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Journal of Applied Physics

Proximity effect bilayer nano superconducting quantum interference devices for millikelvin magnetometry

A. Blois, S. Rozhko, L. Hao, John C. Gallop, Edward J. Romans

Published Dec 18, 2013• 22 citations
Publisher

Abstract

Superconducting quantum interference devices (SQUIDs) incorporating thin film nanobridges as weak links have sensitivities approaching that required for single spin detection at 4.2 K. However, due to thermal hysteresis they are difficult to operate at much lower temperatures which hinder their application to many quantum measurements. To overcome this, we have developed nanoscale SQUIDs made from titanium-gold proximity bilayers. We show that their electrical properties are consistent with a theoretical model developed for heat flow in bilayers and demonstrate that they enable magnetic measurements to be made on a sample at system temperatures down to 60 mK.

DOI
10.1063/1.4843856

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Superconducting quantum interference devices (SQUIDs) incorporating thin film nanobridges as weak links have sensitivities approaching that required for single spin detection at 4.2 K. However, due to thermal hysteresis they are difficult to operate at much lower temperatures which hinder their application to many quantum measurements. To overcome this, we have developed nanoscale SQUIDs made from titanium-gold proximity bilayers. We show that their electrical properties are consistent with a theoretical model developed for heat flow in bilayers and demonstrate that they enable magnetic measurements to be made on a sample at system temperatures down to 60 mK.
Nanoscale Superconducting QUantum Interference Devices (SQUIDs) have spin sensitivities approaching that required to detect the flip of a single spin in close proximity. There is considerable interest in developing them for measuring the properties of small spin populations in magnetic systems. It is desirable that such measurements can be realised at sub-kelvin temperatures thereby allowing the study of magnetic systems that undergo phase changes at such temperatures. However, most nanoscale SQUIDs use nanobridges as the Josephson elements which limits the operating range to temperatures close to the transition temperature of the device. Well below this, the current-phase relation can become non-sinusoidal, and hot spots arising from the large critical current lead to hysteretic I-V characteristics. To extend the temperature range downwards, we have developed a range of nanoSQUIDs fabricated from alternative materials with lower transition temperatures including Ti/Au and Al/Ag bilayers patterned using lift-off and e-beam lithography (EBL). We report on their I-V characteristics, noise performance and behaviour in applied magnetic fields at temperatures down to 60 mK. We discuss theoretical analysis and computer modelling of the heat flow in the nanobridge structure, and consider the effects of bank geometry and kinetic inductance on the overall device performance. Finally, we present measurements of several magnetic systems: control lines, superconducting islands and ground planes and discuss the feasibility of magnetic measurements of novel materials of interest, including the heterointerface between lanthanium aluminate and strontium titanate.
We study operation of a superconducting quantum interference devices (SQUIDs) based on a new bilayer material. They can be used for the ultra-sensitive detection of magnetic momentum at temperatures down to milliKelvin range. Typically, thermal origin hysteresis of the symmetric SQUID current-voltage curves limits operating temperatures to T>0.6Tc. We used a new bilayer material for SQUID fabrication, namely proximity-coupled superconductor/normal-metal (S/N) bilayers (aluminum 25 nm/platinum 5 nm). Because of the 5 nm Pt-layer, Al/Pt devices show nonhysteretic behavior in a broad temperature range from 20 mK to 0.8 K. Furthermore, the Al/Pt bilayer devices demonstrate an order of magnitude lower critical current compared to the Al devices, which decreases the screening parameter (βL) and improves the modulation depth of the critical current by magnetic flux. Operation at lower temperatures reduces thermal noise and increases the SQUID magnetic field resolution. Moreover, we expect strong decrease of two-level fluctuators on the surface of aluminum due to Pt-layer oxidation protection and hence significant reduction of the 1/f noise. Optimized geometry of Al/Pt symmetric SQUIDs is promising for the detection of single-electron spin flip.
Nano-Superconducting Quantum Interference Devices (nano-SQUIDs) are usually fabricated from a single layer of either Nb or Al. We describe here a simple method for fabricating suspended nano-bridges in Nb/Al thin-film bilayers. We use these suspended bridges, which act as Josephson weak links, to fabricate nano-SQUIDs which show critical current oscillations at temperatures up to 1.5 K and magnetic flux densities up to over 20 mT. These nano-SQUIDs exhibit flux modulation depths intermediate between all-Al and all-Nb devices, with some of the desirable characteristics of both. The suspended geometry is attractive for magnetic single nanoparticle measurements.
Nanoscale superconducting quantum interference devices (nano-SQUIDS) where the weak links are made from nanobridges, i.e., nanobridge SQUIDs (NBSs), are one of the most sensitive magnetometers for nanoscale magnetometry. Because of very strong nonlinearity in the nanobridge-electrode joints, the applied magnetic flux (${\mathrm{\ensuremath{\Phi}}}_{a}$)--critical current (Ic{I}_{c}Ic​) characteristics of NBSs differ very significantly from conventional tunnel-junction SQUIDs, especially when the nanobridges are long and/or the screening parameter is large. However, in most of the theoretical descriptions, NBSs have been treated as the conventional tunnel-junction SQUIDs, which are based on the dc Josephson effect. Here, I present a model demonstrating that for long nanobridges and/or large screening parameters the ${I}_{c}({\mathrm{\ensuremath{\Phi}}}_{a})$ of a NBS can be explained by merely considering the fluxoid quantization in the NBS loop and the energy of the NBS; it is not necessary to take the Josephson effect into consideration. I also demonstrate that using the model, one can derive useful expressions such as the modulation depth and transfer function. I discuss the role of the kinetic inductance fraction ($\ensuremath{\kappa}$) in determining ${I}_{c}({\mathrm{\ensuremath{\Phi}}}_{a})$. I compare the predictions of the present model with the experimental data already published by several groups.
SQUIDs (superconducting quantum interference devices) have been in use for more than half a century and constitute one of the first macroscopic quantum devices. SQUIDs operating at millikelvin temperatures can act as qubits for quantum computers and the recent reports of more than 50 qubit circuits indicate how far the technology has developed. In this talk, the author will describe two other applications of SQUIDs as quantum detectors, focusing on single spin and single photon energy resolving detection. Most superconducting devices rely on tri-layer Josephson tunnel junctions which are not easily scalable to the nanoscale. We have developed a Josephson junction fabrication method, based on electron beam lithography or focused ion beam milling of a single thin film of superconductor (Nb generally) which can provide sizes down to 50 nm. These devices are particularly relevant for two main applications in quantum technology and metrology. First, by shrinking the size of the SQUID loop and the junctions to around 200 nm, the sensitivity of the SQUID for magnetization measurements is improved to the level where a single electron spin flip may be detected. This is possible at the relatively elevated temperature of 4K.  We are working with Surrey University to implant single magnetic ions within the SQUID loop to provide a platform to test this combination as the basis for a new form of qubit operating at higher temperatures than the conventional Transmon superconducting devices. A second SQUID based detector which we are developing is an inductive transition edge sensor device (ISTED) for energy resolving measurements of single photons. This is based on the development of conventional transition edge sensors where we detect the change of the penetration depth of a small thin film of superconductor when it absorbs a photon. In this way, a major source of noise in conventional TES may be avoided since the absorber remains in the superconducting state at all times. In this way we have demonstrated single photon detection at 633 nm with 0.1eV resolution at operating temperature of 7.5K.
Abstract SQUIDs (Superconducting Quantum Interference Devices) are macroscopic quantum devices capable of detecting and measuring a wide variety of physical parameters with unprecedented sensitivity. SQUIDs based on nanobridge weak links have shown increasing promise for quantum information and quantum sensing applications such as single spin detection. Focussed ion beam etched nanobridges have properties which can enhance nanoSQUID device performance but are often limited in terms of their non-hysteretic operating temperature range. Here we describe measurements of FIB-milled nanobridges, as single weak links or in nanoSQUIDs, made using either Ga, Xe or Ne ion beam sources. Their properties as a function of temperature, bias current, magnetic field and microwave power are measured and modelled according to a range of superconductivity models, as a means for improved understanding of the associated nanobridge parameters. We further propose techniques to extend the non-hysteretic operating temperature range of the devices.