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Applied Physics Letters

Nuclear quadrupole resonance detected at 30 MHz with a dc superconducting quantum interference device

Claude Hilbert, John L. Clarke, Tycho Sleator, Erwin Louis Hahn

Published Sep 15, 1985• 60 citations
Publisher

Abstract

A dc superconducting quantum interference device is used as a tuned radio frequency amplifier at liquid helium temperatures to detect pulsed nuclear quadrupole resonance at ∼30 MHz. At a bath temperature of 4.2 K, a total system noise temperature of 6±1 K has been achieved, with a quality factor Q of 2500. A novel Q spoiler, consisting of a series array of Josephson tunnel junctions, reduces the ring-down time of the tuned circuit after each pulse. The minimum number of Bohr magnetons observable from a free precession signal after a single pulse is ∼2×1016 in a bandwidth of 10 kHz.

DOI
10.1063/1.96042

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Applied Physics Letters•Nov 29, 1999•37 citations
A dc superconducting quantum interference device is used as a tuned radio frequency amplifier at liquid helium temperatures to detect pulsed nuclear quadrupole resonance at ∼30 MHz. At a bath temperature of 4.2 K, a total system noise temperature of 6±1 K has been achieved, with a quality factor Q of 2500. A novel Q spoiler, consisting of a series array of Josephson tunnel junctions, reduces the ring-down time of the tuned circuit after each pulse. The minimum number of Bohr magnetons observable from a free precession signal after a single pulse is ∼2×1016 in a bandwidth of 10 kHz.
Sensitive radio-frequency (rf) amplifiers based on dc Superconducting QUantum Interface Devices (SQUIDS) are available for frequencies up to 200 MHz. At 4.2 K, the gain and noise temperature of a typical tuned amplifier are 18.6 +- 0.5 dB and 1.7 +- 0.5 K at 93 MHz. These amplifiers are being applied to a series of novel experiments on nuclear magnetic resonance (NMR) and nuclear quadrupole resonance (NQR). The high sensitivity of these amplifiers was demonstrated in the observation of ''nuclear spin noise'', the emission of photons by /sup 35/Cl nuclei in a state of zero polarization. In the more conventional experiments in which one applies a large rf pulse to the spins, a Q-spoiler, consisting of a series array of Josephson junctions, is used to reduce the Q of the input circuit to a very low value during the pulse. The Q-spoiler enables the circuit to recover quickly after the pulse, and has been used in an NQR experiment to achieve a sensitivity of about 2 /times/ 10/sup 16/ nuclear Bohr magnetons in a single free precession signal with a bandwidth of 10 kHz. In a third experiment, a sample containing /sup 35/Cl nuclei was placed in a capacitor and the signal detected electrically using a tuned SQUID amplifier and Q-spoiler. In this way, the electrical polarization induced by the precessing Cl nuclear quadrupole moments was detected: this is the inverse of the Stark effect in NQR. Two experiments involving NMR have been carried out. In the first, the 30 MHz resonance in /sup 119/Sn nuclei is detected with a tuned amplifier and Q-spoiler, and a single pulse resolution of 10/sup 18/ nuclear Bohr magnetons in a bandwidth of 25 kHz has been achieved. For the second, a low frequency NMR system has been developed that uses an untuned input circuit coupled to the SQUID. The resonance in /sup 195/Pt nuclei has been observed at 55 kHz in a field of 60 gauss. 23 refs., 11 figs.
Superconducting QUantum Interference Devices (SQUIDs) have been used for more than a decade for the detection of magnetic resonance. Until recently, these devices had mostly been confined to operation in the audiofrequency range, so that experiments have been restricted to measurements of resonance at low frequencies, or of changes in the static susceptibility of a sample induced by rf irradiation at the resonant frequency. However, the recent extension of the operating range of low noise dc SQUIDs to radiofrequencies (rf) allows one to detect magnetic resonance directly at frequencies up to several hundred megahertz. In this paper, we begin by summarizing the properties of dc SQUIDs as tuned rf amplifers. We then describe first, the development of a SQUID system for the detection of pulsed nuclear quadrupole resonance (NQR) at about 30 MHz and second, a novel technique for observing magnetic resonances in the absence of any externally applied rf fields.
A dc superconducting quantum interference device (SQUID) with a resonant microstrip input and a cooled heterostructure field-effect transistor as a postamplifier is used as a radio-frequency amplifier in the frequency range 90–500 MHz. At liquid He3 temperatures, gains of 24 and 20 dB and intrinsic noise temperatures of 0.06±0.02 and 0.12±0.10 K were achieved at 89.6 and 438 MHz, respectively. The system noise temperature at 438 MHz was also estimated from the Nyquist noise produced by a resonant circuit coupled to the input of the microstrip SQUID.
A dc superconducting quantum interference device (SQUID) was used to amplify radio-frequency signals that were coupled to one end of the microstrip formed by the input coil and the SQUID washer. For one device, the resonant frequency of the microstrip was increased from about 200 to 620 MHz by progressively shortening the length of the coil. At an operating temperature of 4.2 K, the gain was typically 18 dB, and the system noise temperature ranged from 0.5±0.3 K at 80 MHz to 3.0±0.7 K at 500 MHz.
We present measurements of an amplifier operating at 3.8 GHz with 150 MHz of bandwidth based on the microstrip input-coil resonance of a dc superconducting quantum interference device (SQUID) with submicron Josephson junctions. The noise temperature is measured using two methods: comparing the signal-to-noise ratio of the system with and without the SQUID in the amplifier chain, and using a modified Y-factor technique where calibrated narrowband noise is mixed up to the SQUID amplifier operating frequency. With the SQUID cooled to 0.35 K, we observe a minimum system noise temperature of 0.55 ± 0.13 K, dominated by the contribution from the SQUID amplifier.
The resonant frequency of an amplifier based on a low-temperature dc superconducting quantum interference device (SQUID) is tuned by varying the capacitance across the end of the input microstrip by means of a varactor diode. The resonant frequency can be reduced substantially, for example, from 190 to 110 MHz, while maintaining an on-resonance gain of 27–28 dB. Two microstrip SQUID amplifiers with the same resonant frequency are cascaded to achieve a gain of 33.5±1 dB at 386 MHz; with the SQUIDs tuned to different frequencies, the gain is 22 dB or higher from about 260 to 420 MHz.