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International Conference on Optical and Photonic Engineering (icOPEN)

Improving the sensitivity of diamond NV center ensemble magnetometer based on microsphere

Yangyang Zhou, Jiong Tang, Bingxu Ma, Jian Qiu

Published Feb 5, 2025• 0 citations
Publisher

Abstract

Diamond nitrogen-vacancy (NV) center ensemble magnetometer is a novel solid quantum magnetometer with high sensitivity and high spatial resolution, which can be used at normal temperature and pressure. However, the low fluorescence collection efficiency of the magnetometer in confocal optical system hinders further improvement in sensitivity. To solve the problem, based on silica microspheres, we propose a method to enhance the excitation and collection efficiency of NV center ensemble in massive diamond. Experimental results show, compared with the NV diamond magnetometer without microspheres, the photon collection efficiency of NV diamond magnetometer coated with a layer of microspheres is increased by 110%. Thus, the sensitivity of the NV center magnetometer is increased by 4 times to 5.3μT/√Hz.

DOI
10.1117/12.3057419

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IntechOpen eBooks•Feb 8, 2021•1 citation
Diamond nitrogen-vacancy (NV) center ensemble magnetometer is a novel solid quantum magnetometer with high sensitivity and high spatial resolution, which can be used at normal temperature and pressure. However, the low fluorescence collection efficiency of the magnetometer in confocal optical system hinders further improvement in sensitivity. To solve the problem, based on silica microspheres, we propose a method to enhance the excitation and collection efficiency of NV center ensemble in massive diamond. Experimental results show, compared with the NV diamond magnetometer without microspheres, the photon collection efficiency of NV diamond magnetometer coated with a layer of microspheres is increased by 110%. Thus, the sensitivity of the NV center magnetometer is increased by 4 times to 5.3μT/√Hz.
Abstract The ensemble of nitrogen-vacancy (NV) centers in diamond allows for the potential realization of the sensitive magnetometers by leveraging their excellent spin properties. However, the NV-based magnetometers are limited by their experimental magnetic field sensitivity owing to its inefficient photon collection. Moreover, they are a disadvantage to the reduced spatial resolution and excessive excitation power. To overcome these issues, we propose a ultra-sensitive diamond magnetometer based on nanocavities. The device structure can attain a high collective efficiency and enhance the photon emission intensity of the NV ensemble. This device can allow the efficient photon collection even when considering the positional distribution of the NV centers. Our theoretical analysis indicates that the minimum expected sensitivity is 60 fT/ H z . The proposed design can achieve a volume-normalized sensitivity of 0.92 aT/ H z c m − 3 along with the required power of 7 μW, both of which are superior to those of bulk diamond. The proposed approach offers a promising route towards highly sensitive and energy-efficient magnetometers.
Magnetometers using ensemble nitrogen-vacancy (NV) centers are promising because of their ability to measure magnetic fields in a variety of environments. To achieve high magnetic sensitivity, high collection efficiency of the fluorescence from the NV centers is essential. Due to the high refractive index of diamond, some of the photons from NVs diffuse to the sides of the diamond substrate[1]. In this study, we propose a method to improve the light collection efficiency by polishing the sides of the 12C-enriched chemical vapor deposition (CVD) growth diamond at an angle of 30 degrees and investigating the magnetic sensitivity.
Among quantum sensors, the single nitrogen-vacancy (NV) defect in diamond has the highest sensitivity-to-size factor. For instance, a single-NV spin when used as a magnetometer could achieve sensitivities of the order of nT/Hz, while the dimensions of the sensor are merely atomic in size. The sensitivity is limited only by the photon shot noise. One method to boost the magnetometer sensitivity to pico-tesla scales is to use many NV defect centers as an ensemble sensor [Phys. Rev. X5, 041001 (2015)PRXHAE2160-330810.1103/PhysRevX.5.041001]. However, during the absorption-emission (fluorescence) optical cycles, the NV centers transfer a portion of the irradiation laser energy into phonons and heat the diamond matrix. This results in unintended fluorescence decrease, spin resonance lines shifts, and fluctuations. Hence, the advantages gained by packing a high density of NV centers are significantly reduced. Here we investigate the heat generation of ensemble NV centers in micrometer-sized diamond under 532 nm laser irradiation and its effects pertaining to sensing applications. These investigations help us to find strategies that mitigate the detrimental effects of heating and yet permits the use of ensemble NV defects for improved metrology applications.
We report experimental studies of microsphere-enhanced fluorescence collection of nitrogen vacancy (NV) centers using silica microspheres with diameters ranging between 15 and 50 μm and employing 20× and 40× objectives with numerical aperture of 0.42 and 0.64, respectively. Photoluminescence-excitation saturation counts as high as 95 kHz have been observed. These studies show that due to the effective collimation of fluorescence by the microsphere, objectives with relatively low numerical aperture (NA) can be used without sacrificing collection enhancement, in agreement with a theoretical model based on Mie scattering. The large enhancement of fluorescence collection with relatively low NA objectives, which feature extralong working distance and are relatively inexpensive, can potentially enable wider use of NV-based quantum sensing in real world applications.
A magnetic field sensor based on a fiber-optic integrated probe at the center of a nitrogen vacancy (NV) is proposed and demonstrated. Fiber optics are utilized to replace all conventional spatial optics while efficiently enabling laser excitation and fluorescence collection from diamond. Optical models were developed to study the fluorescence collection efficiency of diamond. The fiber-coupled probe was simulated and its efficiency was improved to 3.062% compared to the 0.607% fluorescence coupling efficiency of the fiber. The optical probe magnetic resonance (ODMR) phenomenon was successfully observed and significantly improved the magnetic field sensitivity to 5.3 nT/Hz1/2, which proved the feasibility and performance compared with the conventional confocal NV-centered magnetometer.
In modern-day quantum metrology, quantum sensors are widely employed to detect weak magnetic fields or nanoscale signals. Quantum devices, exploiting quantum coherence, are inevitably connected to physical constants and can achieve accuracy, repeatability, and precision approaching fundamental limits. As a result, these sensors have shown utility in a wide range of research domains spanning both science and technology. A rapidly emerging quantum sensing platform employs atomic-scale defects in crystals. In particular, magnetometry using nitrogen-vacancy (NV) color centers in diamond has garnered increasing interest. NV systems possess a combination of remarkable properties, optical addressability, long coherence times, and biocompatibility. Sensors based on NV centers excel in spatial resolution and magnetic sensitivity. These diamond-based sensors promise comparable combination of high spatial resolution and magnetic sensitivity without cryogenic operation. The above properties of NV magnetometers promise increasingly integrated quantum measurement technology, as a result, they have been extensively developed with various protocols and find use in numerous applications spanning materials characterization, nuclear magnetic resonance (NMR), condensed matter physics, paleomagnetism, neuroscience and living systems biology, and industrial vector magnetometry. In this chapter, NV centers are explored for magnetic sensing in a number of contexts. In general, we introduce novel regimes for magnetic-field probes with NV ensembles. Specifically, NV centers are developed for sensitive magnetometers for applications where microwaves (MWs) are prohibitively invasive and operations need to be carried out under zero ambient magnetic field. The primary goal of our discussion is to improve the utility of these NV center-based magnetometers.