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IEEE Transactions on Applied Superconductivity

Accurate Real-Time Monitoring of Quality Factor and Center Frequency of Superconducting Resonators

Sebastian E. de Graaf, Andrey V. Danilov, Sergey Kubatkin

Published Apr 9, 2014• 8 citations
Publisher

Abstract

In this paper, we track both center frequency and quality factor of a superconducting microwave resonator with very high precision using a modified Pound-Drever-Hall frequency locking scheme. The quality factor measurements can be done with high enough bandwidth to study different processes in a superconducting resonator in real time. With this added functionality, the frequency readout remains unaffected, with typical accuracy around 10-30 Hz/√(Hz), whereas the cavity loss rate can be determined to within 0.1% on a millisecond time scale (34 dB/√(Hz)). As we demonstrate, this can be particularly useful for electron spin resonance measurements, where we achieve a minimum number of detectable spins coupled to the resonator N = 5 ·105spins/√(Hz), based on quality factor measurements. It also enables the study of fast dynamic processes, for example, vortex dynamics, in these devices on a short time scale.

DOI
10.1109/tasc.2014.2316202

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In this paper, we track both center frequency and quality factor of a superconducting microwave resonator with very high precision using a modified Pound-Drever-Hall frequency locking scheme. The quality factor measurements can be done with high enough bandwidth to study different processes in a superconducting resonator in real time. With this added functionality, the frequency readout remains unaffected, with typical accuracy around 10-30 Hz/√(Hz), whereas the cavity loss rate can be determined to within 0.1% on a millisecond time scale (34 dB/√(Hz)). As we demonstrate, this can be particularly useful for electron spin resonance measurements, where we achieve a minimum number of detectable spins coupled to the resonator N = 5 ·105spins/√(Hz), based on quality factor measurements. It also enables the study of fast dynamic processes, for example, vortex dynamics, in these devices on a short time scale.
In this master's thesis, I present the design, fabrication, and characterisation of superconducting microwave resonators. These resonators are quarter-wavelength coplanar waveguide resonators, operating at resonance frequencies between 4 GHz and 8 GHz. This kind of resonator is a key component in several applications, ranging from quantum computation devices to parametric amplifiers. Minimising the losses (achieving high internal quality factors) in these resonators is important to maximise performance of the applications they are used for. During the thesis work, we have studied several possible changes to improve the resonator quality.\n\nFabrication of the resonators was done in the Nanofabrication Laboratory at Chalmers University of Technology, and consist of the following steps: cleaning a sapphire or silicon wafer, depositing a layer of superconducting niobium, photolithography, and etching the waveguide. We then measured the resonators in a cryogen-free dilution refrigerator, at a temperature of 10 mK. The measurements consisted of a power sweep, in order to quantify the quality factor at high and low excitation powers. As an example, the first resonator we fabricated had a quality factor of 4.3 x 10^4 at high power (about 10^5 photons in the resonator), and quality factor of 3.7 x 10^4 at the single-photon level.\n\nWe then investigated different loss mechanisms that we expect to negatively affect the quality factor, and how to reduce this loss. Firstly, to reduce radiation losses and magnetic vortex losses, we reduced the lateral dimensions of the resonator. Secondly, as two-level system (TLS) losses are believed to mainly reside at the surfaces of the materials and interfaces between them, we etched into the substrate to selectively move a part of the TLS away from the resonator. We also studied the effect of the meandering of the resonator on the quality factor, as well as using two different etching gasses.\n\nBy gathering all this data, we were then able to compare the different combinations to see the effect of the changing parameters. In conclusion, the reduced lateral dimensions and the removal of part of the substrate indeed reduce the losses, as expected from the theory. We also found interesting behaviour with regards to the meandering, namely that having a meandered structure negatively affects the quality factor.\n\nCombining all results, we can give a guideline for the fabrication of resonators in the future, which gave us a quality factor up to 4.9 x 10^5 at high excitation power, and 3.0 x 10^5 at the single photon level.
Slow noise processes, with characteristic timescales $\ensuremath{\sim}$1 s, have been studied in planar superconducting resonators. A frequency-locked loop is employed to track deviations of the resonator center frequency with high precision and bandwidth. Comparative measurements are made in varying microwave drive and temperature, and between bare resonators and those with an additional dielectric layer. All resonators are found to exhibit flicker frequency noise which increases with decreasing microwave drive. We also show that an increase in temperature results in a saturation of flicker noise in resonators with an additional dielectric layer, while bare resonators stop exhibiting flicker noise, instead showing a random frequency walk process.
Abstract The performance of superconducting resonators underpins a wide range of modern quantum technologies, yet their quality factor often deviates at low temperatures from standard Mattis-Bardeen predictions. This discrepancy is often attributed to nonthermal quasiparticles generated by microwave readout power, which limits the sensitivity of superconducting devices. We present a macroscopic model based on modified Rothwarf-Taylor equations that incorporates a power-dependent phonon generation term, providing an explicit relationship between quality factor, bath temperature and readout power. The model shows excellent agreement with temperature sweep measurements of NbN microstrip resonators with β-Ta terminations over a wide dynamic range of readout power levels, accurately capturing the transition between thermally-dominated and microwave-induced loss regimes. This framework provides a predictive tool for optimizing superconducting resonators and advancing the design of high-Q devices for quantum sensing and quantum information processing.
A wide variety of applications of microwave cavities, such as measurement and control of superconducting qubits, magnonic resonators, and phase noise filters, would be well served by having a highly tunable microwave resonance. Often this tunability is desired in situ at low temperatures, where one can take advantage of superconducting cavities. To date, such cryogenic tuning while maintaining a high quality factor has been limited to ∼500 MHz. Here we demonstrate a three-dimensional superconducting microwave cavity that shares one wall with a pressurized volume of helium. Upon pressurization of the helium chamber, the microwave cavity is deformed, which results in in situ tuning of its resonant frequency by more than 5 GHz, greater than 60% of the original 8 GHz resonant frequency. The quality factor of the cavity remains approximately constant at ≈7 × 103 over the entire range of tuning. As a demonstration of its usefulness, we implement a tunable cryogenic phase noise filter, which reduces the phase noise of our source by approximately 10 dB above 400 kHz.
Vortices trapped in thin-film superconducting microwave resonators can have a significant influence on the resonator performance. Using a variable-linewidth geometry for a weakly coupled resonator, we are able to observe the effects of a single vortex trapped in the resonator through field cooling. For resonant modes where the vortex is near a current antinode, the presence of even a single vortex leads to a measurable decrease in the quality factor and a dispersive shift of the resonant frequency. For modes with the vortex located at a current node, the presence of the vortex results in no detectable excess loss and, in fact, produces an increase in the quality factor. We attribute this enhancement to a reduction in the density of nonequilibrium quasiparticles in the resonator due to their trapping and relaxation near the vortex core.
We propose a method for detecting the presence of a single spin in a crystal by coupling it to a high-quality factor superconducting planar resonator. By confining the microwave field in the vicinity of a constriction of nanometric dimensions, the coupling constant can be as high as 5--10 kHz. This coupling affects the amplitude of the field reflected by the resonator and the integrated homodyne signal allows detection of a single spin with unit signal-to-noise ratio within few milliseconds. We further show that a stochastic master equation approach and a Bayesian analysis of the full time-dependent homodyne signal improves this figure by $\ensuremath{\sim}30%$ for typical parameters.