy level splitting linearly coupled to the applied flux, our calculations of the dependence of the pure dephasing time tauphitau_phitaup​hi of Ramsey and echo pulse sequences on alphaalphaalpha for fixed AAA show that tauphitau_phitaup​hi decreases rapidly as alphaalphaalpha is reduced. We find that tauphitau_phitaup​hi is relatively insensitive to the noise bandwidth, f1leqfleqf2f_1 leq f leq f_2f1​leqfleqf2​, for all alphaalphaalpha provided the ultraviolet cutoff frequency f2>1/tauphif_2 > 1/tau_phif2​>1/taup​hi. We calculate the ratio tauphi,E/tauphi,Rtau_{phi,E} / tau_{phi,R}tauphi,E​/tauphi,R​ of the echo (EEE) and Ramsey (RRR) sequences, and the dependence of the decay function on alphaalphaalpha and f2f_2f2​. We investigate the case in which SPhi(f0)S_Phi(f_0)SP​hi(f0​) is fixed at the ``pivot frequency'' f0neq1f_0 neq 1f0​neq1~Hz while alphaalphaalpha is varied, and find that the choice of f0f_0f0​ can greatly influence the sensitivity of tauphi,Etau_{phi,E}tauphi,E​ and tauphi,Rtau_{phi,R}tauphi,R​ to the value of alphaalphaalpha.Finally, we conclude with a brief review of our principal results and conclusions. We also comment on promising avenues of future research.
Direct current-superconducting quantum interference devices (SQUIDs) characterized by asymmetric Josephson junctions have never been used for applications. In order to demonstrate their potential advantages, a throughout numerical analysis of different asymmetric configurations has been carried out. A damping resistance has been included in the SQUID circuit and the thermal noise associated with junction and damping resistances has been considered in the numerical model. Magnetic modulations and flux noise spectral densities have been computed as a function of many parameters (bias current, asymmetry, SQUID inductance, and damping resistance) and the performance of symmetric and asymmetric devices have been compared. The results show that, by properly optimizing the SQUID design, asymmetric SQUIDs are characterized by higher magnetic flux to voltage transfer coefficient and lower flux noise. As a result, asymmetric configurations can be very useful in all the applications where high sensitivity is required.
An integrated magnetic nanosensor based on a niobium dc SQUID (superconducting quantum interference device) for nanoscale applications is presented. The sensor, having a washer shape with a hole of 200 nm and two Josephson-Dayem nanobridges of 80 nm × 100 nm, consists of a Nb(30 nm)/Al(30 nm) bilayer patterned by electron beam lithography (EBL) and shaped by lift-off and reactive ion etch (RIE) processes. The presence of the niobium coils, integrated on-chip and tightly coupled to the SQUID, allows us to easily excite the sensor in order to get the voltage-flux characteristics and to flux bias the SQUID at its optimal point. The measurements were performed at liquid helium temperature. A voltage swing of 75 µV and a maximum voltage-flux transfer coefficient (responsivity) as high as 1 mV/Φ(0) were directly measured from the voltage-flux characteristic. The noise measurements were performed in open loop mode, biasing the SQUID with a dc magnetic flux at its maximum responsivity point and using direct-coupled low-noise readout electronics. A white magnetic flux noise spectral density as low as 2.5 μΦ(0) Hz(-1/2) was achieved, corresponding to a magnetization or spin sensitivity in units of the Bohr magneton of 100 spin Hz(-1/2). Possible applications of this nanosensor can be envisaged in magnetic detection of nanoparticles and small clusters of atoms and molecules, in the measurement of nanoobject magnetization, and in quantum computing.
We investigated, at temperature 4.2 K, electric transport, flux noise, and resulting spin sensitivity of miniaturized Nb direct current superconducting quantum interference devices (SQUIDs) based on submicron Josephson junctions with HfTi barriers. The SQUIDs are either of the magnetometer-type or gradiometric in layout. In the white noise regime, for the best magnetometer we obtain a flux noise SΦ1/2=250nΦ0/Hz1/2, corresponding to a spin sensitivity Sμ1/2≥29μB/Hz1/2. For the gradiometer we find SΦ1/2=300nΦ0/Hz1/2 and Sμ1/2≥44μB/Hz1/2. The devices can still be optimized with respect to flux noise and coupling between a magnetic particle and the SQUID, leaving room for further improvement towards single spin resolution.