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Applied Physics Letters

Temperature-dependent performance of all-NbN DC-SQUID magnetometers

Quansheng Liu, Huiwu Wang, Qiyu Zhang, Hai Wang, Wei Peng, Zhen Wang

Published May 29, 2017• 17 citations
Publisher

Abstract

Integrated NbN direct current superconducting quantum interference device (DC-SQUID) magnetometers were developed based on high-quality epitaxial NbN/AlN/NbN Josephson junctions for SQUID applications operating at high temperatures. We report the current–voltage and voltage–flux characteristics and the noise performance of the NbN DC-SQUIDs for temperatures ranging from 4.2 to 9 K. The critical current and voltage swing of the DC-SQUIDs decreased by 15% and 25%, respectively, as the temperature was increased from 4.2 to 9 K. The white flux noise of the DC-SQUID magnetometer at 1 kHz increased from 3.9 μΦ0/Hz1/2 at 4.2 K to 4.8 μΦ0/Hz1/2 at 9 K with 23% increase, corresponding to the magnetic field noise of 6.6 and 8.1 fT/Hz1/2, respectively. The results show that NbN DC-SQUIDs improve the tolerance of the operating temperatures and temperature fluctuations in SQUID applications.

DOI
10.1063/1.4984300

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Integrated NbN direct current superconducting quantum interference device (DC-SQUID) magnetometers were developed based on high-quality epitaxial NbN/AlN/NbN Josephson junctions for SQUID applications operating at high temperatures. We report the current–voltage and voltage–flux characteristics and the noise performance of the NbN DC-SQUIDs for temperatures ranging from 4.2 to 9 K. The critical current and voltage swing of the DC-SQUIDs decreased by 15% and 25%, respectively, as the temperature was increased from 4.2 to 9 K. The white flux noise of the DC-SQUID magnetometer at 1 kHz increased from 3.9 μΦ0/Hz1/2 at 4.2 K to 4.8 μΦ0/Hz1/2 at 9 K with 23% increase, corresponding to the magnetic field noise of 6.6 and 8.1 fT/Hz1/2, respectively. The results show that NbN DC-SQUIDs improve the tolerance of the operating temperatures and temperature fluctuations in SQUID applications.
In this article, an all-NbN superconducting quantum interference device (SQUID) array was developed for future applications by taking advantage of the higher critical temperature of a NbN film compared with Nb. The NbN SQUID array was composed of 100 SQUIDs with equal loop areas connected in series. The array was fabricated on a single-crystal MgO (100) substrate using 3-μm-diameter NbN/AlN/NbN Josephson junctions. The hysteresis and shielding parameters of the SQUID were 0.67 and 0.15, respectively. The SQUIDs in the array were coherently modulated by injecting current in a common flux control line, which resulted in a modulation voltage of 3.54 mV with consistent periodicity and a flux-to-voltage transfer coefficient of 23 mV/Φ0. Using a flux locked loop circuit, the fabricated NbN SQUID array exhibited excellent performance with a low white flux noise of 1.4 μΦ0/√Hz, which included the preamplifier noise.
We investigated, at temperature 4.2 K, electric transport, flux noise, and resulting spin sensitivity of miniaturized Nb direct current superconducting quantum interference devices (SQUIDs) based on submicron Josephson junctions with HfTi barriers. The SQUIDs are either of the magnetometer-type or gradiometric in layout. In the white noise regime, for the best magnetometer we obtain a flux noise SΦ1/2=250nΦ0/Hz1/2, corresponding to a spin sensitivity Sμ1/2≥29μB/Hz1/2. For the gradiometer we find SΦ1/2=300nΦ0/Hz1/2 and Sμ1/2≥44μB/Hz1/2. The devices can still be optimized with respect to flux noise and coupling between a magnetic particle and the SQUID, leaving room for further improvement towards single spin resolution.
Planar niobium nitride (NbN) dc superconducting quantum interference devices (SQUIDs) magnetometers were developed based on high-quality epitaxial NbN/AlN/NbN Josephson junctions for SQUID applications at higher operating temperatures. To improve the design of NbN dc SQUIDs, we measured the SQUID washer's inductance, which is a key SQUID parameter. A set of NbN dc SQUIDs with washers with different dimensions were implemented. The washer inductances were obtained from the periodic flux variation in the SQUIDs when a control current was injected directly into the SQUID washers; the results agree well with the ones calculated with a numerical simulation in InductEX software. We obtained an empirical expression to estimate the NbN SQUID inductance with washers with different geometric structures. Our results will be useful for designing NbN dc SQUID magnetometers in future.
In an effort to eliminate the intrinsic noise sources that contained within the superconducting qubit circuits, we successfully fabricate superconducting flux qubit circuits (rf SQUID) with full epitaxially grown NbN/AlN/NbN tunnel junctions. The temperature dependent of magnetic flux shift has been investigated by using a NbN/AlN/NbN dc SQUID magnetometer in the temperature range from 20 mK to 2.5 K. Our results show that the shift of the magnetic flux is in the level of ∼1 mF 0 during the experiment.
We investigate electric transport and noise properties of microstrip-type submicron direct current superconducting quantum interference devices (dc SQUIDs) based on Nb thin films and overdamped Josephson junctions with a HfTi barrier. The SQUIDs were designed for optimal spin sensitivity Sμ1/2 upon operation in intermediate magnetic fields B (tens of mT), applied perpendicular to the substrate plane. Our, so far, best SQUID can be continuously operated in fields up to B≈±50 mT with rms flux noise SΦ,w1/2≤250 nΦ0/Hz1/2 in the white noise regime and spin sensitivity Sμ1/2≤29 μB/Hz1/2. Furthermore, we demonstrate operation in B = 0.5 T with high sensitivity in flux SΦ,w1/2≈680 nΦ0/Hz1/2 and in electron spin Sμ1/2≈79 μB/Hz1/2. We discuss strategies to further improve the nanoSQUID performance.
For the fabrication of nanoscale SQUIDs, for example having loop diameters of order 1 µm or smaller, the conventional trilayer window-type Josephson junctions are too large. Instead, we consider the use of nanobridge junctions with dimensions of order 100 nm. The problem of hysteresis in the junctions' current–voltage characteristic (IVC) is avoided by depositing a gold overlayer, which serves as both a thermal and electrical shunt. Noise measurement of dc SQUIDs which incorporate such Nb nanobridges as the Josephson junctions are reported. Devices having different IVCs were fabricated and characterized. The best device has a flux noise of 5 × 10 −6 Φ 0 Hz −1/2 at 4.2 K, and there is no significant increase in the noise level in a static magnetic field up to 2 mT. Techniques for increasing the voltage modulation depth, and hence improving the flux noise performance, are discussed.