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Current Science

Cryogenic Measurement Set-Up for Characterization of Superconducting Nano Structures for Single-Photon Detection Applications

Manju Singh, Rishu Chaujar B, Rajib Kumar Rakshit

Published Sep 1, 2018• 6 citations
Publisher

Abstract

We discuss the design and development of a cryogenic set-up down to ~1.8 K for carrying out measurements on superconducting nanowire single-photon detectors.The set-up consists of two separate low-temperature inserts, one for electrical characterization and the other for optical measurements and characterization of single-photon detectors.A sample holder with necessary arrangements for precise alignment of laser light with the active area of the device to enhance optical coupling efficiency has been designed for the optical probe.The invar alloy has been used for the sample holder to ensure that the alignment is not disturbed at low temperature.Single-mode fibres due to their high transmission rate, minimum attenuation and least distortion have been used to shine light on the samples.The sample holder with 20-pin LCC socket and matching chip carrier provides convenient and fast sample mounting in the electrical insert.Mumetal has been employed to cover the sample space in both the inserts in order to attenuate any electromagnetic interference.Temperature stability with the passage of time has been monitored.It has been found that variation in temperature is less than 10 mK at the lowest operating temperature.Another important advantage of the system is its low enough liquid helium loss rate (~100 ml/h) with all inserts, which allows uninterrupted measurements for several days without any refilling of liquid helium.

DOI
10.18520/cs/v115/i6/1085-1090

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We discuss the design and development of a cryogenic set-up down to ~1.8 K for carrying out measurements on superconducting nanowire single-photon detectors.The set-up consists of two separate low-temperature inserts, one for electrical characterization and the other for optical measurements and characterization of single-photon detectors.A sample holder with necessary arrangements for precise alignment of laser light with the active area of the device to enhance optical coupling efficiency has been designed for the optical probe.The invar alloy has been used for the sample holder to ensure that the alignment is not disturbed at low temperature.Single-mode fibres due to their high transmission rate, minimum attenuation and least distortion have been used to shine light on the samples.The sample holder with 20-pin LCC socket and matching chip carrier provides convenient and fast sample mounting in the electrical insert.Mumetal has been employed to cover the sample space in both the inserts in order to attenuate any electromagnetic interference.Temperature stability with the passage of time has been monitored.It has been found that variation in temperature is less than 10 mK at the lowest operating temperature.Another important advantage of the system is its low enough liquid helium loss rate (~100 ml/h) with all inserts, which allows uninterrupted measurements for several days without any refilling of liquid helium.
Superconducting nanowire single-photon detectors (SNSPDs) are nanodevices usually made from thin niobium nitride (NbN) films. Operated at liquid helium temperature, they can exhibit high detection efficiency with low dark-counts associated with a fast response time and a low timing jitter. Covering a broad detection range from ultraviolet to mid-infrared, SNSPDs are a very attractive alternative to silicon or gallium arsenide based semiconductor detectors for fiber based telecommunication when single-photon sensitivity and high counting rates are necessary. \nEfficient packaging and fiber coupling of a SNSPD is in itself a real challenge and is often a limiting factor in reaching high system quantum efficiency. Our approach makes use of a controlled expansion alloy which has been adequately heat treated to enhance its characteristics for cryogenic operation. This insures the integrity of the optical coupling at cryogenic temperatures while done at room temperature. It also provides a good attenuation for electromagnetic interference due to the high relative permeability of the nickel-iron alloy. The small form factor of this pigtailed optical fiber package makes it versatile and could be easily integrated with a commercial cryogen-free system or simply dipped into a standard helium transport Dewar. We report on our theoretical and experimental methodology to evaluate the optical coupling quality and present the optoelectronic characterization of two devices packaged in this way. Electrical simulation is studied to understand the speed limitation factor inherent to these devices and preliminary speed and jitter measurements are reported.
Superconducting nanowire single photon detectors (SNSPDs) are a rapidly maturing detector technology that offer superior performance relative to competing infrared photon counting technologies. The original experimental work presented here explores three novel methods of improving and analysing detector characteristics, employing low-temperature piezoelectric motors at temperatures below 4 K in a closed-cycle cryostat. Utilizing the low-temperature piezoelectric nanopositioners in tandem with a miniature confocal microscope, this work specifically shows a spatially-separable parallel-wire SNSPD demonstrating one- and two-pixel photon discrimination, with the detector responding more quickly when triggering two pixels. The work demonstrates nanoantenna-coupled SNSPDs, which are simulated, designed, and tested using the same nano-optical setup. In these an increased local absorption into the nanowire is seen at the antennas' resonant wavelengths, enhancing the efficiency of the detector by up to 130 %. Finally, a modified optical setup using a distributed Bragg reflector fibre in place of the microscope to form a tunable cavity around two configurations of SNSPD is demonstrated, improving absorption of the incident light into the nanowire across the whole active area. For these, enhancement in the system detection efficiency of up to 40 % is seen.
Efficient packaging and fiber coupling of a superconducting niobium nitride nanowire single photon detector is in itself a real challenge and is often a limiting factor to reach a high system quantum efficiency. Our approach makes use of a controlled expansion alloy, Carpenter Invar 36, that has been adequately heat treated to enhance its characteristics for cryogenic operation. This insures the integrity of the optical coupling done at room temperature while providing a good attenuation for electromagnetic interference due to the high relative permeability of this nickel-iron alloy. The small form factor of this optical fiber pigtailed package makes it versatile and could be easily integrated with a commercial cryogen-free system or simply dipped into a standard helium transport Dewar. We report on our experimental methodology to evaluate the optical coupling quality and present the optoelectronic characterization of two devices packaged in this way.
We have developed a practical superconducting nanowire single photon detector (SNSPD) system with our superconducting thin films and devices fabrication, optical coupling packaging, and cryogenic technology. The SNSPD devices were fabricated from high-quality niobium nitride (NbN) ultra-thin films that were epitaxially grown on single-crystal MgO substrates, and optical cavity structure were applied for improvement of photo absorption efficiency. The SNSPD system was developed based on a compact Gifford-McMahon (GM) cryocooler, in which SNSPD can operate continuously at temperature of 2.9 K +/- 10 mK with low power consumption without any liquid cryogens. The system detection efficiencies at 1550 nm wavelength (at a 100 Hz dark count rate) were found to be 2.6% for device without optical cavity and 21% for device with optical cavity. The response speed of devices showed maximally 200 MHz with 5 × 5 mm square device, and timing jitter of 100 ps full width at a half maximum (FWHM) was observed.
Single photon detection advanced rapidly in the last decade. The superconducting nanowire single-photon detector (SNSPD) is an emerging technology, which offers low dark count rates, broadband sensitivity from visible to mid-infrared wavelengths and very high quantum efficiency. All these features are appealing for future emerging applications in remote gas sensing, quantum key distribution and quantum information processing. By enclosing the detector in an optical cavity, tuned to the operating wavelength, the total system detection of the SNSPD is improved. Based on the cavity design, the detector absorption is boosted at the desired experimental wavelength. Devices have been fabricated and tested, in this thesis, with enhanced detection efficiency at near-infrared, infrared and mid-infrared wavelengths. NbTiN detectors fabricated on Ta2O5 / SiO2 distributed Bragg reflectors (DBR) for front-side coupling exhibit a system detection efficiency of ≈ 90% at λ = 940 nm for the best device measured. SNSPDs were also fabricated in NbTiN on metallic mirrors for back-side coupling for 1550 and 2333 nm experimental wavelengths. The first design exhibited a system detection efficiency of ≈ 84.5%, at λ = 1550 nm for the best device measured. The second exhibited low system detection efficiency since the device suffered from unexpectedly high dark count rate mainly due to blackbody radiation at 2.2 K. However, it was possible to measure the timing jitter of this device at 350 mK indicating a FWHM of 84 ps. Another technique to improve the total system detection efficiency of the SNSPD, is by fabricating a hairpin-shaped nanowire atop a single mode waveguide. In this design, photons travel through the waveguide and via evanescent coupling are absorbed in the nanowire. These SNSPD devices have been designed to thread along single mode Si ridge waveguides using a hairpin-shaped nanowire structure, which offers enhanced coupling and absorption efficiency via evanescent coupling. These ultra-thin superconducting MoSi detectors are precisely patterned on top of a single mode Si waveguide (600 nm) with alignment error less than 40 nm. Low temperature electrical and nano-optical characterization was carried out using a two-stage pulse tube (PT) coldhead, using an additional 4He / 3He sorption pump, low vibration characterization of SNSPD devices at 350 mK was carried out. Characterised devices exhibit low dark count rate <5 counts per second and timing jitter of ≈ 83 ps full width half maximum (FWHM) at wavelength (λ) = 1550 nm and at critical current ≈ 30 µA.
Superconducting Nanowire Single Photon Detectors (SNSPDs) have become an integral part of quantum optics in recent years because of their high performance in single photon detection. We present a method to replace the electrical input by supplying the required bias current via the photocurrent of a photodiode situated on the cold stage of the cryostat. Light is guided to the bias photodiode through an optical fiber, which enables a lower thermal conduction and galvanic isolation between room temperature and the cold stage. We show that an off-the-shelf InGaAs–InP photodiode exhibits a responsivity of at least 0.55 A/W at 0.8 K. Using this device to bias an SNSPD, we characterize the count rate dependent on the optical power incident on the photodiode. This configuration of the SNSPD and photodiode shows an expected plateau in the single photon count rate with an optical bias power on the photodiode above 6.8 µW. Furthermore, we compare the same detector under both optical and electrical bias, and show there is no significant changes in performance. This has the advantage of avoiding an electrical input cable, which reduces the latent heat load by a factor of 100 and, in principle, allows for low loss RF current supply at the cold stage.