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arXiv:2311.03702

Latched Detection of Zeptojoule Spin Echoes with a Kinetic Inductance Parametric Oscillator

Wyatt Vine, Anders Kringhøj, Mykhailo Savytskyi, Daniel J. Parker, Thomas Schenkel, Brett C. Johnson, Jeffrey Colin McCallum, Andrea Morello, Jarryd J. Pla

Published Nov 7, 2023• 0 citations
arXivHTMLPDF

Abstract

When strongly pumped at twice their resonant frequency, non-linear resonators develop a high-amplitude intracavity field, a phenomenon known as parametric self-oscillations. The boundary over which this instability occurs can be extremely sharp and thereby presents an opportunity for realizing a detector. Here we operate such a device based on a superconducting microwave resonator whose non-linearity is engineered from kinetic inductance. The device indicates the absorption of low-power microwave wavepackets by transitioning to a self-oscillating state. Using calibrated wavepackets we measure the detection efficiency with zeptojoule energy wavepackets. We then apply it to measurements of electron spin resonance, using an ensemble of $^{209}$Bi donors in silicon that are inductively coupled to the resonator. We achieve a latched-readout of the spin signal with an amplitude that is five hundred times greater than the underlying spin echoes.

DOI
10.48550/arxiv.2311.03702

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When strongly pumped at twice their resonant frequency, nonlinear resonators develop a high-amplitude intracavity field, a phenomenon known as parametric self-oscillations. The boundary over which this instability occurs can be extremely sharp and thereby presents an opportunity for realizing a detector. Here, we operate such a device based on a superconducting microwave resonator whose nonlinearity is engineered from kinetic inductance. The device indicates the absorption of low-power microwave wavepackets by transitioning to a self-oscillating state. Using calibrated pulses, we measure the detection efficiency to zeptojoule energy wavepackets. We then apply it to measurements of electron spin resonance, using an ensemble of209Bi donors in silicon that are inductively coupled to the resonator. We achieve a latched readout of the spin signal with an amplitude that is five hundred times greater than the underlying spin echoes.

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In this licentiate thesis, I present the design, fabrication, and characterization of superconducting parametric resonators, for use in quantum information processing. These devices are quarter-wavelength coplanar waveguide resonators (~5 GHz), terminated at one end by a non-linear inductance provided by a SQUID (superconducting quantum interference device). The SQUID acts as a flux-controlled boundary condition, which effectively changes the electrical length of the resonator. This enables the modulation of the resonant frequency by coupling microwave magnetic flux into the SQUID, using on-chip transmission lines. The modulation occurs on a timescale much faster than the photon loss out of the resonator. The non-linearity provides several different regimes for operating this device. I focused on the parametric regime, in which the non-linear element was being modulated (pumped) at or near twice the resonant frequency. This pumping can lead to amplification and frequency conversion of an incoming signal. It can also give rise to instabilities and self-oscillations "parametric oscillations" - that is, the generation of an intense electric field in the resonator (the creation of photons). Parametric oscillations set in when the pumping strength exceeds a threshold value, and also depends on the pump-frequency detuning from twice the resonance and on the static flux through the SQUID. I characterized the devices over a wide parameter range by doing homodyne detection of the reflected signal or of the emitted field oscillations. In particular, I investigated the damping and two leading nonlinearities, dominating in different operating regimes, which influence the dynamics of the parametric resonator. First, I extracted the Duffing nonlinearity by studying the line width of the resonator as a function of the input signal (without pumping the SQUID). Second, with high pump amplitude, I extracted the pump-induced nonlinearity by determining the threshold parameters (pump amplitude and detuning) for the onset of parametric oscillations; this nonlinearity leads to the generation of higher-order pump terms that complicate the system dynamics, but can be mitigated now that they have been understood. My results validate a recent theoretical model for the classical, non-linear dynamics of parametric resonance, and helps determine workable design parameters. Finally, I helped develop a linearized model $-$ the "pumpistor" - describing this device in terms of a flux-controlled impedance. This will be useful when designing more complex circuits. One goal of this work is to demonstrate single-shot measurements on superconducting qubits (quantum bits of information). We will use the parametric resonator as a threshold discriminator, associating the qubit's two energy eigenstates with the parametric oscillations either turning on or not. This would be a very useful device in the quantum engineer's toolbox when designing systems for quantum information processing and communication.

•Jan 1, 2013•1 citation

Design and measurement of superconducting microwave kinetic inductance detectors

Florian Blauth

Microwave kinetic inductance detectors (MKID) are superconducting broadband direct detectors. If a superconducting thin film patterned into a resonator is illuminated with photons, Cooper pairs break up and the kinetic inductance of the film changes. This shifts the resonance frequency downwards and the dissipation of the resonator increases, which can be detected in the phase and amplitude of a transmitted signal. \n \nIn this thesis, a waveguide coupled MKID is designed and simulated. 350 GHz radiation is coupled into a copper waveguide via a horn antenna. A waveguide probe leads the signal onto a 9 µm silicon membrane where it is absorbed in a 40 nm superconducting aluminum film which is the inductive part of a superconducting resonator. The capacitor of the resonator is made of niobium. Two versions of the device are developed, a transmission line resonator and a lumped element resonator design. The new design will enable an accurate understanding of the optical sensitivity of MKIDs and allow comparison of different resonator materials. Since two different resonator types are used, the direct comparison of transmission line and lumped resonators will also be possible. \n \nA measurement setup is developed including an ADR cryostat to cool MKID devices down to below 40 mK. An analog readout system using either a vector network analyzer or an IQ mixer is designed and built. The necessary software to control the ADR, the temperature monitoring, the readout signal generation and detection and the signal acquisition of the setup is also developed. \n \nThe waveguide coupled MKID design is fabricated in our in-house microfabrication laboratory and measured in the new setup. In my measurements, the devices do not show a resonance feature. The VNA and DC measurements are analyzed to determine a plausible hypothesis of the failure. The devices are diagnosed for critical issues during fabrication which will be addressed in a future iteration. \n \nTo verify the measurement setup, a test device of the IRAM NIKA 2 MKID camera is measured and the complete analysis pipeline is exercised. The quasi-particle lifetime in the aluminum thin films is measured and a dark and optical noise equivalent power are determined. The results are within the uncertainty comparable to measurements of IRAM themselves. \n \nA test chip designed in my master thesis that contains eight NbTiN resonators is measured in the new setup and non-linear effects under strong readout power are studied. Parametric amplification and oscillation of a resonator are shown qualitatively.

•Oct 1, 2019•0 citations
When strongly pumped at twice their resonant frequency, non-linear resonators develop a high-amplitude intracavity field, a phenomenon known as parametric self-oscillations. The boundary over which this instability occurs can be extremely sharp and thereby presents an opportunity for realizing a detector. Here we operate such a device based on a superconducting microwave resonator whose non-linearity is engineered from kinetic inductance. The device indicates the absorption of low-power microwave wavepackets by transitioning to a self-oscillating state. Using calibrated wavepackets we measure the detection efficiency with zeptojoule energy wavepackets. We then apply it to measurements of electron spin resonance, using an ensemble of 209^{209}209Bi donors in silicon that are inductively coupled to the resonator. We achieve a latched-readout of the spin signal with an amplitude that is five hundred times greater than the underlying spin echoes.
When strongly pumped at twice their resonant frequency, nonlinear resonators develop a high-amplitude intracavity field, a phenomenon known as parametric self-oscillations. The boundary over which this instability occurs can be extremely sharp and thereby presents an opportunity for realizing a detector. Here, we operate such a device based on a superconducting microwave resonator whose nonlinearity is engineered from kinetic inductance. The device indicates the absorption of low-power microwave wavepackets by transitioning to a self-oscillating state. Using calibrated pulses, we measure the detection efficiency to zeptojoule energy wavepackets. We then apply it to measurements of electron spin resonance, using an ensemble of209Bi donors in silicon that are inductively coupled to the resonator. We achieve a latched readout of the spin signal with an amplitude that is five hundred times greater than the underlying spin echoes.
Microwave kinetic inductance detectors are typically operated at high readout power to raise the detector signal above system noise. At sufficiently large readout power, the current-dependent kinetic inductance couples the detector response to its readout bias. Using a nonlinear resonator framework and time-domain circuit calculations, we show that the amplitude, shape, and relaxation time of the driven detector's response depend on both the absorbed energy and on the readout bias. Strongly driven bias points produce amplified, extended, and non-exponential pulse responses. Qualitative agreement between calculated and measured pulse responses indicates that these effects are dominated by the driven nonlinear resonator dynamics rather than by altered quasiparticle dynamics. Beyond resonance bifurcation, sufficiently large pulse events drive the resonator between stable branches, resulting in a metastable latched state which persists after the quasiparticle transient has decayed. The pulse energy required for branch switching is set by the readout bias, suggesting a mode of triggered detection with an in-situ tunable threshold. Although nonlinear operation requires calibration of the bias- and energy-dependent response, the enhanced pulse amplitude and duration, together with tunable latching and the ability to select these parameters via the readout operating state, are likely to be of interest for single-photon and rare-event experiments, especially those limited by amplifier or system noise.
The use of superconducting microresonators together with quantum-limited Josephson parametric amplifiers has enhanced the sensitivity of pulsed electron spin resonance (ESR) measurements by more than four orders of magnitude. So far, the microwave resonators and amplifiers have been designed as separate components due to the incompatibility of Josephson junction–based devices with magnetic fields. This has produced complex spectrometers and raised technical barriers toward adoption of the technique. Here, we circumvent this issue by coupling an ensemble of spins directly to a weakly nonlinear and magnetic field–resilient superconducting microwave resonator. We perform pulsed ESR measurements with a 1-pL mode volume containing 6 × 10 7 spins and amplify the resulting signals within the device. When considering only those spins that contribute to the detected signals, we find a sensitivity of 2.8 × 1 0 3 spins / Hz for a Hahn echo sequence at a temperature of 400 mK. In situ amplification is demonstrated at fields up to 254 mT, highlighting the technique’s potential for application under conventional ESR operating conditions.
The use of superconducting micro-resonators in combination with quantum-limited Josephson parametric amplifiers has in recent years lead to more than four orders of magnitude improvement in the sensitivity of pulsed Electron Spin Resonance (ESR) measurements. So far, the microwave resonators and amplifiers have been designed as separate components, largely due to the incompatibility of Josephson junction-based devices with even moderate magnetic fields. This has led to complex spectrometers that operate under strict environments, creating technical barriers for the widespread adoption of the technique. Here we circumvent this issue by inductively coupling an ensemble of spins directly to a weakly nonlinear microwave resonator, which is engineered from a magnetic field-resilient thin superconducting film. We perform pulsed ESR measurements with a 111~pL effective mode volume and amplify the resulting spin signal using the same device, ultimately achieving a sensitivity of 2.8×1032.8 \times 10^32.8×103 spins in a single-shot Hahn echo measurement at a temperature of 400 mK. We demonstrate the combined functionalities at fields as large as 254~mT, highlighting the technique's potential for application under more conventional ESR operating conditions.
In this licentiate thesis, I present the design, fabrication, and characterization of superconducting parametric resonators, for use in quantum information processing. These devices are quarter-wavelength coplanar waveguide resonators (~5 GHz), terminated at one end by a non-linear inductance provided by a SQUID (superconducting quantum interference device). The SQUID acts as a flux-controlled boundary condition, which effectively changes the electrical length of the resonator. This enables the modulation of the resonant frequency by coupling microwave magnetic flux into the SQUID, using on-chip transmission lines. The modulation occurs on a timescale much faster than the photon loss out of the resonator. The non-linearity provides several different regimes for operating this device. I focused on the parametric regime, in which the non-linear element was being modulated (pumped) at or near twice the resonant frequency. This pumping can lead to amplification and frequency conversion of an incoming signal. It can also give rise to instabilities and self-oscillations "parametric oscillations" - that is, the generation of an intense electric field in the resonator (the creation of photons). Parametric oscillations set in when the pumping strength exceeds a threshold value, and also depends on the pump-frequency detuning from twice the resonance and on the static flux through the SQUID. I characterized the devices over a wide parameter range by doing homodyne detection of the reflected signal or of the emitted field oscillations. In particular, I investigated the damping and two leading nonlinearities, dominating in different operating regimes, which influence the dynamics of the parametric resonator. First, I extracted the Duffing nonlinearity by studying the line width of the resonator as a function of the input signal (without pumping the SQUID). Second, with high pump amplitude, I extracted the pump-induced nonlinearity by determining the threshold parameters (pump amplitude and detuning) for the onset of parametric oscillations; this nonlinearity leads to the generation of higher-order pump terms that complicate the system dynamics, but can be mitigated now that they have been understood. My results validate a recent theoretical model for the classical, non-linear dynamics of parametric resonance, and helps determine workable design parameters. Finally, I helped develop a linearized model −-− the "pumpistor" - describing this device in terms of a flux-controlled impedance. This will be useful when designing more complex circuits. One goal of this work is to demonstrate single-shot measurements on superconducting qubits (quantum bits of information). We will use the parametric resonator as a threshold discriminator, associating the qubit's two energy eigenstates with the parametric oscillations either turning on or not. This would be a very useful device in the quantum engineer's toolbox when designing systems for quantum information processing and communication.
Microwave kinetic inductance detectors (MKID) are superconducting broadband direct detectors. If a superconducting thin film patterned into a resonator is illuminated with photons, Cooper pairs break up and the kinetic inductance of the film changes. This shifts the resonance frequency downwards and the dissipation of the resonator increases, which can be detected in the phase and amplitude of a transmitted signal. \n \nIn this thesis, a waveguide coupled MKID is designed and simulated. 350 GHz radiation is coupled into a copper waveguide via a horn antenna. A waveguide probe leads the signal onto a 9 µm silicon membrane where it is absorbed in a 40 nm superconducting aluminum film which is the inductive part of a superconducting resonator. The capacitor of the resonator is made of niobium. Two versions of the device are developed, a transmission line resonator and a lumped element resonator design. The new design will enable an accurate understanding of the optical sensitivity of MKIDs and allow comparison of different resonator materials. Since two different resonator types are used, the direct comparison of transmission line and lumped resonators will also be possible. \n \nA measurement setup is developed including an ADR cryostat to cool MKID devices down to below 40 mK. An analog readout system using either a vector network analyzer or an IQ mixer is designed and built. The necessary software to control the ADR, the temperature monitoring, the readout signal generation and detection and the signal acquisition of the setup is also developed. \n \nThe waveguide coupled MKID design is fabricated in our in-house microfabrication laboratory and measured in the new setup. In my measurements, the devices do not show a resonance feature. The VNA and DC measurements are analyzed to determine a plausible hypothesis of the failure. The devices are diagnosed for critical issues during fabrication which will be addressed in a future iteration. \n \nTo verify the measurement setup, a test device of the IRAM NIKA 2 MKID camera is measured and the complete analysis pipeline is exercised. The quasi-particle lifetime in the aluminum thin films is measured and a dark and optical noise equivalent power are determined. The results are within the uncertainty comparable to measurements of IRAM themselves. \n \nA test chip designed in my master thesis that contains eight NbTiN resonators is measured in the new setup and non-linear effects under strong readout power are studied. Parametric amplification and oscillation of a resonator are shown qualitatively.