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Journal of Physics Conference Series

Spectroscopic Characterization and Vapor Pressure Analysis of Homemade Rubidium Vapor Cells

A Kaewko, N Chattrapiban, Nithiwadee Thaicharoen

Published Jan 1, 2025• 0 citations
Publisher

Abstract

Abstract Vapor glass cells play a crucial role in spectroscopic research and metrology applications. As the demand for portable quantum devices grows, characterizing vapor glass cells based on their form factor becomes essential. Therefore, exploring cost-effective homemade alternatives is increasingly important in this regard. To address this, we have successfully produced a cost-effective homemade vapor cells containing rubidium atoms in our laboratory. In this work, we characterized the atomic absorption properties of the homemade vapor cells to extract the vapor pressure of atoms inside the cell and compare it to commercially available reference cells. The experimental procedure involves directing a laser beam with a wavelength of 780 nm through the vapor cell and measuring the absorption signals using a photodiode. Additionally, we calculate rubidium absorption cross section to extract the absorption data and compare it to the experimental obtained result to determine the vapor pressure within the cell. This study demonstrates that our homemade cell exhibits a comparable absorption profile and vapor pressure to that of a commercial cell. This suggests that our homemade cell is suitable for spectroscopic measurements and presents a cost-effective solution for future applications in portable quantum devices.

DOI
10.1088/1742-6596/2934/1/012019

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Abstract Vapor glass cells play a crucial role in spectroscopic research and metrology applications. As the demand for portable quantum devices grows, characterizing vapor glass cells based on their form factor becomes essential. Therefore, exploring cost-effective homemade alternatives is increasingly important in this regard. To address this, we have successfully produced a cost-effective homemade vapor cells containing rubidium atoms in our laboratory. In this work, we characterized the atomic absorption properties of the homemade vapor cells to extract the vapor pressure of atoms inside the cell and compare it to commercially available reference cells. The experimental procedure involves directing a laser beam with a wavelength of 780 nm through the vapor cell and measuring the absorption signals using a photodiode. Additionally, we calculate rubidium absorption cross section to extract the absorption data and compare it to the experimental obtained result to determine the vapor pressure within the cell. This study demonstrates that our homemade cell exhibits a comparable absorption profile and vapor pressure to that of a commercial cell. This suggests that our homemade cell is suitable for spectroscopic measurements and presents a cost-effective solution for future applications in portable quantum devices.
Abstract Glass cells containing neutral atoms are commonly employed in spectroscopy experiments and have potential applications in metrology. The temperature of the vapor plays a vital role as it directly influences the absorption rate of rubidium atoms. In this research, we study the effect of vapor temperature on the absorption spectrum of rubidium atoms. We observed the broadening of the spectral line and increased absorption, enabling us to determine the absorbance of atoms within the cell. These results provide valuable insights for our future work to characterize absorbance of homemade vapor cells for portable quantum device applications.
A new method and its principle are presented for measuring the each component gas pressures in Rubidium (Rb) by the analysis of absorption spectral profile. The experiment system is set up to obtain Rb absorption spectra. And then each component gas pressures in atom vapor cell is estimated. First, the relationships between transmittance of probe light, atom density and absorption cross section are introduced, and the factors which influence the absorption spectral profile and methods to measure gas pressures are given. Second, the frequency-dependence curves of transmittance and the absorption spectra are obtained through tuning the laser frequency through the Rb D1 transition. Finally, the gas pressures of Rb, N2 and He are achieved, through fitting absorption spectral profile referring to half-width and minimum transmittance value of absorption spectra. The experiment results show that gas pressures in Rb atom vapor cell can be accurately measured by absorption spectrometric methods, which will be helpful for the following study of atom vapor cell. The gas pressures of N2 and He measured by the experiments are well matched with design values. The Rb gas pressure is 30%~50% less than the saturated vapor pressure and the suppression may be due to the adsorption of the cell surfaces coated with octadecyltrichlorosilane (OTS) film.
We report on the atomic spectroscopy and laser frequency stabilization using a new type of a miniaturized glass vapor cell with a scalable thickness varying from 500 nm up to 8 μm. The cell is fabricated by lithography and etching techniques in a Pyrex glass substrate, followed by anodic bonding. It is filled with rubidium vapor using a distillation procedure. This simple and cost-effective fabrication method provides an attractive and compact solution for atomic cells, with applications in quantum metrology, sensing, communication, and light-vapor manipulations at the subwavelength scale. Using the fabricated cell, we have performed fluorescence and transmission spectroscopy of the Rubidium D2 line and observed sub-Doppler broadened lines. As an example, for a potential application, we have used the fabricated cell to demonstrate the stabilization of a 780 nm diode laser to the level about 10−10 in fractional frequency.
In the sealed-off cesium vapor cell studied in this work, a residual rubidium fraction of approximately $\sim1%wasobserved.WeinvestigatetheopticalresponseofthesetraceRbatomsinasealed1 cmlongCs−filledvaporcell.Despitethelowconcentration,laserexcitationat795 nmallowstheobservationofsaturatedabsorptionandelectromagneticallyinducedtransparency(EIT)resonances.ThesurroundingCsvaporeffectivelyactsasabuffermedium,reducingtheRbatomicvelocityandincreasingtheinteractiontimewiththelaserfield,whichimprovestheEITsignal.Theexperimentsareperformedinanall−sapphirecellthatcanbeheatedupto5001\% was observed. We investigate the optical response of these trace Rb atoms in a sealed 1~cm long Cs-filled vapor cell. Despite the low concentration, laser excitation at 795~nm allows the observation of saturated absorption and electromagnetically induced transparency (EIT) resonances. The surrounding Cs vapor effectively acts as a buffer medium, reducing the Rb atomic velocity and increasing the interaction time with the laser field, which improves the EIT signal. The experiments are performed in an all-sapphire cell that can be heated up to 5001%wasobserved.WeinvestigatetheopticalresponseofthesetraceRbatomsinasealed1 cmlongCs−filledvaporcell.Despitethelowconcentration,laserexcitationat795 nmallowstheobservationofsaturatedabsorptionandelectromagneticallyinducedtransparency(EIT)resonances.ThesurroundingCsvaporeffectivelyactsasabuffermedium,reducingtheRbatomicvelocityandincreasingtheinteractiontimewiththelaserfield,whichimprovestheEITsignal.Theexperimentsareperformedinanall−sapphirecellthatcanbeheatedupto500^{\circ}$C without window blackening, unlike conventional glass cells. From the measured spectra, Cs--Rb collisional cross sections are estimated. These results show that residual atomic species in high-temperature vapor cells can be exploited for spectroscopic and nonlinear-optical studies.
Abstract : An absorption spectrum of a rubidium alkali metal dispenser (AMD) cell was obtained in order to determine the system s suitability for use in a diode pumped alkali laser (DPAL) and use in high-temperature spectroscopic studies. The AMD produced a concentration of 3.65 0.16 1010 cm-3, which is in the ideal range for Beer s Law region absorption spectroscopy, but too low to make a high-power DPAL in a 10 cm cell with a poor Q resonator. Before AMDs can be used to determine pressure broadening and shifting coefficients, issues concerning contamination and producing rubidium vapor at pressure must be resolved. A separate portion of this study focused on a sealed rubidium Pyrex cell with neon buffer gas. A continuous wave titanium sapphire beam was focused into the cell with various lenses to maximize pump intensity through the cell. Images were taken of the side fluorescence of the cell to determine the bleached regions. The total horizontal propagation of the bleached region for each image was proportional to the pump laser power and the inverse of the rubidium vapor density. Disparity between the bleached volume estimated from the beam parameters and the theoretical bleached volume suggested the beam intensity had a strong radial dependence. When the pump wavelength was changed, visible side fluorescence occurred in regions where the laser intensity was at least 0.125 times the saturation intensity and therefore not in the regions where the decay was determined by Beer s Law.
The microfabricated alkali atomic vapor cells are essential for the chip scale quantum sensing instruments which provide a robust, simple platform for precision measurement for a quantum system. In order to solve the problems of difficult quantitative filling of alkali atoms and poor hermeticity in the fabricated process of the cells, the preparation of microfabricated alkali atomic vapor cells with good hermeticity is studied. The cells are fabricated by the microelectromechanical system (MEMS) technology. Rubidium (Rb) atomic vapor cells with nitrogen (N 2 ) as buffer gas are successfully obtained by photolysis of rubidium azide (RbN 3 ), which is confirmed by the presence of Rb vapor in the cells through absorption spectroscopy for the 5S 1/2 → 5P 3/2 and 5S 1/2 → 5P 1/2 transitions in Rb atoms at 780 nm and 795 nm. The influences of filling amount and baking temperature of RbN 3 solution on the hermeticity of the microfabricated atomic vapor cells are demonstrated. Also, the influences of filling amount of Rb atoms and temperature on the absorption spectrum intensities of Rb vapor in the cells are studied through a theoretical analysis. This research provides a reference for the design and preparation of high quality microfabricated alkali atomic vapor cells.