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Applied Physics Letters

Low 1/f noise single-layer YBa2Cu3Ox dc SQUID at 77 K

Gergely Friedl, M. Vildić, Bernhard Roas, D. Uhl, Franz Bömmel, Michael Romheld, B. Hillenbrand, B. Stritzker, G. Daalmans

Published Jun 15, 1992• 72 citations
Publisher

Abstract

Autonomous single-layer dc superconducting quantum interference devices (SQUIDs) have been prepared from epitaxial, laser-deposited YBa2Cu3Ox films on step edge SrTiO3 and LaAlO3 substrates. For device patterning, a SiOx inhibit technique as well as conventional ethylenediaminetetraacetic wet etch was used. The Josephson junctions are of grain boundary type. Their widths are 5 μm. The SQUID hole is a square of about 5 μm; the SQUID inductance is estimated to be about 20 pH. We obtained a very regular, nonhysteretic flux to voltage modulation over more than 100 flux quanta (Φ0). The maximum voltage signal is of the order of 15 μV peak to peak and the maximum transfer function dV/dΦ at the appropriate flux bias is 50 μV/Φ0 at 77 K. The best value of the equivalent flux noise as measured in the flux locked loop mode is 1.4×10−5 Φ0/Hz1/2 at 1 Hz and 1×10−5 Φ0/Hz1/2 in the white noise region for f≳5 Hz. This results in an energy resolution εn,w(f≳5 Hz)=1×10−29 J/Hz in the white noise region and 2×10−29 J/Hz at 1 Hz.

DOI
10.1063/1.106752

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Autonomous single-layer dc superconducting quantum interference devices (SQUIDs) have been prepared from epitaxial, laser-deposited YBa2Cu3Ox films on step edge SrTiO3 and LaAlO3 substrates. For device patterning, a SiOx inhibit technique as well as conventional ethylenediaminetetraacetic wet etch was used. The Josephson junctions are of grain boundary type. Their widths are 5 μm. The SQUID hole is a square of about 5 μm; the SQUID inductance is estimated to be about 20 pH. We obtained a very regular, nonhysteretic flux to voltage modulation over more than 100 flux quanta (Φ0). The maximum voltage signal is of the order of 15 μV peak to peak and the maximum transfer function dV/dΦ at the appropriate flux bias is 50 μV/Φ0 at 77 K. The best value of the equivalent flux noise as measured in the flux locked loop mode is 1.4×10−5 Φ0/Hz1/2 at 1 Hz and 1×10−5 Φ0/Hz1/2 in the white noise region for f≳5 Hz. This results in an energy resolution εn,w(f≳5 Hz)=1×10−29 J/Hz in the white noise region and 2×10−29 J/Hz at 1 Hz.
We have fabricated Y1Ba2Cu3O7−x step-edge junction dc superconducting quantum interference devices (SQUIDs) and characterized their noise performance. The current-voltage characteristics of our SQUIDs are of resistively shunted junction type with critical current densities jc of about 104 A/cm2 and maximum flux to voltage transfer functions δV/δΦ of 20 μV/Φ0 at 77 K. We compare model predictions for 1/f noise in dc SQUIDs with experimental data and show that the frequency dependent noise in our devices results from critical current fluctuations of the Josephson junctions. A bias current reversing technique is effective in suppressing this noise contribution. A flux noise Φn of 80 μΦ0/Hz1/2 at 1 Hz and 77 K was measured on a dc SQUID with an inductance Ls of 60 pH.
We have studied white (high-frequency)-noise properties of YBa2Cu3O7-δ grain-boundary dc superconducting quantum interference devices (SQUIDs). Bias voltage (V) dependence of the white-noise voltage spectral density (S v) was measured for dc-SQUIDs and junctions. As a result, S v at low bias voltage can be explained by the thermal noise theory of tunnel junctions. Furthermore, the energy resolution of 1.96×10-32 J/Hz is obtained at 43 K in the white-noise region. The measured energy resolution of the dc-SQUIDs is in good agreement with the theoretical results. According to the above results, YBa2Cu3O7-δ dc-SQUIDs with a quantum noise limit might be realized at 4.2 K.
We have fabricated superconducting quantum interference devices (SQUIDs) with an inductance of 140 pH by using sub- µm Nb/Al–AlO x –Al/Nb edge junctions. The small capacitance of the junction resulted in the very large voltage swing of 210 µV and gradient dV/ dΦ of 940 µV/Φ0. Consequently, the very low flux noise of 0.61 µΦ0/ Hz0.5 corresponding to the energy sensitivity ε of 8.6h at the white noise level was obtained by using a conventional flux-locked loop configuration. The low-frequency noise was also very low, 2.7 µΦ0/ Hz0.5 corresponding to ε= 170 h at 1 Hz. We could obtain very low flux noise for the SQUID which had the practical inductance using only a conventional readout circuit.
DC superconducting quantum interference devices (dc-SQUIDs) were fabricated in Co-doped BaFe 2 As 2 epitaxial films on (La, Sr)(Al, Ta)O 3 bicrystal substrates with 30° misorientation angles. The 18 × 8 µm 2 SQUID loop with an estimated inductance of 13 pH contained two 3 µm wide grain boundary junctions. The voltage–flux characteristics clearly exhibited periodic modulations with Δ V = 1.4 µV at 14 K, while the intrinsic flux noise of dc-SQUIDs was 7.8 × 10 − 5 Φ 0 Hz − 1/2 above 20 Hz. The rather high flux noise is mainly attributed to the small voltage modulation depth which results from the superconductor–normal-metal–superconductor junction nature of the bicrystal grain boundary.
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We have fabricated and measured the properties of micron-size single grain boundary junctions and dc superconducting quantum interference devices (SQUIDs). The width of the junctions was varied between 0.25 and 2 μm. The junctions were formed in c-axis oriented epitaxial films with a single 24° tilt boundary. They were fabricated using electron beam lithography and ion milling. All of the junctions operate at 77 K. The noise properties of SQUIDs made of these junctions have been characterized. They show a significant 1/f component which is comparable to published values. However, the white noise level, 3×10−31 J/Hz measured at 77 K, is the lowest ever reported.