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arXiv:1106.1985 · Applied Physics Letters

Superconducting quantum interference devices with submicron Nb/HfTi/Nb junctions for investigation of small magnetic particles

J. Nagel, O. F. Kieler, T. Weimann, R. Wölbing, J. Kohlmann, Alexander B Zorin, R. Kleiner, D. Koelle, M. Kemmler

Published Jul 18, 2011• 61 citations
arXivHTMLPDF

Abstract

We investigated, at temperature 4.2 K, electric transport, flux noise, and resulting spin sensitivity of miniaturized Nb direct current superconducting quantum interference devices (SQUIDs) based on submicron Josephson junctions with HfTi barriers. The SQUIDs are either of the magnetometer-type or gradiometric in layout. In the white noise regime, for the best magnetometer we obtain a flux noise SΦ1/2=250nΦ0/Hz1/2, corresponding to a spin sensitivity Sμ1/2≥29μB/Hz1/2. For the gradiometer we find SΦ1/2=300nΦ0/Hz1/2 and Sμ1/2≥44μB/Hz1/2. The devices can still be optimized with respect to flux noise and coupling between a magnetic particle and the SQUID, leaving room for further improvement towards single spin resolution.

DOI
10.1063/1.3614437

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We investigated, at temperature 4.2 K, electric transport, flux noise, and resulting spin sensitivity of miniaturized Nb direct current superconducting quantum interference devices (SQUIDs) based on submicron Josephson junctions with HfTi barriers. The SQUIDs are either of the magnetometer-type or gradiometric in layout. In the white noise regime, for the best magnetometer we obtain a flux noise SΦ1/2=250nΦ0/Hz1/2, corresponding to a spin sensitivity Sμ1/2≥29μB/Hz1/2. For the gradiometer we find SΦ1/2=300nΦ0/Hz1/2 and Sμ1/2≥44μB/Hz1/2. The devices can still be optimized with respect to flux noise and coupling between a magnetic particle and the SQUID, leaving room for further improvement towards single spin resolution.
We investigate electric transport and noise properties of microstrip-type submicron direct current superconducting quantum interference devices (dc SQUIDs) based on Nb thin films and overdamped Josephson junctions with a HfTi barrier. The SQUIDs were designed for optimal spin sensitivity Sμ1/2 upon operation in intermediate magnetic fields B (tens of mT), applied perpendicular to the substrate plane. Our, so far, best SQUID can be continuously operated in fields up to B≈±50 mT with rms flux noise SΦ,w1/2≤250 nΦ0/Hz1/2 in the white noise regime and spin sensitivity Sμ1/2≤29 μB/Hz1/2. Furthermore, we demonstrate operation in B = 0.5 T with high sensitivity in flux SΦ,w1/2≈680 nΦ0/Hz1/2 and in electron spin Sμ1/2≈79 μB/Hz1/2. We discuss strategies to further improve the nanoSQUID performance.
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We report on the development of highly sensitive SQUIDs featuring sub-micrometer loop dimensions. The integration of high quality and low capacitance SIS Nb/AlO x /Nb cross-type Josephson tunnel junctions results in white flux noise levels as low as 66 n Φ 0 Hz −1/2 , well below state-of-the-art values of their Nb-based counterparts based on constriction type junctions. Estimation of the spin sensitivity of the best SQUIDs yield S μ 1/2 < 7 μ B Hz −1/2 in the white noise region, suitable for the investigation of small spin systems. We discuss fabrication challenges, show results on the electrical characterization of devices with various pickup loops, and describe options for further improvement, which may push the sensitivity of such devices even to single spin resolution.
We have fabricated superconducting quantum interference devices (SQUIDs) with an inductance of 140 pH by using sub- µm Nb/Al–AlO x –Al/Nb edge junctions. The small capacitance of the junction resulted in the very large voltage swing of 210 µV and gradient dV/ dΦ of 940 µV/Φ0. Consequently, the very low flux noise of 0.61 µΦ0/ Hz0.5 corresponding to the energy sensitivity ε of 8.6h at the white noise level was obtained by using a conventional flux-locked loop configuration. The low-frequency noise was also very low, 2.7 µΦ0/ Hz0.5 corresponding to ε= 170 h at 1 Hz. We could obtain very low flux noise for the SQUID which had the practical inductance using only a conventional readout circuit.
We report on the fabrication and characterization of micrometer-sized superconducting quantum interference devices (SQUIDs) based on nanoscale vanadium/copper/vanadium Josephson weak links. Magnetically driven quantum interference patterns have been measured for temperatures in the 0.24–2 K range. As DC SQUIDs, these devices obtain flux-to-voltage transfer function values as high as 450 μV/Φ0 leading to promising magnetic flux resolution ΦN<3 μΦ0/Hz, being here limited by the room temperature preamplification stage. Significant improvement in the flux noise performance figures is expected with the adoption of cryogenic preamplification. The presented devices are suitable for operation as small-area SQUIDs at sub-Kelvin temperature, but their design can also be upscaled to include input coils enabling their use as sensitive magnetometers via the adoption of optimized electronic readout stages based on flux feedback schemes.
Integrated NbN direct current superconducting quantum interference device (DC-SQUID) magnetometers were developed based on high-quality epitaxial NbN/AlN/NbN Josephson junctions for SQUID applications operating at high temperatures. We report the current–voltage and voltage–flux characteristics and the noise performance of the NbN DC-SQUIDs for temperatures ranging from 4.2 to 9 K. The critical current and voltage swing of the DC-SQUIDs decreased by 15% and 25%, respectively, as the temperature was increased from 4.2 to 9 K. The white flux noise of the DC-SQUID magnetometer at 1 kHz increased from 3.9 μΦ0/Hz1/2 at 4.2 K to 4.8 μΦ0/Hz1/2 at 9 K with 23% increase, corresponding to the magnetic field noise of 6.6 and 8.1 fT/Hz1/2, respectively. The results show that NbN DC-SQUIDs improve the tolerance of the operating temperatures and temperature fluctuations in SQUID applications.