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arXiv:2208.02102 · Review of Scientific Instruments

An apparatus for in-vacuum loading of nanoparticles into an optical trap

Evan Weisman, Chethn Galla, Cris Montoya, Eduardo Alejandro, Jason Chu-Shern Lim, Melanie Beck, George Winstone, Alexey Grinin, William Eom, Andrew A. Geraci

Published Nov 1, 2022• 14 citations
arXivHTMLPDF

Abstract

We describe the design, construction, and operation of an apparatus that utilizes a piezoelectric transducer for in-vacuum loading of nanoparticles into an optical trap for use in levitated optomechanics experiments. In contrast to commonly used nebulizer-based trap-loading methods that generate aerosolized liquid droplets containing nanoparticles, the method produces dry aerosols of both spherical and high-aspect ratio particles ranging in size by approximately two orders of magnitude. The device has been shown to generate accelerations of order 107 g, which is sufficient to overcome stiction forces between glass nanoparticles and a glass substrate for particles as small as 170 nm in diameter. Particles with sizes ranging from 170 nm to ∼10μm have been successfully loaded into optical traps at pressures ranging from 1 bar to 0.6 mbar. We report the velocity distribution of the particles launched from the substrate, and our results indicate promise for direct loading into ultra-high-vacuum with sufficient laser feedback cooling. This loading technique could be useful for the development of compact fieldable sensors based on optically levitated nanoparticles as well as matter–wave interference experiments with ultra-cold nano-objects, which rely on multiple repeated free-fall measurements and thus require rapid trap re-loading in high vacuum conditions.

DOI
10.1063/5.0118083

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We describe the design, construction, and operation of an apparatus that utilizes a piezoelectric transducer for in-vacuum loading of nanoparticles into an optical trap for use in levitated optomechanics experiments. In contrast to commonly used nebulizer-based trap-loading methods that generate aerosolized liquid droplets containing nanoparticles, the method produces dry aerosols of both spherical and high-aspect ratio particles ranging in size by approximately two orders of magnitude. The device has been shown to generate accelerations of order 107 g, which is sufficient to overcome stiction forces between glass nanoparticles and a glass substrate for particles as small as 170 nm in diameter. Particles with sizes ranging from 170 nm to ∼10μm have been successfully loaded into optical traps at pressures ranging from 1 bar to 0.6 mbar. We report the velocity distribution of the particles launched from the substrate, and our results indicate promise for direct loading into ultra-high-vacuum with sufficient laser feedback cooling. This loading technique could be useful for the development of compact fieldable sensors based on optically levitated nanoparticles as well as matter–wave interference experiments with ultra-cold nano-objects, which rely on multiple repeated free-fall measurements and thus require rapid trap re-loading in high vacuum conditions.
Many experiments in the field of optical levitation with nanoparticles today are limited by the available technologies for particle loading. Here, we introduce a particle loading method that solves the main challenges, namely deterministic positioning of the particles and clean delivery at ultra-high vacuum levels as required for quantum experiments. We demonstrate the efficient loading, positioning, and repositioning of nanoparticles in the range of 100–755 nm diameter into different lattice sites of a standing wave optical trap, as well as direct loading of 143–365 nm diameter particles into ultra-high vacuum, down to an unprecedented pressure below 10−9 mbar. Our method relies on the transport of nanoparticles within a hollow-core photonic crystal fiber using an optical conveyor belt, which can be precisely positioned with respect to the target trap. Our work opens the path for increasing nanoparticle numbers in the study of multiparticle dynamics and high turn-around times for exploiting the quantum regime of levitated solids in ultra-high vacuum.
Accurate delivery of small targets in high vacuum is a pivotal task in many branches of science and technology. Beyond the different strategies developed for atoms, proteins, macroscopic clusters, and pellets, the manipulation of neutral particles over macroscopic distances still poses a formidable challenge. Here, we report an approach based on a mobile optical trap operated under feedback control that enables cooling and long range 3D manipulation of a silica nanoparticle in high vacuum. We apply this technique to load a single nanoparticle into a high-finesse optical cavity through a load-lock vacuum system. We foresee our scheme to benefit the field of optomechanics with levitating nano-objects as well as ultrasensitive detection and monitoring.
We perform free-fall experiments with a charge-neutral, optically levitated nanoparticle. This is achieved using an optical tweezer that can be rapidly toggled on and off and vertically displaced, enabling the particle to be released and recaptured after each free fall. The particle is insensitive to electric fields due to its charge neutrality and, during free evolution, is not subject to photon recoil heating. We achieve free-fall durations of up to 0.25 ms and observe a nearly two hundred-fold increase in the particle's position uncertainty at recapture. The current limit on the free-fall time arises from the performance of the initial cooling step. By implementing linear feedback techniques and reducing the background pressure, we expect to perform millisecond-scale free-fall experiments in ultra-high vacuum, opening new opportunities for generating large delocalizations of levitated objects.
We perform free-fall experiments with a charge-neutral, optically levitated nanoparticle. This is achieved using an optical tweezer that can be rapidly toggled on and off and vertically displaced, enabling the particle to be released and recaptured after each free fall. The particle is insensitive to electric fields due to its charge neutrality and, during free evolution, is not subject to photon recoil heating. We achieve free-fall durations of up to 0.25 ms and observe a nearly two hundred-fold increase in the particle's position uncertainty at recapture. The current limit on the free-fall time arises from the performance of the initial cooling step. By implementing linear feedback techniques and reducing the background pressure, we expect to perform millisecond-scale free-fall experiments in ultra-high vacuum, opening new opportunities for generating large delocalizations of levitated objects.
We perform free-fall experiments with a charge-neutral, optically levitated nanoparticle. This is achieved using an optical tweezer that can be rapidly toggled on and off and vertically displaced, enabling the particle to be released and recaptured after each free fall. The particle is insensitive to electric fields due to its charge neutrality, and during free evolution, is not subject to photon recoil heating. We achieve free-fall durations of up to 0.25ms and observe a nearly 200-fold increase in the particle's position uncertainty at recapture. The current limit on the free-fall time arises from the performance of the initial cooling step. By implementing linear feedback techniques and reducing the background pressure, we expect to perform millisecond-scale free-fall experiments in an ultrahigh vacuum, opening new opportunities for generating large delocalizations of levitated objects.
We demonstrate optical levitation and feedback cooling of a silica nanoparticle (radius = 78~nm) trapped within a radial vector beam (RVB) in high vacuum. Radial vector beams, when focused by a high-NA lens, produce a smaller focal spot than conventional Gaussian beams, yielding tighter optical potentials and potentially reduced photon-recoil heating rates. A vortex wave plate was used to generate the RVB using an aspheric lens (NA = 0.77) to form the trap. Cold-damping feedback was used to cool the center of mass motion in the radial and axial trap directions to temperatures in the mK range. At higher temperatures and pressures, additional trap frequencies arising from the nonlinear RVB optical potential are observed. This demonstration is a step toward exploiting structured light for levitated quantum optomechanics where these traps can be used to suppress bulk and motional heating.