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Proceedings of SPIE, the International Society for Optical Engineering/Proceedings of SPIE

Sealing techniques for on-chip atomic vapor cells

John F. Hulbert, Brandon T. Carroll, Aaron R. Hawkins, Bin Wu, Holger Schmidt

Published Jan 10, 2008• 1 citation
Publisher

Abstract

We have recently reported atomic spectroscopy using on-chip rubidium vapor cells based on hollow core waveguides. To make the cells more robust and capable of multiple temperature cycles, we examined several techniques for Rb introduction and sealing. To date the most successful sealing technique has been pinching off the end of a short length of copper tubing. This technique not only hermetically seals the cells, but also allows them to be evacuated to a desired pressure. We have been able to evacuate glass prototype Rb vapor cells to a pressure as low as 80 mTorr and as high as 2 Torr and successfully observe the Rb optical absorption spectrum. Along with our testing of sealing techniques we have been observing the effects of different epoxies and inert gas atmospheres on the robustness of vapor cells. With optimal parameters we have successfully observed the Rb optical absorption spectrum through multiple temperature cycles. These new Rb introduction and sealing methods will be applied to on-chip cells containing integrated hollow waveguides which can be used for a number of different optical applications, such as electromagnetically induced transparency, single-photon nonlinearities, and slow light.

DOI
10.1117/12.763642

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•Jan 1, 2010•0 citations
We have recently reported atomic spectroscopy using on-chip rubidium vapor cells based on hollow core waveguides. To make the cells more robust and capable of multiple temperature cycles, we examined several techniques for Rb introduction and sealing. To date the most successful sealing technique has been pinching off the end of a short length of copper tubing. This technique not only hermetically seals the cells, but also allows them to be evacuated to a desired pressure. We have been able to evacuate glass prototype Rb vapor cells to a pressure as low as 80 mTorr and as high as 2 Torr and successfully observe the Rb optical absorption spectrum. Along with our testing of sealing techniques we have been observing the effects of different epoxies and inert gas atmospheres on the robustness of vapor cells. With optimal parameters we have successfully observed the Rb optical absorption spectrum through multiple temperature cycles. These new Rb introduction and sealing methods will be applied to on-chip cells containing integrated hollow waveguides which can be used for a number of different optical applications, such as electromagnetically induced transparency, single-photon nonlinearities, and slow light.
The author presents the successful development of an on-chip, monolithic, integrated rubidium vapor-cell. These vapor-cells integrate ridge waveguide techniques with hollow-core waveguiding technology known as Anti-Resonant Reflecting Optical Waveguides (ARROWs). These devices are manufactured on-site in BYU's Integrated Microelectronic Laboratory (IML) using common silicon wafer microfabrication techniques. The ARROW platform fabrication is outlined, but the bulk of the dissertation focuses on novel packaging techniques that allow for the successful introduction and sealing of rubidium vapor into these micro-sized vapor-cells. The unique geometries and materials utilized in the ARROW platform render common vapor-cell sealing techniques unusable. The development of three generations of successful vapor-cells is chronicled. The sealing techniques represented in these three generations of vapor-cells include high-temperature epoxy seals, cold-weld copper crimping, variable pressure vacuum capabilities, indium solder seals, and electroplated passivation coatings. The performance of these seals are quantified using accelerated lifetime tests combined with optical spectroscopy. Finally, the successful probing of the rubidium absorption spectrum, electromagnetically induced transparency, and slow light on the ARROW-based vapor-cell platform is reported.
This thesis presents the integration of atomic vapor cells with anti-resonant reflecting optical waveguides (ARROWs) fabricated on silicon chips. These potentially provide a compact platform for a number of optical applications, including the study of quantum coherence effects such as electromagnetically induced transparency and single-photon nonlinearities, as well as frequency stabilization standards. The use of hollow waveguides allows for light propagation in low index (vapor) media with compact mode areas. ARROWs make particularly attractive waveguides for this purpose because they can be interfaced with solid core waveguides, microfabricated on a planar substrate, and are effectively single mode. ARROW fabrication utilizes an acid-removed sacrificial core surrounded by alternating plasma deposited dielectric layers, which act as Fabry-Perot reflectors. To demonstrate the effectiveness of the ARROW as a vapor cell, a platform consisting of solid and hollow core waveguides integrated with rubidium vapor cells was developed. A variety of sealing techniques were tested for vapor cell integration with the ARROW chip and for compatibility with rubidium. Rubidium was used because it is of particular interest for studying quantum coherence effects. Liquefied rubidium was transferred from a bulk supply into an on-chip vapor cell in an anaerobic atmosphere glovebox. Optical absorption measurements confirmed the presence of rubidium vapor within the hollow waveguide platform. Further analysis of the measurements revealed high optical density of rubidium atoms in the hollow core. Saturated absorption spectroscopy measurements verified that the on-chip integrated vapor cell was suitable for common precision spectroscopy applications.
Atomic spectroscopy relies on photons to probe the energy states of atoms, typically in a gas state. In addition to providing fundamental scientific information, this technique can be applied to a number of photonic devices including atomic clocks, laser stabilization references, slow light elements, and eventually quantum communications components. Atomic spectroscopy has classically been done using bulk optics and evacuated transparent vapor cells. Recently, a number of methods have been introduced to dramatically decrease the size of atomic spectroscopy systems by integrating optical functionality. We review three of these techniques including: 1) photonic crystal fiber based experiments, 2) wafer bonded mini-cells containing atomic vapors and integrated with lasers and detectors, and 3) hollow waveguides containing atomic vapors fabricated on silicon substrates. In the context of silicon photonics, we will emphasize the hollow waveguide platform. At the heart of these devices is the anti-resonant reflecting optical waveguide (ARROW). ARROW fabrication techniques will be described for both hollow and solid core designs. Solid-core waveguides are necessary to direct light on and off the silicon chip while confining atomic vapors to hollow-core waveguides. We will also discuss the methods and challenges of attaching rubidium vapor reservoirs to the chip. Experimental results for optical spectroscopy of rubidium atoms on a chip will be presented.
We review the current status of integrating optical quantum interference effects such as electromagnetically induced transparency (EIT), slow light, and highly efficient nonlinear processes on a semiconductor chip. A necessary prerequisite for combining effects such as slow light and related phenomena with the convenience of integrated optics is the development of integrated alkali vapor cells. Here, we describe the development of integrated rubidium cells based on hollow-core antiresonant reflecting optical waveguides (ARROWs). Hollow-core waveguides were fabricated on a silicon platform using conventional microfabrication and filled with rubidium vapor using different methods. Rubidium absorption through the waveguides was successfully observed which opens the way to integrated atomic and molecular on a chip. The realization of quantum coherence effects requires additional surface treatment of the waveguide walls, and the effects of the surface coating on the waveguide properties are presented.
Light-matter interactions are fundamentally based on the quantum mechanical principles that govern photons, electrons and other fundamental particles. One very interesting phenomenon within all of light-matter interactions is Electromagnetically Induced Transparency(EIT). This phenomenon causes an otherwise absorbing atomic transition to stop absorbing through quantum mechanical interference of probability wave functions. Corresponding to that change in absorption, will be a sudden, large change in the index of refraction. This change in the index of refraction leads to another phenomenon in which the group velocity of light can be slowed down dramatically. In the past, many researchers have been able to achieve both EIT and slow light in bulk atomic vapor cells. In an attempt to miniaturize this process and we have been using a platform of Anti Resonant Reflecting Optical Waveguides (ARROW) devices to both guide light and contain the interacting matter. However, the platform creates a whole new set of challenges when integrating rubidium vapor into the hollow waveguides as rubidium is highly reactive and it is difficult to maintain an inert atmosphere for the rubidium vapor. A variety of sealing methods were attempted and their appropriateness and effectiveness was analyzed. Among these sealing methods were PMMA, Crystal Wax, Active Solder, Epoxy, and Indium Solder. PMMA, Crystal Wax and Active Solder each had major faults in one or more of the sealing requirements. We have used a high temperature epoxy with relative success to contain the rubidium vapor. However, the epoxy degrades very quickly at the high temperatures required for EIT testing. Indium solder is the most recent application method. It has high potential although we have yet to fully test its effectiveness. We were able to successfully demonstrate the first EIT and slow light on a chip with our ARROW atomic vapor cell system. In the slow light experiment, we were able to slow light down to 2.5x105m/s. The group velocity of light decreased from the standard 3x108m/s by a factor of 1200. We believe we can achieve even lower group velocities using this same platform through further experimentation.