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arXiv:0905.1726 · Nano Letters

Current-Phase Relationship, Thermal and Quantum Phase Slips in Superconducting Nanowires Made on a Scaffold Created Using Adhesive Tape

Myung-Ho Bae, Robert C. Dinsmore, Thomas Aref, Matthew Brenner, Alexey Bezryadin

Published Apr 3, 2009• 42 citations
arXivHTMLPDF

Abstract

Quantum phase slippage (QPS) in a superconducting nanowire is a new candidate for developing a quantum bit [Mooij et al. New J. Phys. 2005, 7, 219; Mooij et al. Nat. Phys. 2006, 2, 169; Khlebnikov http://arxiv.org/abs/quant-ph/0210019 2007]. It has also been theoretically predicted that the occurrence of QPS significantly changes the current-phase relationship (CPR) of the wire due to the tunneling between topologically different metastable states [Khlebnikov Phys. Rev. B 2008, 78, 014512]. We present studies on the microwave response of the superconducting nanowires to reveal their CPRs. First, we demonstrate a simple nanowire fabrication technique, based on commercially available adhesive tapes, which allows making thin superconducting wire from different metals. We compare the resistance vs temperature curves of Mo(76)Ge(24) and Al nanowires to the classical and quantum models of phase slips. In order to describe the experimentally observed microwave responses of these nanowires, we use the McCumber-Stewart model [McCumber J. Appl. Phys. 1968, 39, 3113; Stewart Appl. Phys. Lett. 1968, 12, 277], which is generalized to include either classical or quantum CPR.

DOI
10.1021/nl803894m

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Quantum phase slippage (QPS) in a superconducting nanowire is a new candidate for developing a quantum bit [Mooij et al. New J. Phys. 2005, 7, 219; Mooij et al. Nat. Phys. 2006, 2, 169; Khlebnikov http://arxiv.org/abs/quant-ph/0210019 2007]. It has also been theoretically predicted that the occurrence of QPS significantly changes the current-phase relationship (CPR) of the wire due to the tunneling between topologically different metastable states [Khlebnikov Phys. Rev. B 2008, 78, 014512]. We present studies on the microwave response of the superconducting nanowires to reveal their CPRs. First, we demonstrate a simple nanowire fabrication technique, based on commercially available adhesive tapes, which allows making thin superconducting wire from different metals. We compare the resistance vs temperature curves of Mo(76)Ge(24) and Al nanowires to the classical and quantum models of phase slips. In order to describe the experimentally observed microwave responses of these nanowires, we use the McCumber-Stewart model [McCumber J. Appl. Phys. 1968, 39, 3113; Stewart Appl. Phys. Lett. 1968, 12, 277], which is generalized to include either classical or quantum CPR.
Quantum phase slips (QPS) or the macroscopic quantum tunneling (MQT) of a nanowire’s order parameter through an activation energy barrier have remained the subject of intense debate for many years. They are expected to occur at low enough temperature where thermally activated phase slips (TAPS) have been frozen out in analogy with Josephson junctions where the macroscopic tunneling of phase at low temperatures has been conclusively experimentally demonstrated. We address this question by following a similar experimental strategy to that employed for establishing MQT in JJs. By measuring switching current distributions, we can probe the phase slip rate and determine if it corresponds to thermal activation or quantum tunneling. Having established that the behavior we see is consistent with being in the quantum regime, we can alter properties of the nanowires and see if the response is consistent with the expectations of the quantum model. To do this we employ an in-situ modification technique using high bias voltage pulses. Using these pulses, we can change resistance, critical temperature, critical current and morphology of the nanowire. We can also change the shunting capacitance of the nanowire by altering the photolithography step used to create the nanowires electrodes. The resulting response of the nanowires agrees well with being in the quantum tunneling dominated regime. An interesting side benefit of the pulsing technique is that we can exactly set the nanowires switching current to a desired value. This may be instrumental in the development of superconducting nanowire qubits.
The topic of superconducting nanowires has recently been an interesting field of research which has included the study of the superconductor to insulator transition (SIT), the observation of macroscopic quantum behavior such as quantum phase slips (QPS), and the potential use of nanowires as qubits. Superconducting coplanar microwave waveguide resonators have also become a popular way of studying superconducting junctions and qubits, as they provide an extremely low noise environment. For example, superconducting two-dimensional Fabry-Perot resonators have been used by other groups to make non-demolition measurements of a qubit. The motivation of this thesis will be the merging of the fields of superconducting nanowires and the technique of using superconducting microwave resonators to study junctions by incorporating a nanowire into the resonator itself at a current anti-node. By doing this, the nonlinear effects of the nanowire can be studied which may find application in single photon detectors, mixers, and the readout of qubits. We also employ the technique of molecular templating to fabricate some of the thinnest superconducting nanowires ever studied (down to ~ 5 nm in diameter in some cases). In this thesis, we extend the understanding of the nonlinear properties of a nanowire- resonator system and investigate a new type of nonlinearity that involves a pulsing regime between the superconducting and normal phases of the nanowire. We develop a model, which describes the results quantitatively and by modeling the system, we are able to extract information regarding the relaxation time of the nanowire back into the superconducting state. We also study double nanowire-resonator systems where two closely spaced parallel nanowires interrupt the resonator center conductor and form a loop where vortex tunneling processes can occur. Using a double nanowire-resonator we are able to observe the Little-Parks effect at low temperatures (where the resistance of the wires is immeasurably low) and are able to confirm the multivalued nature of the current phase relationship (CPR) in nanowires. Additionally, we observe an anomalous transmission regime where the periodic pulsing is replaced by stochastic amplitude fluctuations. In addition to microwave measurements on nanowires, we also study the normal state in resistively shunted nanowires with dc measurements where the inclusion of a shunt resistor is observed to change the nature of the normal state from the Joule heated state to a state that preserves phase coherence. Finally, the statistics on switching current events in graphene proximity junctions are analyzed and compared to the well known results for Josephson junctions. Only thermal activation (and no macroscopic quantum tunneling) is observed in graphene proximity superconducting junctions down to temperatures of ~ 300 mK.
Abstract Quantum phase slip (QPS) is an important effect that occurs in one-dimensional (1D) or quasi-1D superconducting (SC) materials. Due to the extremely high requirements on the uniformity and quality of SC nanowires, it is currently very challenging to obtain repeatable and controllable QPS devices. Here, we report a systematic study of the QPS effect in NbN SC nanowires. High-quality NbN nanowires with different widths are fabricated by combining the processes of photo-lithography, electron beam lithography, and inductively coupled plasma etching. It is found that the electrical transport of the nanowires showed a systematic variation with the wire width, and a clear evolution from single to multiple QPS events with the decrease in wire width is uncovered at low temperatures. Based on these experimental results, the phase diagram reflecting the evolution of the physical states of the nanowires with wire width and temperature is obtained. In addition, we observed the features of the critical voltage, which is a characteristic of the occurrence of coherent QPS (cQPS), in samples with a width of 36 nm in the multiple QPS region. It is worth noting that this cQPS behavior was detected in a non-high-impedance environment.
We present a detailed report of microwave irradiation of ultranarrow superconducting nanowires. In our nanofabricated circuits containing a superconducting NbSi nanowire, a dc blockade of current flow was observed at low temperatures below a critical voltage Vc{V}_{\mathrm{c}}Vc​, a strong indicator of the existence of quantum phase-slip (QPS) in the nanowire. We describe the results of applying microwaves to these samples, using a range of frequencies and both continuous-wave and pulsed drive, in order to search for dual Shapiro steps which would constitute an unambiguous demonstration of quantum phase-slip. We observed no steps, and our subsequent thermal analysis suggests that the electron temperature in the series CrO resistors was significantly elevated above the substrate temperature, resulting in sufficient Johnson noise to wash out the steps. To understand the system and inform future work, we have constructed a numerical model of the dynamics of the circuit for dc and ac bias (both continuous-wave and pulsed drive signals) in the presence of Johnson noise. Using this model, we outline important design considerations for device and measurement parameters which should be used in any future experiment to enable the observation of dual Shapiro steps at experimentally accessible temperatures and, thus, lead to the development of a QPS-based quantum current standard.
In quasi-one-dimensional nanowires, superconductivity is destroyed by phase slip events. Phase slips can be caused by thermal activation over a free energy barrier (TAPS) or quantum tunneling through the barrier (QPS). Quantum phase slip is an example of macroscopic quantum tunneling. Here, we report the observation of QPS experimentally separated from interference of TAPS in aluminum nanowires. This separation between the low-temperature QPS and the high-temperature TAPS regions is made possible by a phase slip free superconducting region stabilized by the dissipative environment viz. the normal electrodes. Individual QPSs are detected by means of a single-shot voltage measurement protocol, in which they appear as stochastic switching events from the superconducting to the normal state.