The radiative lifetime of
1s2s3S1 Li+ ions has been measured by a comparison of the count rate of spontaneous decay photons (210 \AA{}) to a laser-induced fluorescence signal proportional to the total number of metastable ions. The ions were confined in a rf-quadrupole trap, and the fluorescence signal used was the intercombination transition
1s2p3P1 to $1{s}^{2}^{1}S_{0}$ at 202 \AA{}. The
3P1 state was populated from
3S1 by absorption of laser photons at 5485 \AA{}. The result is ${\ensuremath{\tau}}_{r}=58.6\ifmmode\pm\else\textpm\fi{}12.9$ sec (95% confidence level); theory predicts ${\ensuremath{\tau}}_{r}=49.1$ sec.