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IEEE Transactions on Applied Superconductivity

Study of Low-Frequency Noise Performance of Nanobridge-Based SQUIDs in External Magnetic Fields

S. Rozhko, T. Hino, A. Blois, L. Hao, John C. Gallop, David Cox, Edward J. Romans

Published Dec 11, 2012• 6 citations
Publisher

Abstract

We report on the low-frequency noise performance of niobium dc superconducting quantum interference devices (SQUIDs), which contain nanobridges fabricated by focused ion beam lithography as the active Josephson elements. The devices have feature sizes down to 70 nm. We have measured devices of different loop sizes in two readout configurations: nano-scale loop sizes in small signal mode using a series SQUID array as a low-temperature pre-amplifier, and larger micron-scale loop sizes in a conventional flux-locked loop. We investigate the different contributions to the low frequency noise and report on electrical measurements made in applied magnetic fields of up to 0.5 T (in-plane) and 0.1 T (perpendicular to the plane) at operating temperatures around 7 K. We compare the measurements with the existing theories of noise in a dc SQUID.

DOI
10.1109/tasc.2012.2233537

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We report on the low-frequency noise performance of niobium dc superconducting quantum interference devices (SQUIDs), which contain nanobridges fabricated by focused ion beam lithography as the active Josephson elements. The devices have feature sizes down to 70 nm. We have measured devices of different loop sizes in two readout configurations: nano-scale loop sizes in small signal mode using a series SQUID array as a low-temperature pre-amplifier, and larger micron-scale loop sizes in a conventional flux-locked loop. We investigate the different contributions to the low frequency noise and report on electrical measurements made in applied magnetic fields of up to 0.5 T (in-plane) and 0.1 T (perpendicular to the plane) at operating temperatures around 7 K. We compare the measurements with the existing theories of noise in a dc SQUID.
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An integrated magnetic nanosensor based on a niobium dc SQUID (superconducting quantum interference device) for nanoscale applications is presented. The sensor, having a washer shape with a hole of 200 nm and two Josephson-Dayem nanobridges of 80 nm × 100 nm, consists of a Nb(30 nm)/Al(30 nm) bilayer patterned by electron beam lithography (EBL) and shaped by lift-off and reactive ion etch (RIE) processes. The presence of the niobium coils, integrated on-chip and tightly coupled to the SQUID, allows us to easily excite the sensor in order to get the voltage-flux characteristics and to flux bias the SQUID at its optimal point. The measurements were performed at liquid helium temperature. A voltage swing of 75 µV and a maximum voltage-flux transfer coefficient (responsivity) as high as 1 mV/Φ(0) were directly measured from the voltage-flux characteristic. The noise measurements were performed in open loop mode, biasing the SQUID with a dc magnetic flux at its maximum responsivity point and using direct-coupled low-noise readout electronics. A white magnetic flux noise spectral density as low as 2.5 μΦ(0) Hz(-1/2) was achieved, corresponding to a magnetization or spin sensitivity in units of the Bohr magneton of 100 spin Hz(-1/2). Possible applications of this nanosensor can be envisaged in magnetic detection of nanoparticles and small clusters of atoms and molecules, in the measurement of nanoobject magnetization, and in quantum computing.
DC SQUIDs with outer loop size ∼10 μmx 10 μm have been fabricated with nanobridge Josephson junctions in thin Niobium films (25, 100 and 200 nm) using either electron beam or focused ion beam techniques. Such SQUIDs are ideally suited to incorporate into the centre strip of a superconducting coplanar waveguide. The current-voltage characteristics and magnetic field modulation of the SQUIDs are compared for the two methods. The temperature dependence of the critical current is quite linear for the e-beam devices whilst the focused ion beam devices fit an exponential. Here we also investigate trimming methods to reduce the critical currents of the nanojunctions fabricated in the thicker films, in order to improve the SQUID parameters at lower temperatures.
We report on the design, the fabrication and the performance of an integrated magnetic nano-sensor based on niobium dc-SQUID (Superconducting QUantum Interference Device) for nanoscale applications is presented. The nano-sensors are based on nanometric niobium constrictions (Dayem bridges) inserted in a square loop having a side length of 200 nm. Measurements of voltage-flux characteristic, flux to voltage transfer factor and noise performances are reported. In small signal mode, the sensors have shown a magnetic flux noise spectral density of 1.5 μΦ 0 /Hz 1/2 corresponding to a spin sensitivity in unit of Bohr magneton of 60 spin/Hz 1/2 . Supercurrent decay measurements of these devices are also reported. Such measurements provide useful information for applications which employ the SQUID as a trigger where the sensor works on the zero voltage state. The experimental data, have shown an intrinsic current fluctuation less than 0.2% of the critical current at liquid helium temperature, corresponding to an intrinsic sensor magnetic flux resolution of a few mΦ 0 . In view of the nano-SQUID employments in the detection of small spin populations, the authors calculated the spin sensitivity and the magnetic response relative to the single spin, as a function of its position within the SQUID hole. The results show that the SQUID response depends strongly on the spin position.
Superconducting QUantum Interference Devices (SQUIDs) based on nanobridge junctions have shown increasing promise for single particle detection. This paper describes the development of the fabrication of improved and reproducible nanobridge junctions fabricated by focused ion beam (FIB) milling from niobium thin films. Although the very low noise properties of nanobridge SQUIDs are well known, the nature of the milling process is little understood at the level of local superconducting properties. In this paper, we report the results for nanobridge Josephson devices and SQUIDs, which we believe are the first to be made by Xenon (Xe) FIB milling. Temperature-dependent current-voltage behavior, microwave-induced Shapiro steps, and SQUID response to magnetic fields have been measured. We make preliminary comparisons with nominally identical devices milled from Nb thin films using either Xe or Ga ions.