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Applied Physics Letters

NbTiN SQUID-on-tip fabricated by self-aligned deposition using reactive DC magnetron sputtering

N. Kokubo, B. Gerelkhuu

Published Jun 24, 2024• 1 citation
Publisher

Abstract

We fabricate superconducting quantum interference devices (SQUIDs) made of niobium-titanium nitride (NbTiN) thin films on the apex of sharp quartz capillaries. By incorporating reactive DC magnetron sputtering into the self-aligned deposition process for the SQUID-on-tip (SOT) fabrication, we produce NbTiN SOT devices with an effective diameter of ∼100 nm. The ø110 nm device has a superconducting transition temperature of 13.2 K, magnetic flux noise down to 0.7 μΦ0/Hz0.5 (4 K), and operating temperatures of 1.8–10 K. The developed technique enables the synthesis of nitride and other superconductors, thereby expanding the range of materials available for SOT devices.

DOI
10.1063/5.0211176

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We fabricate superconducting quantum interference devices (SQUIDs) made of niobium-titanium nitride (NbTiN) thin films on the apex of sharp quartz capillaries. By incorporating reactive DC magnetron sputtering into the self-aligned deposition process for the SQUID-on-tip (SOT) fabrication, we produce NbTiN SOT devices with an effective diameter of ∼100 nm. The ø110 nm device has a superconducting transition temperature of 13.2 K, magnetic flux noise down to 0.7 μΦ0/Hz0.5 (4 K), and operating temperatures of 1.8–10 K. The developed technique enables the synthesis of nitride and other superconductors, thereby expanding the range of materials available for SOT devices.
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Integration of superconducting devices on photonic platforms opens up a wide range of functionalities and applications. We report on NbTiN thin films deposited on SiO2, Si3N4, GaAs, LiNbO3, and AlN as well as on a monolayer of hexagonal boron nitride, using a universal reactive co-sputtering recipe. The morphology and the superconducting properties of the NbTiN thin films with a thickness of 10 nm were characterized by atomic force microscopy and electrical transport measurements. Superconducting strip photon detectors were fabricated using a design suitable for waveguide integration and compared in terms of their internal quantum efficiency and detection pulse kinetics. Our results show well-comparable performances for detectors integrated on different platforms, while also demonstrating that reactive co-sputter deposition of NbTiN at room temperature provides a robust method for realizing superconducting devices on various materials.
Electron-beam lithography and reactive ion etching have been used to fabricate thin-film Au/Nb bridges with widths ∼50 nm. The Au layer was used as both a mask for etching the Nb superconducting bridge and as a resistive shunt in the completed devices. Using these junctions, a dc superconducting quantum interference device (SQUID) design with a hole size of 200 nm×200 nm (nano-SQUID) has also been fabricated and characterized. A flux noise of approximately 7×10−6 Φ0/Hz1/2 at 4.2 K has been achieved, from which a calculated spin sensitivity of 250 spin/Hz1/2 is predicted.
We have fabricated superconducting quantum interference devices (dc SQUID’s) from thin films of the superconducting oxide YBa2Cu3Oy. The devices were made by first lithographically patterning an ion implant mask containing a 40 by 40 μm loop and two 17-μm-wide weak links over a ∼1-μm-thick oxide film. Ion implantation was then used to destroy the superconductivity in the film surrounding the device without actually removing material, resulting in a completely planar structure for the SQUID’s. The SQUID’s were operated in the temperature range from 4.2 to 68 K. The superconducting flux quantum was measured to be h/2e in these materials.
Abstract We propose the fabrication of micro-superconducting quantum interference devices via nano laser direct writing (NLDW). A 20 nm thick Nb film with a critical transition temperature of 9.2 K was deposited on a silicon substrate by sputtering, and nanopatterning was performed with NLDW. After optimizing parameters such as the laser pulse width and power, we investigated the electrical performance of SQUIDs by varying the laser power between 245 mW and 270 mW in 5 mW steps. Experimentally, the voltage–flux (V–Φ) characteristics of micro SQUIDs exhibited typical periodic modulation, confirming the Josephson effect and magnetic flux quantization effect based on the NLDW process. The noise spectral density measurements of SQUID fabricated with laser power of 265 mW achieved a white noise level of 3 μ Φ 0 /Hz 1 / 2 , demonstrating comparable flux noise sensitivity compared to electron beam and ion beam fabrication processes. Furthermore, the devices retained stable superconducting and electrical performance after 101 days, illustrating excellent long-term stability. To some extent, the NLDW shows the potential to perform micro-nanopatterning of superconducting devices efficiently and cost-effectively, as well as an avenue for conducting nanoscale thermal engineering on superconducting devices for basic science research.
Lithium niobate-on-insulator (LNOI) is an emerging photonic platform with high potential for scalable quantum information processing due to its strong second-order nonlinearity. However, little progress has been made in developing on-chip single-photon detectors on LNOI. Niobium tita nium nitride (NbTiN) superconducting nanowire single-photon detectors (SNSPDs) are a promising candidate for this application. In this work, we use DC reactive magnetron sputtering to grow high quality NbTiN thin films using an ultra-high vacuum deposition system with a base pressure lower than 2×10‾¹⁰ mbar. Enabled by the low concentration of background impurities in this system, we investigate the impact of substrate temperature during NbTiN growth. We achieve four nm thick superconducting films with a critical temperature (Tc) of 12.3 K grown at a substrate temperature of 825 K. We find that the NbTiN films grow in the (111) orientation and evolve from a porous pillar structure when grown at low temperatures to densely packed fibrous grains at higher temper atures. Furthermore, we demonstrate that the increased substrate temperature reduces the oxygen concentration in our films and improves the overall stoichiometry. In addition, we integrate these films with the LNOI platform and investigate the obtained interface quality. Lastly, we fabricate SNSPDs from the NbTiN film on LNOI and characterize the detector performance.