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IEEE Transactions on Applied Superconductivity

Dielectric Loss in Superconducting NbN (200) CPW Resonator Developed on Si Substrate

Wei Qiu, Kazumasa Makise, Hirotaka Terai

Published Jan 9, 2017• 5 citations
Publisher

Abstract

In current superconducting qubit circuit development, coherence time is limited by low-frequency flux noise introduced from localized two-level systems (TLSs) in the fabricated superconducting circuit, including superconducting materials, the interface between thin films, and the substrate. As a part of the effect to tackle this issue from a substrate standpoint, we succeed in fabricating NbN (200) oriented coplanar waveguide resonator (CPWR) on a thin titanium nitride (TiN) (200) buffered Si (100) substrate. The internal loss is close to 3 × 10-5nearphoton> ~1, improved from ~2 × 10-4in NbN (200) CPWR fabricated on MgO (100). For NbN (200) resonators grown on Si (100), the internal loss shows microwave energy independent. To further clarity if this energy independence is due to the change of substrate material, we also fabricated TiN (200) CPWR on Si (100). In contrast to NbN (200) CPWR, the loss of TiN (200) resonator shows a strong microwave dependent, an indication of TLSs originated from the interface and the surface. We suggest TLSs in NbN (200) CPWR are dominated from different mechanism other than arising from the interface and surface.

DOI
10.1109/tasc.2017.2649840

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In current superconducting qubit circuit development, coherence time is limited by low-frequency flux noise introduced from localized two-level systems (TLSs) in the fabricated superconducting circuit, including superconducting materials, the interface between thin films, and the substrate. As a part of the effect to tackle this issue from a substrate standpoint, we succeed in fabricating NbN (200) oriented coplanar waveguide resonator (CPWR) on a thin titanium nitride (TiN) (200) buffered Si (100) substrate. The internal loss is close to 3 × 10-5nearphoton> ~1, improved from ~2 × 10-4in NbN (200) CPWR fabricated on MgO (100). For NbN (200) resonators grown on Si (100), the internal loss shows microwave energy independent. To further clarity if this energy independence is due to the change of substrate material, we also fabricated TiN (200) CPWR on Si (100). In contrast to NbN (200) CPWR, the loss of TiN (200) resonator shows a strong microwave dependent, an indication of TLSs originated from the interface and the surface. We suggest TLSs in NbN (200) CPWR are dominated from different mechanism other than arising from the interface and surface.
We report on the fabrication and characterization of superconducting coplanar waveguide (CPW) resonators based on titanium nitride (TiN) thin films deposited on 200\,mm diameter high-resistivity Si(100) substrates. We systematically investigate how deposition conditions, dry-etch power and in-situ resist strip temperature affect morphology, superconducting properties and dielectric losses. By tuning reactive sputtering conditions, three distinct preferred out-of-plane crystal orientations - (111), (200), and a mix of both are achieved. Our results demonstrate that all films exhibit similar minimal two-level system (TLS) losses, with TiN111 exhibiting the lowest median TLS losses δ~TLS\tildeδ_\mathrm{TLS}δ~TLS​, and greater robustness against reoxidation. The applied structuring process, in contrast, has a far greater influence on the TLS loss than the crystal orientation of the TiN film and, consequently, the intrinsic material properties of the superconducting layer. The lowest TLS losses for all TiN depositions were achieved with a low power etch and low temperature resist strip. An additional buffered oxide etch (BOE) treatment could remove high-loss interfacial oxides at the metal-air (MA) and substrate-air (SA) interface and recover the etch-induced TLS losses. Consequently, TiN resonators exhibiting δ~TLS\tildeδ_\mathrm{TLS}δ~TLS​ values as low as 9.67×10−79.67 \times 10^{-7}9.67×10−7 were realized. The corresponding median low-power loss, δ~LP\tildeδ_\mathrm{LP}δ~LP​, amounts to 11.04×10−711.04 \times 10^{-7}11.04×10−7, which translates to an internal quality factor approaching one million. These findings highlight the critical role of process induced oxide formation at the MA and SA interfaces in limiting the performance of TiN resonators and provide a scalable, low-loss process compatible with industry-grade 200\,mm CMOS qubit fabrication workflows.
Superconducting coplanar waveguide (CPW) microwave resonators are crucial elements in Photon detectors, Quantum-limited parametric amplifiers, Narrow-band filters, Read-out, interconnect in quantum processors and Hybrid devices, connecting solid-state spins with superconducting circuits [1-3]. In the quantum regime, the dominant loss mechanism for high-Q superconducting resonators can be attributed to parasitic two-level systems (TLSs) in the dielectrics. Interface TLSs are common by products of the fabrication process, often introduced by impurities associated with Si surfaces [3]. To reduce intrinsic losses, we employ isotropic deep reactive-ion etching (DRIE) of Si substrate to create suspended NbN superconducting resonators (SSR).In this study, thin films of niobium (Nb) and niobium nitride (NbN) are deposited on Si substrate by a DC magnetron sputtering system. The influence of the N2/Ar gas ratio, the deposition current, the substrate bias potential on the superconducting critical temperature of the films are investigated. Plasma etching of Nb and NbN in a SF6 and Cl2-BCl3 gas plasma is studied using an inductively coupled plasma (icp) reactor. Parametric studies on the effects of total gas flow rate and chamber pressure on the edge angles and etch rates are reported. Finally, the suspended NbN superconducting resonator is fabricated and will be tested. This could be applied to the fabrication of superconducting qubits in integrated circuits, offering a path towards longer qubit coherence times.Reference:[1] Landig et al. Coherent spin–photon coupling using a resonant exchange qubit. Nature 560, 179–184 (2018)[2] Tosi et al. Silicon quantum processor with robust long-distance qubit couplings. Nat Commun 8, 450 (2017)[3] Bruno et al. Reducing intrinsic loss in superconducting resonators by surface treatment and deep etching of silicon substrates, Appl. Phys. Lett. 106, 182601 (2015)[4] Kennedy et al. Tunable Nb Superconducting Resonator Based on a Constriction Nano-SQUID Fabricated with a Ne Focused Ion Beam, Phys. Rev. Applied 11, 014006 (2019).
Dielectric loss from two-level systems (TLSs) formed by local defects have shown a significant impact on the qubit coherence time. These defects can originate in the insulation material for superconducting wires isolation or in the Josephson junction tunnel barrier material. Due to the complexity of the qubit circuit fabrication process, identifying the contribution from each decoherence source is challenging. In an effort to address this issue, we have developed superconducting qubit that consists of full epitaxially-grown NbN/AlN/NbN Josephson junctions in NbN coplanar waveguide (CPW) resonator circuit. The dielectric loss introduced from TLFs in tunnel junction barrier has been largely reduced due to the unique epitaxial feature of the tunnel junction. The quality factor Qi of the CPW resonator was measured and the dielectric loss tanδ is 3×10−4. The relaxation time inferred from the measured resonator quality factor was comparable to the qubit relaxation time.
© 2019 American Physical Society. Superconducting quantum-computing architectures comprise resonators and qubits that experience energy loss due to two-level systems (TLSs) in bulk and interfacial dielectrics. An understanding of these losses is critical to improving performance in superconducting circuits. In this work, we present a method for quantifying the TLS losses of different bulk and interfacial dielectrics present in superconducting coplanar-waveguide (CPW) resonators. By combining statistical characterization of sets of specifically designed CPW resonators on isotropically etched silicon substrates with detailed electromagnetic modeling, we determine the separate loss contributions from individual material interfaces and bulk dielectrics. This technique for analyzing interfacial TLS losses can be used to guide targeted improvements to qubits, resonators, and their superconducting fabrication processes.
We investigated the loss mechanisms of superconducting circuits with epitaxially grown NbN(100) on MgO(100) substrates by measuring quarter-wave coplanar waveguide resonators with various strip and slot widths. The power dependence of the internal quality factor and the temperature dependence of the resonance frequency shift were evaluated in a dilution refrigerator. The measurement and analysis of the loss in these resonators indicate that the loss was dominated by a two-level system (TLS) loss and the TLS host materials were primarily distributed at the surface of the substrate.
Lossy dielectrics are a significant source of decoherence in superconducting quantum circuits. In this report, we model and compare the dielectric loss in bulk and interfacial dielectrics in titanium nitride (TiN) and aluminum (Al) superconducting coplanar waveguide resonators. We fabricate isotropically trenched resonators to produce a series of device geometries that accentuate a specific dielectric region's contribution to the resonator quality factor. While each dielectric region contributes significantly to loss in TiN devices, the metal–air interface dominates the loss in the Al devices. Furthermore, we evaluate the quality factor of each TiN resonator geometry with and without a post-process hydrofluoric etch and find that it reduced losses from the substrate–air interface, thereby improving the quality factor.