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arXiv:2304.13293 · Physical Review Applied

Handheld Device for Noncontact Thermometry via Optically Detected Magnetic Resonance of Proximate Diamond Sensors

Gabriel Abrahams, Ethan Ellul, Islay O. Robertson, Asma Khalid, Andrew D. Greentree, Brant C. Gibson, Jean‐Philippe Tetienne

Published May 23, 2023• 11 citations
arXivHTMLPDF

Abstract

Optically detected magnetic resonance (ODMR) spectroscopy of defect-rich semiconductors is being increasingly exploited for realizing a variety of practical quantum sensing devices. A prime example is the on-going development of compact magnetometers based on the nitrogen-vacancy (N-$V$) defect in diamond for the remote sensing of magnetic signals with high accuracy and sensitivity. In these applications, the ODMR-active material is integrated into the overall apparatus to form a self-contained sensor. However, some emerging applications require the sensing material to be in physical contact with an external object of interest, thus requiring an independent readout device. Here we present an ODMR meter, a compact device specially designed to allow convenient, contactless monitoring of ODMR in a target object, and demonstrate its application to temperature monitoring with N-$V$ defects. Our prototype is composed of a handheld readout head (integrating all the necessary optical components and a microwave antenna) and a control box connected to a laptop computer, all made primarily from commercial off-the-shelf components. We test our device using a N-$V$-rich bulk diamond as the object, demonstrate a temperature sensitivity of $10\phantom{\rule{0.2em}{0ex}}\mathrm{mK}/\sqrt{\mathrm{Hz}}$ in static conditions, and demonstrate the feasibility of handheld operation. The limitations to measurement speed, sensitivity, and accuracy are discussed. The presented device may find immediate use in medical and industrial applications where accurate thermometry is required, and can be extended to magnetic field measurements.

DOI
10.1103/physrevapplied.19.054076

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Optically detected magnetic resonance (ODMR) spectroscopy of defect-rich semiconductors is being increasingly exploited for realizing a variety of practical quantum sensing devices. A prime example is the on-going development of compact magnetometers based on the nitrogen-vacancy (N-VVV) defect in diamond for the remote sensing of magnetic signals with high accuracy and sensitivity. In these applications, the ODMR-active material is integrated into the overall apparatus to form a self-contained sensor. However, some emerging applications require the sensing material to be in physical contact with an external object of interest, thus requiring an independent readout device. Here we present an ODMR meter, a compact device specially designed to allow convenient, contactless monitoring of ODMR in a target object, and demonstrate its application to temperature monitoring with N-VVV defects. Our prototype is composed of a handheld readout head (integrating all the necessary optical components and a microwave antenna) and a control box connected to a laptop computer, all made primarily from commercial off-the-shelf components. We test our device using a N-VVV-rich bulk diamond as the object, demonstrate a temperature sensitivity of 10mK/Hz10\phantom{\rule{0.2em}{0ex}}\mathrm{mK}/\sqrt{\mathrm{Hz}}10mK/Hz​ in static conditions, and demonstrate the feasibility of handheld operation. The limitations to measurement speed, sensitivity, and accuracy are discussed. The presented device may find immediate use in medical and industrial applications where accurate thermometry is required, and can be extended to magnetic field measurements.
Modern sensing applications increasingly require the simultaneous measurement of multiple physical parameters with high sensitivity. However, traditional sensors often suffer from cross-sensitivity to different variables, making it difficult to separate overlapping effects, such as those caused by temperature and magnetic fields, in complex environments. This challenge highlights the need for robust multiparametric sensors capable of independently and accurately monitoring diverse conditions in real time. In this context, nitrogen-vacancy (NV) centers in diamond present a promising solution. These atomic-scale defects can be optically initialized, manipulated, and read out via laser excitation using optically detected magnetic resonance (ODMR), and they can operate under ambient and harsh conditions. In this work, we demonstrate a simultaneous and internally cross-validated sensing platform capable of detecting both magnetic fields and temperature with a sensitivity of around 500 nT/Hz and 10 mK/Hz, respectively. Our method integrates ODMR, zero-phonon line spectral shifts, and linewidth broadening, each providing independent spectral signatures sensitive to distinct physical effects. This approach enhances measurement precision, enables internal consistency checks, and decouples intertwined phenomena such as temperature-induced variations in magnetization. The demonstrated technique significantly expands the functional capabilities of NV-based sensors, advancing their potential for high-precision metrology in complex environments.
In modern-day quantum metrology, quantum sensors are widely employed to detect weak magnetic fields or nanoscale signals. Quantum devices, exploiting quantum coherence, are inevitably connected to physical constants and can achieve accuracy, repeatability, and precision approaching fundamental limits. As a result, these sensors have shown utility in a wide range of research domains spanning both science and technology. A rapidly emerging quantum sensing platform employs atomic-scale defects in crystals. In particular, magnetometry using nitrogen-vacancy (NV) color centers in diamond has garnered increasing interest. NV systems possess a combination of remarkable properties, optical addressability, long coherence times, and biocompatibility. Sensors based on NV centers excel in spatial resolution and magnetic sensitivity. These diamond-based sensors promise comparable combination of high spatial resolution and magnetic sensitivity without cryogenic operation. The above properties of NV magnetometers promise increasingly integrated quantum measurement technology, as a result, they have been extensively developed with various protocols and find use in numerous applications spanning materials characterization, nuclear magnetic resonance (NMR), condensed matter physics, paleomagnetism, neuroscience and living systems biology, and industrial vector magnetometry. In this chapter, NV centers are explored for magnetic sensing in a number of contexts. In general, we introduce novel regimes for magnetic-field probes with NV ensembles. Specifically, NV centers are developed for sensitive magnetometers for applications where microwaves (MWs) are prohibitively invasive and operations need to be carried out under zero ambient magnetic field. The primary goal of our discussion is to improve the utility of these NV center-based magnetometers.
This thesis investigates the theoretical foundations, material properties, and experimental realization of quantum sensors based on the Nitrogen-Vacancy (NV) centers in diamond, a solid-state system that combines quantum coherence with room-temperature operability. The first chapter introduces the principles of quantum sensing, outlining the fundamental definitions, operating protocols, and physical processes underlying the quantum measurement paradigm. Emphasis is placed on the quantum sensing Hamiltonian and the distinction between various classes of quantum sensors. The second chapter focuses on diamond as a host material and on the NV center as a quantum defect. The electronic structure, optical transitions, and spin properties of the NV center are analyzed in detail. Several techniques of NV-based magnetometry are presented, including continuouswave and pulsed optically detected magnetic resonance (ODMR). The discussion also addresses coherence times (T1, T2, and T∗2 ) and methods of diamond synthesis together with NV-center generation through irradiation and annealing. Chapter three develops the physical theory describing the NV center. The Hamiltonian formalism includes spin-spin, hyperfine, and quadrupolar interactions, as well as couplings to external magnetic fields. The chapter further introduces the Bloch sphere representation, magnetic resonance phenomena, and models of lightmatter interaction, ranging from the semiclassical to the fully quantum Rabi framework. A seven-level rate-equation model is proposed to capture the spin dynamics and optical cycling processes of the NV center. The fourth chapter reports the experimental results. After describing materials and methods, several ODMR-based vector magnetometry experiments are presented, highlighting different spectral regimes and the dependence of resonance features on the external magnetic field geometry. Additional studies demonstrate temperature sensing and microwave-free magnetometry techniques for mapping magnetic field distributions. Sensitivity analysis and calibration procedures are also discussed.
In this work we present a compact and portable tabletop magnetometer that utilizes negatively charged nitrogen-vacancy (NV) centers in diamond. The magnetometer is operated using a dual microwave resonance detection approach in combination with an optically detected magnetic resonance (ODMR) technique (mitigating drifts in results due to changes of the diamond temperature), capable of simultaneously exciting and registering two ODMR transitions. The experimentally measured magnetic field noise-floor is ≈2.3 nTHz\approx 2.3~\textrm{nT}\sqrt{\textrm{Hz}}≈2.3 nTHz​ while the calculated shot-noise-limited magnetic field sensitivity is ≈585 pTHz\approx 585~\textrm{pT}\sqrt{\textrm{Hz}}≈585 pTHz​ when excited with a continuous wave laser at 0.5~W. These results pave the way for realizing a simple set-up magnetometer for precise single axis magnetic field measurements for example for accurate electric current measurements for stabilization purposes and magnetic communication applications.
Optically detected magnetic resonance (ODMR) of nitrogen-vacancy centers in diamonds, in addition to optical excitation with green light, requires microwave excitation and thus a microwave structure. While many different microwave structures including microwave resonators have been presented in the past, none of them fulfilled the need to fit inside the miniaturized quantum magnetometer with limited space used in this work. This is why a novel microwave resonator design using commercially available printed circuit board technology is proposed. It is demonstrated that this design is of small form factor, highly power efficient and low-cost, with very good reproducibility, and in addition, it can be fabricated as a flexible printed circuit board to be bent and thus fit into the miniaturized sensor used in this work. The design choices made for the resonator and the way in which it was trimmed and optimized geometrically are presented and ODMR spectra made with a miniaturized quantum sensor in combination with such a resonator, which was fed by a microwave generator set to different microwave powers, are shown. These measurements revealed that a microwave power of −4 dBm is sufficient to excite the ms = ±1 states of the nitrogen-vacancy centers, while exceeding −1 dBm already introduces sidebands in the ODMR spectrum. This underlines the efficiency of the resonator in exciting the nitrogen-vacancies of the diamond in the sensor platform used and can lead to development of low-power quantum sensors in the future.
Wide-field nitrogen-vacancy (NV) magnetic imaging at cryogenic temperatures requires microwave excitation and reliable knowledge of the temperature near the sensing region. Here, we report an integrated diamond quantum-sensing platform combining an ensemble of NV centers with a boron-doped diamond (BDD) microwave antenna and thermometer formed on the same diamond substrate. The BDD antenna provides microwave excitation for optically detected magnetic resonance measurements, and the BDD thermometer monitors the thermal environment near the NV sensing region. The BDD thermometer detected laser-induced local heating that was not clearly resolved by a stage-mounted thermometer. Using this platform, we imaged the temperature-dependent Meissner response of multiple cuprate superconductors while recording the temperature. These results demonstrate that the integrated BDD--NV platform provides a practical approach for cryogenic wide-field magnetic imaging with integrated microwave delivery and local thermometry.