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Applied Physics Letters

Performance of 3 cm3 ion trap vacuum package sealed for 10 years

Daniel Thrasher, Peter D. D. Schwindt

Published Mar 1, 2025• 3 citations
Publisher

Abstract

Miniature atomic clocks based on the interrogation of the ground state hyperfine splitting of buffer gas cooled ions confined in radio frequency Paul traps have shown great promise as high precision prototype clocks. We report on the performance of two miniature ion trap vacuum packages after being sealed for as much as 10 years. We find the lifetime of the ions within the trap has increased over time for both traps and can be as long as 50 days. We form two clocks using the two traps and compare their relative frequency instability one with another to demonstrate a short-term instability of 5×10−13τ−1/2 integrating down to 1×10−14 after 2 ks of integration. The trapped ion lifetime and clock instability demonstrated by these miniature devices despite only being passively pumped for many years represents a critical advance toward their proliferation in the clock community.

DOI
10.1063/5.0243517

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Miniature atomic clocks based on the interrogation of the ground state hyperfine splitting of buffer gas cooled ions confined in radio frequency Paul traps have shown great promise as high precision prototype clocks. We report on the performance of two miniature ion trap vacuum packages after being sealed for as much as 10 years. We find the lifetime of the ions within the trap has increased over time for both traps and can be as long as 50 days. We form two clocks using the two traps and compare their relative frequency instability one with another to demonstrate a short-term instability of 5×10−13τ−1/2 integrating down to 1×10−14 after 2 ks of integration. The trapped ion lifetime and clock instability demonstrated by these miniature devices despite only being passively pumped for many years represents a critical advance toward their proliferation in the clock community.
We describe the development and frequency instability measurements of a highly miniaturized, buffer gas cooled, trapped-ion atomic clock. The clock utilizes the 12.6 GHz hyperfine transition of the171Yb+ion. A custom-built 3 cm3vacuum package containing the ion trap is integrated with other key elements of the atomic frequency standard, including a photo multiplier tube, miniaturized laser sources at 369 nm and 935 nm, a local oscillator, and control electronics. With the clock physics package assembled on a 10 cm × 15 cm breadboard, the long-term fractional frequency instability was measured to be 6 × 10-14at 25 days of integration. Later, the clock physics package was further miniaturized, and the frequency instability was measured to be 2 × 10-11/τ1/2at integration times up to 10,000 s.
We report on the development of a highly miniaturized vacuum package for use in an atomic clock utilizing trapped ytterbium-171 ions. The vacuum package is approximately 1 cm(3) in size and contains a linear quadrupole RF Paul ion trap, miniature neutral Yb sources, and a non-evaporable getter pump. We describe the fabrication process for making the Yb sources and assembling the vacuum package. To prepare the vacuum package for ion trapping, it was evacuated, baked at a high temperature, and then back filled with a helium buffer gas. Once appropriate vacuum conditions were achieved in the package, it was sealed with a copper pinch-off and was subsequently pumped only by the non-evaporable getter. We demonstrated ion trapping in this vacuum package and the operation of an atomic clock, stabilizing a local oscillator to the 12.6 GHz hyperfine transition of (171)Y b(+). The fractional frequency stability of the clock was measured to be 2 × 10(-11)/τ(1/2).
In this paper, we report our recent effort on developing a micro mercury trapped ion atomic clock. In particular, we present preliminary results of a mercury-ion clock using a 15-cc vacuum trap tube. The mercury-ion clock can achieve a short-term fractional frequency instability of 1.5 ×10!12τ!1/2and reach a fractional frequency instability of 3 ×10!14after averaging for an hour. The clock can remain at the 10!14fractional frequency instability level up to several hours. Furthermore, the sealed 15-cc vacuum tube has demonstrated a very long ion lifetime of over two hundred days. We also investigated the mercury vapor density inside the vacuum trap tube by measuring the coherence time of the microwave clock transition.
We have recently completed a breadboard ion-clock physics package based on Hg ions shuttled between a quadrupole and a 16-pole rf trap. With this architecture we have demonstrated short-term stability ~1-2x10-13 at 1 second, averaging to 10-15 at 1 day. This development shows that H-maser quality stabilities can be produced in a small clock package, comparable in size to an ultra-stable quartz oscillator required for holding 1-2x10-13 at 1 second. This performance was obtained in a sealed vacuum configuration where only a getter pump was used to maintain vacuum. The vacuum tube containing the traps has now been under sealed vacuum conditions for nearly two years with no measurable degradation of ion trapping lifetimes or clock short-term performance. We have fabricated the vacuum tube, ion trap and UV windows from materials that will allow a ~ 400°C tube bake-out to prepare for tube seal-off. This approach to the vacuum follows the methods used in flight vacuum tube electronics, such as flight TWTA's where tube operation lifetime and shelf life of up to 15 years is achieved. We use neon as a buffer gas with 2-3 times less pressure induced frequency pulling than helium and, being heavier, negligible diffusion losses will occur over the operation lifetime.
We report a demonstration of a very small microwave atomic clock using the 12.6 GHz hyperfine transition of the trapped 171Yb ions inside a miniature, completely sealed-off 3 cm3 ion-trap vacuum package. In the ion clock system, all of the components are highly miniaturized with low power consumption except the 369 nm optical pumping laser still under development for miniaturization. The entire clock, including the control electronics, consumes <300 mW. The fractional frequency instability of the miniature Yb+ clock reaches the 10−14 range after a few days of integration.