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arXiv:1610.09956 · Review of Scientific Instruments

A rubidium Mx-magnetometer for measurements on solid state spins

Daniel Arnold, Steven Siegel, Emily Grisanti, Jörg Wrachtrup, Ilja Gerhardt

Published Feb 1, 2017• 16 citations
arXivHTMLPDF

Abstract

The detection of environmental magnetic fields is well established by optically pumped atomic magnetometers. Another focus of magnetometry can be the research on magnetic or spin-active solid-state samples. Here we introduce a simple and compact design of a rubidium-based Mx magnetometer, which allows for hosting solid-state samples. The optical, mechanical, and electrical design is reported, as well as simple measurements which introduce the ground-state spin-relaxation time, the signal-to-noise ratio of a measurement, and subsequently the overall sensitivity of the magnetometer. The magnetometer is optimized for the most sensitive operation with respect to laser power and magnetic field excitation at the Larmor frequency.

DOI
10.1063/1.4974845

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The detection of environmental magnetic fields is well established by optically pumped atomic magnetometers. Another focus of magnetometry can be the research on magnetic or spin-active solid-state samples. Here we introduce a simple and compact design of a rubidium-based Mx magnetometer, which allows for hosting solid-state samples. The optical, mechanical, and electrical design is reported, as well as simple measurements which introduce the ground-state spin-relaxation time, the signal-to-noise ratio of a measurement, and subsequently the overall sensitivity of the magnetometer. The magnetometer is optimized for the most sensitive operation with respect to laser power and magnetic field excitation at the Larmor frequency.
A rubidium vapour magnetometer has been made which measures the total geomagnetic field and records its variations continuously over the frequency band 0-1 c/s with sensitivity of 5 × 10 -6 Oe. Optical pumping technique is used to observe the energy separation between the Zeeman sub-levels in the ground state of 85 Rb atom, which is the measure of the ambient magnetic field and is equal to 220 kc/s for the local field of 472 × 10 -3 Oe, with the line width of 200 c/s. Resonance is detected when an applied r.f. field at the Larmor frequency causes redistribution of the population of the energy levels thus increasing absorption in the gas cell of the pumping radiation at 7948 Å. A voltage controlled oscillator supplying the r.f. field is locked on to the Larmor frequency. Resonance radiation is obtained from a rubidium lamp excited from a 150 Mc/s, 2 w power supply. The gas cell contains natural rubidium. This is kept at a temperature of 35-45° C thus maintaining vapour pressure of about 10 -6 mmHg. The design of the lamp and the gas cell is given. Further work to improve the light source and the gas cell should improve the sensitivity of the instrument. Redesign of the electronics to make the system oscillate at the Larmor frequency may also improve sensitivity and increase the frequency response of the instrument. The instrument described was demonstrated at The Institute of Physics and The Physical Society Exhibition in January 1961.
We report a rubidium atomic magnetometer based on pump-probe nonlinear magneto-optical rotation. The rubidium vapor cell is placed in a five-layer magnetic shield with inner coils that can generate uniform magnetic fields along the direction of pump beam, and the cell is also placed in the center of a Helmholtz coil that can generate an oscillating magnetic field perpendicular to the direction of pump beam. The atoms are optically pumped by circularly polarized pump beam along a constant magnetic field in a period of time, then the pump beam is turned off and a /2 pulse of oscillating magnetic field for 87Rb atoms is applied. After the above process, the individual atomic magnetic moments become phase coherent, resulting in a transverse magnetization vector precessing at the Larmor frequency in the magnetic field. The linearly polarized probing beam is perpendicular to the direction of magnetic field, and can be seen as a superposition of the left and right circularly polarized light. Because of the different absorptions and dispersions of the left and right circularly polarized light by rubidium atoms, the polarization direction of probing beam rotates when probing beam passes through rubidium vapor cell. The rotation of the polarization is subsequently converted into an electric signal through a polarizing beam splitter. Finally, the decay signal related to the transverse magnetization vector is measured. The Larmor frequency proportional to magnetic field is obtained by the Fourier transform of the decay signal. The value of magnetic field is calculated from the formula:B=(2/) f, where and f are the gyromagnetic ratio and Larmor frequency, respectively. In order to measure the magnetic field in a wide range, the tracking lock mode is proposed and tested. The atomic magnetometer can track the magnetic field jump of 1000 nT or 10000 nT, indicating that the atomic magnetometer has strong locking ability and can be easily locked after start-up. The main performances in different magnetic fields are tested. The results show that the measurement range of the atomic magnetometer is from 100 nT to 100000 nT, the extreme sensitivity is 0.2 pT/Hz1/2, and the magnetic field resolution is 0.1 pT. The transverse relaxation times of the transverse magnetization vector in different magnetic fields are obtained, and the relaxation time decreases with the increase of the magnetic field. When the measurement range is from 5000 nT to 100000 nT, the magnetic field sampling rate of the atomic magnetometer can be adjusted in a range from 1 Hz to 1000 Hz. The atomic magnetometer in high sampling rate can measure weak alternating magnetic field at low frequency. This paper provides an important reference for developing the atomic magnetometer with large measurement range, high sensitivity and high sampling rate.
We demonstrate a way of operating an optically pumped magnetometer with miniaturized cesium cell using the light-narrowing effect. The magnetometer setup shows improvement of shot-noise-limited sensitivity (42fT/Hz42\phantom{\rule{0.16em}{0ex}}\mathrm{fT}/\sqrt{\mathrm{Hz}}42fT/Hz​ in a cell of only 9.3mm39.3\phantom{\rule{0.16em}{0ex}}{\mathrm{mm}}^{3}9.3mm3 volume) due to the suppression of spin-exchange relaxation to a large extent and the use of a strikingly increased fraction of alkali-metal atoms for signal generation, working even in $\ensuremath{\mu}\mathrm{T}$ magnetic fields, by using only a single high-intensity laser beam both for pumping and probing of atomic spins.
A high-sensitivity optically pumped atomic magnetometer working in the geomagnetic range utilizing the light-narrowing effect and in-phase excitation is described. The setup is based on a simple pump–probe arrangement built around a Cs vapor cell whose active volume is 64 mm3. The transverse oscillating field is applied parallel to the probe beam to drive Zeeman resonance, and the in-phase component of the resonance signal is measured to determine the field. The sensitivity of the magnetometer is improved by pumping most atoms into the stretched state. Consequently, spin-exchange relaxation is suppressed, and a sensitivity of 0.1 pT/Hz1/2 in the range of 10 μT is achieved. This magnetometer has the advantages of large dynamic range, high performance of low-frequency stabilization, high response speed, and compact size. It can be used for many cutting-edge applications such as detection of magnetic anomalies.
In order to measure a weak alternating magnetic field, an optically-pumped Rb magnetometer based on pump-probe structure is investigated and demonstrated. The pumping light and probing light propagate along the z axis and x axis, respectively. A constant polarization magnetic field along the pumping light is applied, which not only stabilizes the polarization of Rb atoms but also tunes resonance frequency of Rb atoms. When a weak alternating magnetic field is applied perpendicularly to the constant magnetic field, the magnetic moment will tip off the z axis and rotate around the z axis. And then the polarization plane of probing light is modulated correspondingly. The x component of the magnetic moment can be obtained with a balanced detector. As a result, a signal proportional to weak alternating magnetic field can be obtained.In order to obtain the magnetic response of the magnetometer, we analyze the signal amplitude as a function of polarization magnetic field strength B0 and transverse relaxation time 2 with numerical simulation. The amplitude-frequency response of the magnetometer is determined mainly by two parameters, namely cutoff frequency c=1/2 and resonance frequency 0= B0, where is the gyromagnetic ratio of Rb atom. At low frequency, that is a0 and a 0c2, the magnetometer has a flat response, here a is the frequency of the weak alternating magnetic field. If 0c, the signal amplitude will be large for large 0 or small c. For a given c, the peak response appears at 0=c. In the vicinity of resonance frequency, if c0, a peak will appear and if c 0, no peak occurs. At high frequency, the amplitude will decrease with the increase of a.We verify the above analyses in experiment. A vapor cell with a short transverse relaxation time is used to obtain large frequency response bandwidth. Through optimizing the powers and frequencies of pumping laser and probing laser, high polarization and detection sensitivity of atomic spin can be obtained. Moreover, through choosing an appropriate polarization magnetic field, the magnetometer can be maximally sensitive to the magnetic field to be measured. The experimental results show that the magnetometer has a sensitivity of about m 0.2; pT/HzHz and bandwidth of about 3.5 kHz. It can be used to detect low field magnetic resonance and high frequency abnormal physical phenomena.
Spin-exchange relaxation free alkali-metal magnetometers typically operate in the regime of high optical density, presenting challenges for simple and efficient optical pumping and detection. We describe a high-sensitivity Rb magnetometer using a single elliptically polarized off-resonant laser beam. Circular component of the light creates relatively uniform spin polarization while the linear component is used to measure optical rotation generated by the atoms. Modulation of the atomic spin direction with an oscillating magnetic field shifts the detected signal to high frequencies. Using a fiber-coupled distributed feedback laser, we achieve magnetic field sensitivity of 7 fT/Hz7\text{ }\text{fT}/\sqrt{\text{Hz}}7 fT/Hz​ with a miniature $5\ifmmode\times\else\texttimes\fi{}5\ifmmode\times\else\texttimes\fi{}5\text{ }\text{mm}\text{ }\text{Rb}$ vapor cell.