The first local oscillators based on moving magnetic flux quanta in long Josephson junctions are being developed for superconducting integrated quasi-optical SIS receivers. In order to further refine these oscillators one has to understand the complex dynamics of these devices. Since the local tunnel current is one of the most important internal junction parameters which together with the boundary conditions determine the dynamics, it is of vital importance to experimentally determine the current density throughout the entire junction with high spatial resolution. Here we report on measurements on different oscillator samples, performed with a novel Cryogenic Scanning Laser Microscope (CSLM) having a spatial resolution of less than /spl plusmn/2.5 /spl mu/m over a 500 /spl mu/m/spl times/50 /spl mu/m wide scanning area in the temperature range 2 K-300 K. Even though the dynamical states are extremely sensitive to external noise this microscope enables us to make stable in-situ measurements on operating Josephson junctions. Recent results are presented and discussed.>
The first local oscillators based on moving magnetic flux quanta in long Josephson junctions are being developed for superconducting integrated quasi-optical SIS receivers. In order to further refine these oscillators one has to understand the complex dynamics of these devices. Since the local tunnel current is one of the most important internal junction parameters which together with the boundary conditions determine the dynamics, it is of vital importance to experimentally determine the current density throughout the entire junction with high spatial resolution. Here we report on measurements on different oscillator samples, performed with a novel Cryogenic Scanning Laser Microscope (CSLM) having a spatial resolution of less than /spl plusmn/2.5 /spl mu/m over a 500 /spl mu/m/spl times/50 /spl mu/m wide scanning area in the temperature range 2 K-300 K. Even though the dynamical states are extremely sensitive to external noise this microscope enables us to make stable in-situ measurements on operating Josephson junctions. Recent results are presented and discussed.>
A novel cryogenic scanning laser microscope with a spatial resolution of less than 5 μm has been designed for on-chip in situ investigations of the working properties of normal and superconducting circuits and devices. The instrument relies on the detection of the electrical response of the circuit to a very localized heating induced by irradiation with 675 nm wavelength light from a semiconductor laser. The hot spot is moved by a specially designed piezoelectric scanner sweeping the tip of a single-mode optical fiber a few μm above the circuit. Depending on the scanner design the scanning area can be as large as 50×500 μm2 at 4.2 K. The microscope can be operated in the temperature range 2–300 K using a standard temperature controller. The central microscope body is mounted inside the vacuum can of a dip-stick-type cryoprobe. A damped spring system is used to reduce interference from extraneous mechanical vibrations. The microscope is integrated in a personal-computer-based data acquisition and control setup.
The low-current fluctuations at cryogenic temperatures together with the low dynamical resistance in the resonant states of Josephson tunnel junctions allow for the realization of superconducting oscillators up to the THz range with ultra-low spectral linewidth. By virtue of the Josephson frequency-voltage relationship, we show that the same properties can be exploited for the practical realization of magnetic flux-to-voltage transducers based on the flux–flow in long Josephson tunnel junctions whose intrinsic low-frequency voltage fluctuations at amount to few , that is, too small to be measured by any present semiconductor electronics. Nevertheless, by using a double transformer SQUID amplifier we demonstrate that the (amplitude) voltage spectral density, , of an all-niobium sensor does not exceed the level of and is not affected by excess noise at least down to few hertz. Such ultra-low white noise, corresponding to a magnetic field noise , together with a highly linear and broadband voltage responsivity over a wide magnetic flux range, makes the flux–flow magnetometers potentially competitive with SQUID-based devices.
We have designed and characterized a micro-SQUID with dispersive readout for use in low temperature scanning probe microscopy systems. The design features a capacitively shunted RF SQUID with a tunable resonance frequency from 5 to 12 GHz, micrometer spatial resolution, and integrated superconducting coils for local application of magnetic fields. The SQUID is operated as a nonlinear oscillator with a flux- and power-dependent resonance frequency. Measurements for device characterization and noise benchmarking were carried out at 4 K. The measured flux noise above 10 kHz at 4 K is 80 nΦ0 Hz−1∕2 at a bandwidth of 200 MHz. Estimations suggest that one can benefit from parametric gain based on inherent nonlinearity of the Josephson junction and reduce the flux noise to 30 nΦ0Hz–1∕2 at 100 mK, which corresponds to 10.6 μBHz–1∕2 for a magnetic moment located at the center of the pickup loop.Measuring the magnetic response of mesoscopic samples or mapping it vs. position for extended systems is effective methods for revealing the fundamental quantum properties of condensed matter systems. Over the past few decades, many advanced magnetic imaging schemes have been developed, including magnetic force microscopy,1 scanning Hall probe microscopy,2 superconducting interference devices (SQUIDs),3,4 and NV center based magnetometry.5 The high sensitivity, low back action, and low power dissipation of SQUIDs make them attractive for many types of low temperature experiments. One classic example is the central role of scanning SQUID microscopy in tests of pairing symmetry of high-Tc cuprate superconductors.6 Other prominent applications are the thermodynamic characteristics of persistent currents in normal metal rings7 and proof of edge states in topological insulators in the quantum spin Hall regime.8A key performance for a SQUID is its flux sensitivity. Parametric amplification has been harnessed in nano-SQUIDs based on aluminum junctions9,10 in order to reduce the flux noise down to 30 nΦ0Hz–1∕2 with a bandwidth exceeding 60 MHz.10 Recent studies on parametric amplifiers and dispersive readout of superconducting qubits also harness the nonlinearity of the Josephson junction to boost sensitivity.11–13In scanning SQUID microscopy, signal sources often behave dipole-like, such as superconducting vortices in mesoscopic dots or currents in mesoscopic rings. Smaller SQUIDs provide better coupling to smaller samples which leads to higher spin sensitivity3,14 as the magnetic field of a dipole decreases with 1/r3. Various approaches have been pursued to reduce the size. The smallest nano-SQUID to date has been fabricated by evaporating Nb or Pb15 onto the apex of a sharp quartz tip reaching a loop diameter of below nm and a spin sensitivity of 0.38 μBHz−1/2 at tens of kHz bandwidth. Compared to such size-optimized devices, micro-SQUIDs fabricated using a standard Nb technique have the advantage of on-chip field coils and modulation coils,14 and can be operated at 4 K allowing for a wide range of applications. However, these come at the cost of larger pick-up loops of a few microns and a resulting poorer spin sensitivity of 200 μBHz−1/2 for a magnetic moment located at the center of the pickup loop.The limitation of large pickup loops was previously only overcome by devices with pickup loops defined by the focused-ion-beam,16 but has recently also been achieved by improvements in lithography and shown to offer better spatial resolution as well.17 Here, we present a scanning micro-SQUID which is based on the same fabrication technology incorporating another major advancement. Our design exploits the parametric amplification based on nonlinearities of the SQUID to boost sensitivity. The combination of a smaller pickup loop and parametric amplification of the signal leads to better spin sensitivity (10.6 μBHz−1/2) and higher bandwidth (200 MHz) compared to traditional DC micro-SQUIDs in which the flux sensitivity is mainly limited by internal dissipation.Our devices were fabricated at Hypres Inc. using planarized Nb/AlOx/Nb trilayer Josephson junction technology, including two planarized Nb layers with approximately 0.8 μm minimum feature size. The SQUID consists of a superconducting ring shunted by one Josephson junction with a designed critical current of 20 μA [Fig. 1(a)]. With this geometry, the SQUID is gradiometric, i.e., the effect of any homogeneous background magnetic field approximately cancels out. The smallest pickup loops implemented have an inner (outer) diameter of 1 μm (2 μm). The superconducting loop is shunted by an on-chip parallel-plate capacitor with amorphous silicon dioxide as dielectric which was designed to have a capacitance of 80 pF. The superconducting loop and the capacitor form a resonator with a flux dependent resonance frequency from 5 to 12 GHz. The pickup loops are placed on opposite corners of the parallel-plate capacitor at a distance of about 450 μm so that one loop can be located in close proximity to the sample while the other is kept far away from it. External fields can be applied to the sample by local single-turn field coils situated around each pickup loop. The field coils are fully integrated into the chip layout and can also be used to bias the SQUID at its most sensitive point. Compared to using additional modulation coils,14 this approach has the advantage of reducing the total device inductance, which leads to a higher sensitivity.18 In a scanning microscope, the field coil at the rear end (away from the sample) can be used to bias the SQUID or operate it in flux feedback such that resulting stray fields will not act on the sample, apart from a weak screening current through the pickup loop. The effective diameter of each coil is 7.5 μm, resulting in a mutual inductance of about 0.34 Φ0/mA (for the smallest pickup loop). The SQUID resonator is connected by an on-chip Z0 = 50 Ω coplanar waveguide (CPW) transmission line to the bonding pads. The two field coils are connected by two smaller CPWs to the bottom edge bonding pads [Fig. 1(c)], ending in two parallel-stripline waveguides running alongside the edges of the capacitor towards the respective field coils. Based on estimations, it should thus be possible to apply high frequency signals of at least several GHz to SQUID and sample.
The first object of this work is to theoretically study the effects of tunnel junction parameters on flux-flow Josephson oscillators (FFOs) by numerical simulation and to experimentally study the rf properties of FFOs by integrating them together with an SIS (superconductor-insulator-superconductor) mixer/detector on a chip. By using a CAD modeled integrated sub-mm wave receiver, the composite linewidth of two FFOs was measured to be less than 2.1 MHz in the band 280-330 GHz. The receiver consists of two identical FFOs and an SIS mixer. The linewidth was determined by mixing the two signals in the SIS mixer and analyzing the intermediate frequency. The output power coupled to a 10 .OMEGA. microstripline was about 0.5 µW, and could be adjusted by changing the current bias of the oscillator. The FFOs are connected to the SIS mixer via interdigital capacitors. The FFOs and the SIS element are made of Nb/NbOx/PbBi junctions by the "reactive ion beam oxidation" technique with the critical current density jc controlled by the oxidation time. Lift-off stencils for defining the junction sizes and the top-electrodes were made by using electron-beam writing on PMMA/Copolymer double layer resist. The jc of a long Josephson junction (LJJ) determines the fluxon motion. For LJJs which had jc > 1 kA/cm2, velocity-matching (VM, where the phase velocity of propagating fluxons equals that of the electromagnetic wave in the LJJ) steps could be tuned linearly from about 0.2 to 1.4 mV by an applied magnetic field. Coupled radiation at around 100 GHz (about 3 nW), 261 GHz (4.6 nW), and 330 GHz (0.43 µW), from flux-flow oscillations, was observed. From the step's steepness, the junction quality factor QJ is determined. QJ is between 4 to 7 in the voltage range of 0.4 to 1 mV. Coupled radiation (> 3 nW) at around 100 GHz corresponding to resonant soliton oscillation in low jc samples (250 to 1000 A/cm2) was detected. Simulations show that, for a uniform bias feed, the height of the VM step .gammam increases almost linearly with the external magnetic field .beta.e and the quasiparticle loss .alpha., but is less dependent on the surface loss .beta.. An approximate expression .gammam = a + .alpha(1+b).beta.e agrees with simulations. The maximum ac output voltage decreases with increasing dampings .alpha. and .beta.. It is important to include the .beta.-term in the mathematical model. The second part of this work is devoted to rf properties of long YBa2Cu3O7-.delta. (YBCO) grain boundary junctions made on 0- 32 °. [001]-tilt YSZ bicrystals. Josephson flux-flow resonances and Fiske resonances were observed. The first resonances could be tuned from about 0.5 to 2.0 mV in a 30 µm long junction at 16 K, and we determined the ratio between barrier thickness and relative dielectric constant td/.epsilon.r=2.9 Å and the loss .alpha.= 1.3 at 16 K. Simulations support the experimental observation that Josephson vortices can propagate unidirectionally in an overdamped, homogeneous junction up to .alpha.Ã? 2. From the Fiske resonances at 256-638 GHz, their Q-values, and the Steward-McCumber parameter, we find td/.epsilon.r=4 Å, the London penetration depth .gamma.L=145±5 nm and the surface resistance RS ~20 m.OMEGA. at 280 GHz. We conclude that the boundary is dielectric and the YBCO grains are well superconducting within 5-20 nm from the boundary. The dielectric between the grains could be part of a tunnel barrier and/or a matrix for filamentary conduction. Josephson flux-flow transitors based on long bicrystal junctions were made with an Au loop used as the control line. The line modulated the critical current Ic. Current gain larger than unity was obtained below 70 K. The gain increased with the junction length and varied roughly like the square root Ic when adjusting the temperature. A transresistance larger than 5 .OMEGA. was obtained at 15 K. Better performance is expected from junctions with high current densities.
Low temperature scanning electron microscopy (LTSEM) offers the possibility for spatially resolved investigations of microwave properties of single Josephson junctions, superconducting striplines, resonators, and complex cryoelectric circuits during their operation. The spatial resolution of about 1 μm is at least two orders of magnitude better than the typical wavelength (≳100 μm in the elements) in the frequency range of interest (50–500 GHz). We demonstrate that LTSEM is a well suited tool for the experimental investigation of superconducting microwave devices and cryoelectronic circuits.
We have designed and characterized a micro-SQUID with dispersive readout for use in low temperature scanning probe microscopy systems. The design features a capacitively shunted RF SQUID with a tunable resonance frequency from 5 to 12 GHz, micrometer spatial resolution, and integrated superconducting coils for local application of magnetic fields. The SQUID is operated as a nonlinear oscillator with a flux- and power-dependent resonance frequency. Measurements for device characterization and noise benchmarking were carried out at 4 K. The measured flux noise above 10 kHz at 4 K is 80 nΦ0 Hz−1∕2 at a bandwidth of 200 MHz. Estimations suggest that one can benefit from parametric gain based on inherent nonlinearity of the Josephson junction and reduce the flux noise to 30 nΦ0Hz–1∕2 at 100 mK, which corresponds to 10.6 μBHz–1∕2 for a magnetic moment located at the center of the pickup loop.