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arXiv:cond-mat/0010128 · Physical review. B, Condensed matter

Feasibility of biepitaxial YBa2Cu3O7−x Josephson junctions for fundamental studies and potential circuit implementation

Francesco Tafuri, Franco Carillo, Floriana Lombardi, F. Miletto Granozio, F. Ricci, U. Scotti di Uccio, A. Barone, G. Testa, E. Sarnelli, John R. Kirtley

Published Dec 1, 2000• 23 citations
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Abstract

We present various concepts and experimental procedures to produce biepitaxial ${\mathrm{YBa}}_{2}{\mathrm{Cu}}_{3}{\mathrm{O}}_{7\ensuremath{-}x}$ grain-boundary Josephson junctions. The device properties have an interesting phenomenology, related in part to the possible influence of $\mathrm{``}\ensuremath{\pi}$ loops.'' The performance of our junctions and superconducting quantum interference devices indicates significant improvement in the biepitaxial technique. Further, we propose methods for fabricating circuits in which 0 and $\ensuremath{\pi}$ loops are controllably located on the same chip.

DOI
10.1103/physrevb.62.14431

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IEEE Transactions on Applied Superconductivity•Jan 24, 2019•3 citations
We present various concepts and experimental procedures to produce biepitaxial YBa2Cu3O7\ensuremath−x{\mathrm{YBa}}_{2}{\mathrm{Cu}}_{3}{\mathrm{O}}_{7\ensuremath{-}x}YBa2​Cu3​O7\ensuremath−x​ grain-boundary Josephson junctions. The device properties have an interesting phenomenology, related in part to the possible influence of ‘‘\ensuremathπ\mathrm{``}\ensuremath{\pi}‘‘\ensuremathπ loops.'' The performance of our junctions and superconducting quantum interference devices indicates significant improvement in the biepitaxial technique. Further, we propose methods for fabricating circuits in which 0 and \ensuremathπ\ensuremath{\pi}\ensuremathπ loops are controllably located on the same chip.
We have investigated the properties of biepitaxial ${\mathrm{YBa}}_{2}{\mathrm{Cu}}_{3}{\mathrm{O}}_{7\ensuremath{-}\ensuremath{\delta}}$ grain boundary Josephson junctions, which appear to be characterized by low barrier transmission probabilities. Extrinsic and intrinsic d-wave effects are discussed within the framework of novel designs for $\ensuremath{\pi}$-circuitry and qubits. The absence of spontaneous magnetization and of the consequent additional noise, in a wide range of experimental conditions, seems to be encouraging for designs of ``quiet'' devices.
We present electric noise measurements of nanoscale biepitaxial YBa2{}_{2}2​Cu3{}_{3}3​O${}_{7\ensuremath{-}\ensuremath{\delta}}$ (YBCO) Josephson junctions fabricated by two different lithographic methods. The first (conventional) technique defines the junctions directly by ion milling etching through an amorphous carbon mask. The second (soft patterning) method makes use of the phase competition between the superconducting YBCO (Y123) and the insulating Y2{}_{2}2​BaCuO5{}_{5}5​ (Y211) phase at the grain boundary interface on MgO (110) substrates. The voltage noise properties of the two methods are compared in this study. For all junctions (having a thickness of 100 nm and widths of 250--500 nm), we see a significant amount of individual charge traps. We have extracted an approximate value for the effective area of the charge traps from the noise data. From the noise measurements, we infer that the soft-patterned junctions with a grain-boundary (GB) interface manifesting a large ccc-axis tunneling component have a uniform barrier and a superconductor-insulator-superconductor (SIS) -like behavior. The noise properties of soft-patterned junctions having a GB interface dominated by transport parallel to the ababab planes are in accordance with a resonant tunneling barrier model. The conventionally patterned junctions, instead, have suppressed superconducting transport channels with an area much less than the nominal junction area. These findings are important for the implementation of nanosized Josephson junctions in quantum circuits.
YBa2_22​Cu3_33​O7_77​ 24∘^\circ∘ (30∘^\circ∘) bicrystal grain boundary junctions (GBJs), shunted with 60\,nm (20\,nm) thick Au, were fabricated by focused ion beam milling with widths 80 nm≤w≤7.8 μ80\,{\rm nm} \le w \le 7.8\,μ80nm≤w≤7.8μm. At 4.2\,K we find critical current densities jcj_cjc​ in the 105 A/cm210^5\,{\rm A/cm^2}105A/cm2 range %\dkc{\#1} (without a clear dependence on www) and an increase in resistance times junction area ρρρ with an approximate scaling ρ∝w1/2ρ\propto w^{1/2}ρ∝w1/2. For the narrowest GBJs jcρ≈100 μj_cρ\approx 100\,μjc​ρ≈100μV, which is promising for the realization of sensitive nanoSQUIDs for the detection of small spin systems. We demonstrate that our fabrication process allows the realization of sensitive nanoscale dc SQUIDs; for a SQUID with w≈100w\approx 100w≈100\,nm wide GBJs we find an rms magnetic flux noise spectral density of SΦ1/2≈4 μΦ0/Hz1/2S_Φ^{1/2}\approx 4\,μΦ_0/{\rm Hz}^{1/2}SΦ1/2​≈4μΦ0​/Hz1/2 in the white noise limit. We also derive an expression for the spin sensitivity Sμ1/2S_μ^{1/2}Sμ1/2​, which depends on SΦ1/2S_Φ^{1/2}SΦ1/2​, on the location and orientation of the magnetic moment of a magnetic particle to be detected by the SQUID, and on the SQUID geometry. For the not optimized SQUIDs presented here, we estimate Sμ1/2=390 μB/HzS_μ^{1/2}=390\,μ_B/\sqrt{\rm{Hz}}Sμ1/2​=390μB​/Hz​, which could be further improved by at least an order of magnitude.
A minimal method to fabricate Al/AlOx_xx​/Al Josephson junctions (JJs) using photolithography and argon etching, before metallization and oxidation, is demonstrated. JJs with areas ranging from 1 to 6 μμμm2^22 can be fabricated and, with the appropriate oxidation conditions, the junction resistance can be varied by $\sim$2 orders of magnitude. Transmission electron microscopy reveals the successful fabrication of JJs with few grain boundaries suggesting reduced energy loss from two-level-systems. Superconducting QUantum Interference Devices (SQUIDs) fabricated from this methodology exhibit reduced resistance variation over multiple chips, compared with electron beam lithography, and the devices can sustain repeated thermal cycles to 10 mK with the excellent flux response remaining unchanged. The quantum applications of this technology are demonstrated by embedding a SQUID resonator into a 3D cavity and parametrically amplifying low photon numbers with gains of $\sim$40 dB. This work establishes the simplest approach to fabricating JJs to date, and it could prove pivotal to the widespread utilization of superconducting circuit-based quantum technologies.
We fabricated Josephson junctions (JJs) between the d-wave superconductor (SC) YBa2Cu3O7-x (YBCO) and the s-wave SC Nb (ds-JJs) on graphoepitaxially buffered MgO substrates, studied ds-JJs at temperatures down to 30 mK and employed these JJs in π-loops. Current-voltage characteristics of ds-JJs oriented along the [100] axis of YBCO exhibited up to a factor of 200 higher critical current densities than ds-JJs oriented along the [110] axis of YBCO. The critical currentIcI_{c}Ic​and theIcRnI_{c}R_{n}Ic​Rn​product of [100]-oriented 3 μm wide ds-JJs are ∼70 μA and ∼200 μV, respectively, at 4.2 K. Rectangular arrays of up to 40 000 π-loops based on such ds-JJs were investigated using a low temperature scanning superconducting quantum interference device (SQUID) microscope. We observed ordering of spontaneously generated half integer magnetic flux quanta in the π-loops correlated with minute spurious background magnetic fields, as well as with configurations and mutual coupling of the π-loops. We manipulated the magnetic states of the π-loops by the local application of magnetic fields using nearby planar coils. This paper paves the way for the use of π-loops in computations that are based on annealing processes.