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Review of Scientific Instruments

A highly miniaturized vacuum package for a trapped ion atomic clock

Peter D. D. Schwindt, Yuan‐Yu Jau, Heather L. Partner, Adrian L. Casias, Adrian R. Wagner, Matthew W. Moorman, Ronald P. Manginell, James R. Kellogg, John D. Prestage

Published May 1, 2016• 54 citations
Publisher

Abstract

We report on the development of a highly miniaturized vacuum package for use in an atomic clock utilizing trapped ytterbium-171 ions. The vacuum package is approximately 1 cm(3) in size and contains a linear quadrupole RF Paul ion trap, miniature neutral Yb sources, and a non-evaporable getter pump. We describe the fabrication process for making the Yb sources and assembling the vacuum package. To prepare the vacuum package for ion trapping, it was evacuated, baked at a high temperature, and then back filled with a helium buffer gas. Once appropriate vacuum conditions were achieved in the package, it was sealed with a copper pinch-off and was subsequently pumped only by the non-evaporable getter. We demonstrated ion trapping in this vacuum package and the operation of an atomic clock, stabilizing a local oscillator to the 12.6 GHz hyperfine transition of (171)Y b(+). The fractional frequency stability of the clock was measured to be 2 × 10(-11)/τ(1/2).

DOI
10.1063/1.4948739

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We report on the development of a highly miniaturized vacuum package for use in an atomic clock utilizing trapped ytterbium-171 ions. The vacuum package is approximately 1 cm(3) in size and contains a linear quadrupole RF Paul ion trap, miniature neutral Yb sources, and a non-evaporable getter pump. We describe the fabrication process for making the Yb sources and assembling the vacuum package. To prepare the vacuum package for ion trapping, it was evacuated, baked at a high temperature, and then back filled with a helium buffer gas. Once appropriate vacuum conditions were achieved in the package, it was sealed with a copper pinch-off and was subsequently pumped only by the non-evaporable getter. We demonstrated ion trapping in this vacuum package and the operation of an atomic clock, stabilizing a local oscillator to the 12.6 GHz hyperfine transition of (171)Y b(+). The fractional frequency stability of the clock was measured to be 2 × 10(-11)/τ(1/2).
We report the development of a low-power, miniature Yb-171 ion clock at Sandia National Laboratories. This work is funded by the DARPA micro Position, Navigation, and Timing program under the Integrated Micro Primary Atomic Clock Technology (IMPACT) project. The ultimate goal is to develop a frequency standard that has frequency stability comparable to a commercial Cs beam standard, but with 100 to 1000 times smaller size and power consumption. The Yb-171 ion has a microwave clock traItem MIN :YXB4-01335-A112nsition at 12.6 GHz, and the natural linewidth of the clock resonance is expected to be less than 10-3Hz, which leads to a very high-Q clock resonance. An atomic clock using trapped ions is an excellent candidate for miniaturization because ions are well isolated from the environment independently of the size of the trap. Compared to optical traps for neutral atoms, the trapping depth of RF traps for ions is usually several orders of magnitude deeper. Therefore, the requirement for the vacuum level is more forgiving. We have successfully developed miniature ion-trap vacuum packages as shown in Fig. 1. Usually, a few microTorr of He buffer gas is introduced into each of our miniature ion-trap vacuum packages, which are sealed and passively pumped by non-evaporable getters. Using a sealed 3 cc ion-trap package, we were able to demonstrate long-term clock operation, with the stability reaching the 10-14range after a few days of integration [1].
We describe the development and frequency instability measurements of a highly miniaturized, buffer gas cooled, trapped-ion atomic clock. The clock utilizes the 12.6 GHz hyperfine transition of the171Yb+ion. A custom-built 3 cm3vacuum package containing the ion trap is integrated with other key elements of the atomic frequency standard, including a photo multiplier tube, miniaturized laser sources at 369 nm and 935 nm, a local oscillator, and control electronics. With the clock physics package assembled on a 10 cm × 15 cm breadboard, the long-term fractional frequency instability was measured to be 6 × 10-14at 25 days of integration. Later, the clock physics package was further miniaturized, and the frequency instability was measured to be 2 × 10-11/τ1/2at integration times up to 10,000 s.
This dissertation reports on the development of a low-power, high-stability miniature atomic frequency standard based on 171Yb+ ions. The ions are buffer-gas cooled and held in a linear quadrupole trap that is integrated into a sealed, getter-pumped vacuum package, and interrogated on the 12.6 GHz hyperfine transition. We hope to achieve a long-term fractional frequency stability of 10^-14 with a miniature clock that consumes only 50 mW of power and occupies a volume of 5 cm^3. I discuss our progress over several years of work on this project. We began by building a conventional tabletop clock to use as a test bed while developing several designs of miniature ion-trap vacuum packages, while also developing techniques for various aspects of the clock operation, including ion loading, laser and magnetic field stabilization, and a low power ion trap drive. The ion traps were modeled using boundary element software to assist with the design and parameter optimization of new trap geometries. We expect a novel trap geometry that uses a material new to ion traps to lead to an exceptionally small ion trap vacuum package in the next phase of the project. To achieve the long-term stability required, we have also considered the sensitivity of the clock frequency to magnetic fields. A study of the motion of the individual ions in a room-temperature cloud in the trap was performed with the purpose of understanding the effect of both spatially varying and constant magnetic fields on the clock resonance and therefore the operation of the clock. These effects were studied experimentally and theoretically for several traps. In summary, this dissertation is a contribution to the design, development, and testing of a 171Yb+ ion cloud frequency standard and related techniques, including analyses of trap geometries and parameters, modeling of the ion motion, and the practical operation of the clock.
We report a demonstration of a very small microwave atomic clock using the 12.6 GHz hyperfine transition of the trapped 171Yb ions inside a miniature, completely sealed-off 3 cm3 ion-trap vacuum package. In the ion clock system, all of the components are highly miniaturized with low power consumption except the 369 nm optical pumping laser still under development for miniaturization. The entire clock, including the control electronics, consumes <300 mW. The fractional frequency instability of the miniature Yb+ clock reaches the 10−14 range after a few days of integration.
We have recently completed a breadboard ion-clock physics package based on Hg ions shuttled between a quadrupole and a 16-pole rf trap. With this architecture we have demonstrated short-term stability ~1-2x10-13 at 1 second, averaging to 10-15 at 1 day. This development shows that H-maser quality stabilities can be produced in a small clock package, comparable in size to an ultra-stable quartz oscillator required for holding 1-2x10-13 at 1 second. This performance was obtained in a sealed vacuum configuration where only a getter pump was used to maintain vacuum. The vacuum tube containing the traps has now been under sealed vacuum conditions for nearly two years with no measurable degradation of ion trapping lifetimes or clock short-term performance. We have fabricated the vacuum tube, ion trap and UV windows from materials that will allow a ~ 400°C tube bake-out to prepare for tube seal-off. This approach to the vacuum follows the methods used in flight vacuum tube electronics, such as flight TWTA's where tube operation lifetime and shelf life of up to 15 years is achieved. We use neon as a buffer gas with 2-3 times less pressure induced frequency pulling than helium and, being heavier, negligible diffusion losses will occur over the operation lifetime.
We have recently completed a breadboard ion-clock physics package based on Hg ions shuttled between a quadrupole and a 16-pole rf trap. With this architecture we have demonstrated short-term stability ~1-2times10-13at 1 second, averaging to 10-15at 1 day. This development shows that H-maser quality stabilities can be produced in a small clock package, comparable in size to an ultra-stable quartz oscillator required for holding 1-2times10-13second. This performance was obtained in a sealed vacuum configuration where only a getter pump was used to maintain vacuum. The vacuum tube containing the traps has now been under sealed vacuum conditions for nearly two years with no measurable degradation of ion trapping lifetimes or clock short-term performance. We have fabricated the vacuum tube, ion trap and UV windows from materials that will allow a ~400degC tube bake-out to prepare for tube seal-off. This approach to the vacuum follows the methods used in flight vacuum tube electronics, such as flight TWTA's where tube operation lifetime and shelf life of up to 15 years is achieved. We use neon as a buffer gas with 2-3 times less pressure induced frequency pulling than helium and, being heavier, negligible diffusion losses will occur over the operation lifetime.