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Scientific Reports

Laser light routing in an elongated micromachined vapor cell with diffraction gratings for atomic clock applications

Ravinder Chutani, Vincent N. Maurice, Nicolas Passilly, Christophe Gorecki, Rodolphe Boudot, Moustafa Abdel Hafiz, Philippe Abbé, Serge Galliou, Jean‐Yves Rauch, Emeric de Clercq

Published Sep 14, 2015• 54 citations
Publisher

Abstract

This paper reports on an original architecture of microfabricated alkali vapor cell designed for miniature atomic clocks. The cell combines diffraction gratings with anisotropically etched single-crystalline silicon sidewalls to route a normally-incident beam in a cavity oriented along the substrate plane. Gratings have been specifically designed to diffract circularly polarized light in the first order, the latter having an angle of diffraction matching the (111) sidewalls orientation. Then, the length of the cavity where light interacts with alkali atoms can be extended. We demonstrate that a longer cell allows to reduce the beam diameter, while preserving the clock performances. As the cavity depth and the beam diameter are reduced, collimation can be performed in a tighter space. This solution relaxes the constraints on the device packaging and is suitable for wafer-level assembly. Several cells have been fabricated and characterized in a clock setup using coherent population trapping spectroscopy. The measured signals exhibit null power linewidths down to 2.23 kHz and high transmission contrasts up to 17%. A high contrast-to-linewidth ratio is found at a linewidth of 4.17 kHz and a contrast of 5.2% in a 7-mm-long cell despite a beam diameter reduced to 600 μm.

DOI
10.1038/srep14001

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This paper reports on an original architecture of microfabricated alkali vapor cell designed for miniature atomic clocks. The cell combines diffraction gratings with anisotropically etched single-crystalline silicon sidewalls to route a normally-incident beam in a cavity oriented along the substrate plane. Gratings have been specifically designed to diffract circularly polarized light in the first order, the latter having an angle of diffraction matching the (111) sidewalls orientation. Then, the length of the cavity where light interacts with alkali atoms can be extended. We demonstrate that a longer cell allows to reduce the beam diameter, while preserving the clock performances. As the cavity depth and the beam diameter are reduced, collimation can be performed in a tighter space. This solution relaxes the constraints on the device packaging and is suitable for wafer-level assembly. Several cells have been fabricated and characterized in a clock setup using coherent population trapping spectroscopy. The measured signals exhibit null power linewidths down to 2.23 kHz and high transmission contrasts up to 17%. A high contrast-to-linewidth ratio is found at a linewidth of 4.17 kHz and a contrast of 5.2% in a 7-mm-long cell despite a beam diameter reduced to 600 μm.
This paper describes the fabrication of chip-scale alkali atom vapor cells, for use in highly miniaturized atomic frequency references, using silicon micromachining and anodic bonding technology. The cells consist of silicon cavities with internal volume ranging from a few mm/sup 3/ to less than 1 mm/sup 3/. The cells were filled with cesium and nitrogen buffer gas either by chemical reaction of cesium chloride and barium azide, or by direct injection of elemental cesium within a controlled anaerobic environment. Cesium optical absorption spectra were obtained from the cells, and coherent population trapping resonances with linewidths of about 1 kHz were measured.
We investigate the architecture of microfabricated vapor cells with reflective sidewalls for applications in chip scale atomic sensors. The optical configuration in operation is suitable for both one-beam and two-beam (pump & probe) schemes. In the miniaturized vapor cells, the laser beam is reflected twice by the aluminum reflectors on the wet etched 54.7° sidewalls to prolong the optical length significantly, thus resulting in a return reflectance that is three times that of bare silicon sidewalls. To avoid limitations faced in the fabrication process, a simpler, more universal and less constrained fabrication process of microfabricated vapor cells for chip scale atomic sensors with uncompromised performance is implemented, which also decreases the fabrication costs and procedures. Characterization measurements show that with effective sidewall reflectors, mm³ level volume and feasible hermeticity, the elongated miniature vapor cells demonstrate a linear absorption contrast improvement by 10 times over the conventional micro-electro-mechanical system (MEMS) vapor cells at ~50 °C in the rubidium D1 absorption spectroscopy experiments. At the operating temperature of ~90 °C for chip scale atomic sensors, a 50% linear absorption contrast enhancement is obtained with the reflective cell architecture. This leads to a potential improvement in the clock stability and magnetometer sensitivity. Besides, the coherent population trapping spectroscopy is applied to characterize the microfabricated vacuum cells with 46.3 kHz linewidth in the through cell configuration, demonstrating the effectiveness in chip scale atomic sensors.
Herein, a microfabricated millimeter-level vapor alkali cell with a high hermeticity is fabricated through a wet etching and single-chip anodic bonding process. The vapor cell, containing Rb and N2, was investigated in a coherent population trapping (CPT) setup for the application of a chip-scale atomic clock (CSAC). The contrast of CPT resonance is up to 1.1% within the only 1 mm length of light interacting with atom. The effects of some critical external parameters on the CPT resonance, such as laser intensity, cell temperature, and buffer gas pressure, are thoroughly studied and optimized. The improved microfabricated vapor cell also exhibited great potential for other chip-scale atomic devices.
This paper reports the design, fabrication and evaluation of a reflection-type Rb vapor cell with a Glass/Si/Glass structure for chip-scale micro atomic clocks. To miniaturize the cell and obtain a Rb resonance signal with a high sensitivity, long laser light traveling pass on the horizontal plane is required in the vapor cell. The horizontal Rb vapor cell with integrated mirrors are proposed and developed. A (100)-oriented Si wafer with cut off 9.74° toward [011] direction was used to make 45° mirrors by using anisotropic wet etching. Also, 90° mirrors were fabricated by Si deep RIE (Reactive Ion Etching) and H2annealing. Absorption line of Rb was confirmed and CPT (Coherent Population Trapping) resonance was demonstrated in the fabricated devices.
This paper presents the latest progress in the development, fabrication, and characterization of microfabricated atomic frequency references at NIST. With volumes below 10 mm3 the physics packages contain the complete integrated assembly for probing the ground-state hyperfine splitting frequency of the alkali atoms by coherent population trapping (CPT). This technique allows for a simple and compact device containing a vertical-cavity surface-emitting laser (VCSEL), optics to shape the laser beam, a vapor cell containing the atoms, and a detector. We present an improved technique for microfabricating the miniature alkali vapor cells. When integrated into a CPT clock, a clear reduction of long-term frequency drifts is observed. This leads to a fractional frequency instability of less than 10-11 at one hour of integration, a more than one order of magnitude improvement over previous results. We identify the remaining sensitivities of the clock frequency to environmental influences and propose ways to reduce them.
Atomic clocks represent the most advanced instruments for providing time-frequency standards, with increasing demand for designs that offer high frequency stability while minimizing size. Central to an atomic clock’s function is the atomic vapor cell, which serves as the quantum reference. Compared to traditional cells, wafer-level micro-electro-mechanical systems (MEMS) vapor cells enable cost-effective, scalable production and facilitate integration with silicon-based chips. In this work, we present a wafer-level MEMS vapor cell featuring an innovative silicon-glass-silicon transverse optical path structure. A single wafer is used to fabricate 24 identical atomic vapor cells, each with precise dimensions of 14 mm×14 mm×4.3 mm, ensuring scalability. We demonstrate an optical frequency standard that combines modulation transfer spectroscopy (MTS) with a MEMS vapor cell, featuring a compact design with excellent performance. This frequency standard achieves stability over averaging times of 1–400 s, with short-term stability of 2.6×10 −13 at 1 s and 5.1×10 −14 at 200 s. The laser linewidth is only 3.9 kHz, marking a substantial improvement over existing thermal standards, and opening potential applications in navigation, radar, and precision measurement. This work provides a crucial step toward the development of chip-scale optical clocks.