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Fabrication and Receiver Measurements of a Diffusion-cooled Hot-electron Bolometer at 800 GHz

J. Stodolka, Kristof J. P. Jacobs

Published Dec 1, 2001• 2 citations
OpenAlex

Abstract

We present a fabrication process for diffusion-cooled niobium hot-electron bolometers using a self-aligned process with gold as an initial protection layer and aluminum as an etch mask that is removed by a wet etch. This process proves to be reproducible and has a yield of ~70 % per batch. Great care has been taken to avoid processing temperatures above 120 °C to minimize degradation of the Nb film. We have performed heterodyne measurements of an HEB in a fixed tuned waveguide mixer at 804 GHz and at an IF-range from 1-2 GHz. The approximate dimensions of the bridge are 240 x 200 x 14 nm3. The Niobium bridge has a critical temperature of 6.0 K and a normal state resistance of 16.5 Ω. A standard Y-factor measurement leads to a minimum noise temperature of 1200 K at 1 GHz IF. The coupled LO-power is estimated by the isothermal method to be 21 nW. Introduction Superconducting Hot-Electron-Bolometers (HEB) utilizing thin superconducting films have become established as sensitive mixers in the THz region. The thermal response time τ can be very small if the superconductor is thin enough that only the electron gas is heated and the cooling is fast enough. The bolometers described in this paper are cooled by out-diffusion of the hot electrons in normal conducting heat sinks (diffusion-cooled HEB) rather than interactions with phonons of the lattice (phononcooled HEB) [1]. To meet the requirements for astronomical applications such as SOFIA, thermal response times down to several picoseconds are needed to get intermediate frequencies up to 10 GHz. Because of τ ~ L [1] the dimensions of the bolometer bridge have to be very small. We have fabricated diffusion-cooled HEBs with short (L<300 nm) and narrow (<200 nm) bridges consisting of thin (10-14 nm) Niobium (Nb) on z-cut quartz substrates. The normal conducting heat sinks consist of 70 nm Gold (Au). In the following paragraph 1 e-mail: stodolka@ph1.uni-koeln.de we discuss problems and merits of several approaches for the fabrication of diffusioncooled HEBs. Device Fabrication Aside from a good reproducibility, the essential requirement for the fabrication of a diffusion-cooled HEB is a good transparency of the interface between the heat sinks and the material of the bolometer bridge. A thermal resistance results in a slower out-diffusion of the hot electrons and thus increases the effective bridge length and thermal response time. Defining the bolometer bridge by lift-off with subsequent deposition of the heat sinks (Fig. 1) [2] has the major disadvantage of high requirements for the overlap accuracy of the Electron-Beam-Lithography (EBL) system to position the heat sinks on the contact areas of the bridge. A solution is offered by the self-aligned process (Fig. 2). Here, the substrate is covered with a blanket layer of Nb. The heat sinks and a metal strip of the width of the bolometer bridge are deposited in succession. The bridge is now etched out of the blanket layer by using reactive ion etching (RIE) where the heat sinks and the metal strip serve as etch masks: the spacing between the heat sinks determines the bridge length while the metal strip defines the width. The overlap between Nb and Au heat sinks is large. Fig. 1: Outline of HEB fabrication by lift off (top view) a) Bolometer bridge defined by liftoff. b) Deposition of the heat sinks. The contact area (shaded) to the heat sinks is small. bolometer bridge

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Journal of Applied Physics•Apr 1, 2002•13 citations
We present a fabrication process for diffusion-cooled niobium hot-electron bolometers using a self-aligned process with gold as an initial protection layer and aluminum as an etch mask that is removed by a wet etch. This process proves to be reproducible and has a yield of ~70 % per batch. Great care has been taken to avoid processing temperatures above 120 °C to minimize degradation of the Nb film. We have performed heterodyne measurements of an HEB in a fixed tuned waveguide mixer at 804 GHz and at an IF-range from 1-2 GHz. The approximate dimensions of the bridge are 240 x 200 x 14 nm3. The Niobium bridge has a critical temperature of 6.0 K and a normal state resistance of 16.5 Ω. A standard Y-factor measurement leads to a minimum noise temperature of 1200 K at 1 GHz IF. The coupled LO-power is estimated by the isothermal method to be 21 nW. Introduction Superconducting Hot-Electron-Bolometers (HEB) utilizing thin superconducting films have become established as sensitive mixers in the THz region. The thermal response time τ can be very small if the superconductor is thin enough that only the electron gas is heated and the cooling is fast enough. The bolometers described in this paper are cooled by out-diffusion of the hot electrons in normal conducting heat sinks (diffusion-cooled HEB) rather than interactions with phonons of the lattice (phononcooled HEB) [1]. To meet the requirements for astronomical applications such as SOFIA, thermal response times down to several picoseconds are needed to get intermediate frequencies up to 10 GHz. Because of τ ~ L [1] the dimensions of the bolometer bridge have to be very small. We have fabricated diffusion-cooled HEBs with short (L<300 nm) and narrow (<200 nm) bridges consisting of thin (10-14 nm) Niobium (Nb) on z-cut quartz substrates. The normal conducting heat sinks consist of 70 nm Gold (Au). In the following paragraph 1 e-mail: stodolka@ph1.uni-koeln.de we discuss problems and merits of several approaches for the fabrication of diffusioncooled HEBs. Device Fabrication Aside from a good reproducibility, the essential requirement for the fabrication of a diffusion-cooled HEB is a good transparency of the interface between the heat sinks and the material of the bolometer bridge. A thermal resistance results in a slower out-diffusion of the hot electrons and thus increases the effective bridge length and thermal response time. Defining the bolometer bridge by lift-off with subsequent deposition of the heat sinks (Fig. 1) [2] has the major disadvantage of high requirements for the overlap accuracy of the Electron-Beam-Lithography (EBL) system to position the heat sinks on the contact areas of the bridge. A solution is offered by the self-aligned process (Fig. 2). Here, the substrate is covered with a blanket layer of Nb. The heat sinks and a metal strip of the width of the bolometer bridge are deposited in succession. The bridge is now etched out of the blanket layer by using reactive ion etching (RIE) where the heat sinks and the metal strip serve as etch masks: the spacing between the heat sinks determines the bridge length while the metal strip defines the width. The overlap between Nb and Au heat sinks is large. Fig. 1: Outline of HEB fabrication by lift off (top view) a) Bolometer bridge defined by liftoff. b) Deposition of the heat sinks. The contact area (shaded) to the heat sinks is small. bolometer bridge
We have fabricated Nb diffusion-cooled hot electron bolometers for a waveguide mixer around 700 GHz. The device in this work is a thin (12 nm) Nb bridge with a length and width of 220 nm and is defined by a two-step electron beam lithography process. The resistance as a function of temperature shows two transitions, which we attribute to the Nb bridge (6.1 K) and to parts of the Nb which are covered by the Au pads (5.4 K). We have measured a DSB receiver noise temperature of 2200 K at 735 GHz and a bath temperature of 3.3 K. No significant increase of the noise temperature is observed at IF frequencies between 1.1 and 1.7 GHz. The coupled LO power is estimated to be 35 nW.
Superconducting Hot Electron Bolometers (HEBs) are good candidates for detecting weak signals in the submillimeter or terahertz range. In this thesis work, a novel fabrication method was developed to make two types of niobium HEBs for different applications. HEBs were designed, fabricated, and then characterized at dc, microwave, and THz frequencies. The first type is a diffusion-cooled HEB, made with a short bridge that determines its cooling time. In this thesis, bridges were typically 400 nm long with bandwidths of about 1 GHz. These diffusion-cooled HEBs were developed as part of a collaboration with the University of Arizona (UA), to develop a proof-of-concept heterodyne array submillimeter camera. Devices were fabricated on thin fused quartz and silica substrates for waveguide coupling in the UA system for the astrophysically interesting 345 and 810 GHz atmospheric windows. The goal of this collaboration is to provide a basis of comparison between Nb diffusion-cooled HEB mixers and superconductorinsulator-superconductor mixers at these frequencies. The second type is a phonon-cooled HEB, made with a ∼3 µm long bridge. Its thermal response is dictated by the electron-phonon relaxation time. These devices were developed in collaboration with Prof. C. Schmuttenmaer’s lab in the Yale Chemistry department, Prof. G. Blake at Caltech,
We present a characterization of a 1.5 THz waveguide niobium titanium nitride (NbTiN) superconducting hot electron bolometer (HEB) mixer which can be pumped by a commercial solid state tunable local oscillator (LO) source. The NbTiN HEB mixer is made from a 12 nm thick NbTiN thin film deposited on a quartz substrate at room temperature. A gold electrode is formed in situ on the NbTiN thin film without breaking vacuum to ensure good contact. The uncorrected DSB receiver noise temperature is measured to be 1700 K at 1.5 THz, whereas the mixer noise temperature is derived to be 1000 K after corrections for losses of the input optics and the intermediate frequency (IF) amplifier chain. The required LO power absorbed in the HEB mixer is evaluated to be 340 nW by using an isothermal technique. The IF gain bandwidth is supposed to be about 1.3 GHz or higher. The present results show that good performance can be obtained at 1.5 THz even with a relatively thick NbTiN film (12 nm), as in the case of 0.8 THz. In order to investigate the cooling mechanism of our HEB mixers, we have conducted performance measurements for a few HEB mixers with different microbridge sizes both at 1.5 and 0.8 THz. The noise performance of the NbTiN HEB mixers is found to depend on the length of the NbTiN microbridge. The shorter the microbridge is, the lower the receiver noise temperature is. This may imply a contribution of the diffusion cooling in addition to the phonon cooling.
We report two typical experimental results of waveguide diffusion-cooled Nb hotelectron bolometer (HEB) mixers. The device is a thin (10 nm) Nb bridge with a length of 0.3 Am and a width of 0.9 pm and is defined using photolithography. In the first experiment, the resistance of a HEB is studied as a function of temperature. We observe two critical temperatures, which correspond to the 71. of the Nb bridge and the T, of the Nb under the Au pads, respectively. These two 71. define a superconducting transition width AT of a HEB. The reduced T. of the Nb under the Au pads is explained by the superconducting proximity effect. In the second experiment, we measure relative conversion efficiency vs intermediate frequency (IF) by using two coherent sources, a carcinotron and a Gunn oscillator, and determine an IF roll-off (/F, 011 ,ff ) between 0.6 and 1.2 GHz, in agreement with a value estimated in terms of the diffusion-cooled model.
Recent interest in bolometers for heterodyne mixing applications has prompted development of microbridges which are small enough to allow electron diffusion to dominate over electron-phonon interaction as a cooling mechanism. Prior results at 533 GHz have demonstrated several GHz intermediate frequency (IF) bandwidth. Here we describe our processing method in which the bolometer element is a 10 nm thin film of niobium defined by electron beam lithography down to dimensions of 80 nm. This microbridge is embedded in a normal metal (Au) antenna structure for 1.2 and 2.5 THz applications.
We present microwave (30 GHz) measurements on aluminum superconducting hot-electron bolometer (HEB) mixers. Aluminum HEB mixers have a lower superconducting transition temperature than niobium and niobium nitride devices, and are predicted to have improved sensitivity and require less local oscillator power. The devices studied consist of a narrow superconducting aluminum microbridge with contacts comprised of thick aluminum, titanium, and gold. A perpendicular magnetic field is used to suppress superconductivity in the contacts. The device length is much shorter than the electron–phonon inelastic length [L≪(Dτe–ph)1/2] and thus the intermediate frequency (IF) bandwidth is set by the diffusion time of hot electrons from the microbridge into the contacts. We discuss limitations on the IF bandwidth in very short HEB mixers with fully normal contacts. Overall, the microwave heterodyne mixing results show good performance with a mixer noise temperature inferred from the conversion efficiency and output noise of TM⩾4 K, double side band (DSB). Measurements at 618 GHz yield a conversion efficiency approximately 10 dB lower than observed at 30 GHz. Output saturation by background radiation is postulated to contribute significantly to this difference. A similar decrease in conversion efficiency in the microwave mixing measurements is observed when broadband noise is added to the rf input signal. We discuss the tradeoff between increased sensitivity and the occurrence of saturation effects in low transition temperature HEBs.