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arXiv:2401.03266

Millikelvin confocal microscope with free-space access and high-frequency electrical control

Thomas Descamps, Feng Liu, Tobias Hangleiter, Sebastian Kindel, Beata E. Kardynal, Hendrik Bluhm

Published Jan 6, 2024• 0 citations
arXivHTMLPDF

Abstract

Cryogenic confocal microscopy is a powerful method for studying solid state quantum devices such as single photon sources and optically controlled qubits. While the vast majority of such studies have been conducted at temperatures of a few Kelvin, experiments involving fragile quantum effects often require lower operating temperatures. To also allow for electrical dynamic control, microwave connectivity is required. For polarization-sensitive studies, free space optical access is advantageous compared to fiber coupling. Here we present a confocal microscope in a dilution refrigerator providing all the above features at temperatures below 100 mK. The installed high frequency cabling meets the requirements for state of the art spin qubit experiments. As another unique advantage of our system, the sample fitting inside a large puck can be exchanged while keeping the cryostat cold with minimal realignment. Assessing the performance of the instrument, we demonstrate confocal imaging, sub-nanosecond modulation of the emission wavelength of a suitable sample and an electron temperature of 76 mK. While the instrument was constructed primarily with the development of optical interfaces to electrically controlled qubits in mind, it can be used for many experiments involving quantum transport, solid state quantum optics and microwave-optical transducers.

DOI
10.48550/arxiv.2401.03266

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Cryogenic confocal microscopy is a powerful method for studying solid state quantum devices such as single photon sources and optically controlled qubits. While the vast majority of such studies have been conducted at temperatures of a few Kelvin, experiments involving fragile quantum effects often require lower operating temperatures. To also allow for electrical dynamic control, microwave connectivity is required. For polarization-sensitive studies, free space optical access is advantageous compared to fiber coupling. Here we present a confocal microscope in a dilution refrigerator providing all the above features at temperatures below 100 mK. The installed high frequency cabling meets the requirements for state of the art spin qubit experiments. As another unique advantage of our system, the sample fitting inside a large puck can be exchanged while keeping the cryostat cold with minimal realignment. Assessing the performance of the instrument, we demonstrate confocal imaging, sub-nanosecond modulation of the emission wavelength of a suitable sample and an electron temperature of 76 mK. While the instrument was constructed primarily with the development of optical interfaces to electrically controlled qubits in mind, it can be used for many experiments involving quantum transport, solid state quantum optics and microwave-optical transducers.
Cryogenic confocal microscopy is a powerful method for studying solid state quantum devices such as single photon sources and optically controlled qubits. While the vast majority of such studies have been conducted at temperatures of a few Kelvin, experiments involving fragile quantum effects often require lower operating temperatures. To also allow for electrical dynamic control, microwave connectivity is required. For polarization-sensitive studies, free space optical access is advantageous compared to fiber coupling. Here we present a confocal microscope in a dilution refrigerator providing all the above features at temperatures below 100 mK. The installed high frequency cabling meets the requirements for state-of-the-art spin qubit experiments. As another unique advantage of our system, the sample fitting inside a large puck can be exchanged while keeping the cryostat cold with minimal realignment. Assessing the performance of the instrument, we demonstrate confocal imaging, sub-nanosecond modulation of the emission wavelength of a suitable sample, and an electron temperature of 76 mK. While the instrument was constructed primarily with the development of optical interfaces to electrically controlled qubits in mind, it can be used for many experiments involving quantum transport, solid state quantum optics, and microwave-optical transducers.
Nanophotonic light–matter interfaces hold great promise for quantum technologies. Enhancing local electromagnetic fields, they enable highly efficient detectors, can help realize optically connected processors, or serve as quantum repeaters. In-situ fiber-coupling at sub-Kelvin temperatures, as required for testing and development of new devices, proves challenging as suitable cryogenic microscopes are not readily available. Here, we report on a robust and versatile confocal imaging system integrated in a dilution refrigerator, enabling high-resolution visualization of nanophotonic structures on a transparent diamond substrate. Our imaging system achieves a resolution of 1.1 μm and a field-of-view of 2.5 mm. The system requires no movable parts at cryogenic temperatures and features a large working distance, thereby allowing optical and microwave probe access, as well as direct anchoring of temperature sensitive samples to a cold finger setup, needed for applications with high thermal load. This system facilitates the development of scalable, integrated quantum optics technology, an imperative for research on large scale quantum networks.
We present the design and operation of a fiber-based cryogenic confocal microscope. It is designed as a compact cold-finger that fits inside the bore of a superconducting magnet, and which is a modular unit that can be easily swapped between use in a dilution refrigerator and other cryostats. We aimed at application in quantum optical experiments with electron spins in semiconductors and the design has been optimized for driving with and detection of optical fields with well-defined polarizations. This was implemented with optical access via a polarization maintaining fiber together with Voigt geometry at the cold finger, which circumvents Faraday rotations in the optical components in high magnetic fields. Our unit is versatile for use in experiments that measure photoluminescence, reflection, or transmission, as we demonstrate with a quantum optical experiment with an ensemble of donor-bound electrons in a thin GaAs film.
Spin quantum bits (qubits) in semiconductor silicon quantum dots are one of the most promising candidates for large-scale quantum processor units, since they potentially have higher scalability through advanced semiconductor integration technologies. However, spin qubits require many control signals such as bias voltages, pulses and high-frequency microwaves, which is a major barrier to scale-up of qubits. In current small-scale quantum computer setup, the spin qubits inside the 100 mK cold finger of dilution refrigerator have been controlled by external room temperature instruments via long cables as shown in the left image of Fig. 1. This setup, consisting of fully analog signal transmission between qubits and external instruments, degrades the signal integrity and causes heat injection via cables, making it unsuitable for scalable qubits. Thus, cryogenic CMOS controller solutions have been widely developed to control the qubits from inside the refrigerator by installing the signal generation circuits on 4 K plate as depicted in the middle image of Fig. 1 [1]. This allows for the connection from the external devices to the refrigerator to be made with only digital wirings, which reduces number of cables and heat inflow. However, the distance between the 4 K plate and the 100 mK cold finger is still more than 2 m, degrading the integrity of wideband signals such as pulses.
Rapid thermal cycling is a central bottleneck in the development of superconducting quantum devices: conventional dilution refrigerators require cooldowns of a day or more and substantial cryogenic infrastructure, which throttles the fabricate-measure-redesign loop. We present an ultracompact dilution refrigerator (3 kg in mass and 100 mm in diameter) that completes a full cooldown-warm-up cycle to a base temperature of 70 mK in 1.2 hours when unloaded, and in 2.1 hours when fully equipped with the microwave wiring required for qubit measurements, while delivering 20 microW of cooling power at 100 mK. We validate the platform through a complete characterization of a two-fluxonium device: we extract the full circuit Hamiltonian by two-tone spectroscopy, measure energy-relaxation and coherence times, and benchmark single-qubit control. Although the relaxation time is limited by the base temperature of the system, we reach a single-qubit gate fidelity of up to 99%, at the coherence limit set by our operating temperature. These results demonstrate that compact, fast-cycling dilution refrigeration can support state-of-the-art quantum-device characterization without sacrificing measurement quality, offering a practical route to high-throughput quantum-hardware development.
Accessibility to the microkelvin temperature regime is important for quantum technology research. Cryogen-free dilution refrigerators opened up the millikelvin temperature range, but the perception is that ultralow temperatures are difficult to reach and require specialist infrastructure. The authors report the design of a microkelvin platform based on a nuclear-demagnetization stage, engineered and optimized for operation on a cryogen-free dilution refrigerator. The study demonstrates temperatures as low as 395 $\ensuremath{\mu}$K, and a protocol that enables experiments operated below 1 mK for 95% of the time, providing an efficient cryogen-free microkelvin environment for a wide range of applications.